Cleaning of hollow fibre filters

• US 4,921,610 A
• Filed: 05/04/1988
• Issued: 05/01/1990
• Est. Priority Date: 09/04/1986
• Status: Expired due to Fees

• Current Assignee: Memtec Ltd. (Danaher Corporation)
• Original Assignee: Memtec Ltd. (Danaher Corporation)
• Inventors: Barton, Noel, Ford, Douglas L.
• Primary Examiner(s): SPEAR JR, FRANK
• Application Number:
  US07/236,711
• Time in Patent Office: 727 Days
• Field of Search: 210/411, 210/409, 210/636, 210/140, 210/414, 210/321.69, 210/138, 210/139, 210/500.23
• US Class Current: 210/636
• CPC Class Codes: B01D 2313/48 Mechanisms for switching between regular separation operations and washing
• CPC Class Codes: B01D 2321/04 Backflushing
• CPC Class Codes: B01D 2321/16 Use of chemical agents
• CPC Class Codes: B01D 2321/18 Use of gases
• CPC Class Codes: B01D 61/145 Ultrafiltration
• CPC Class Codes: B01D 61/22 Controlling or regulating
• CPC Class Codes: B01D 63/02 Hollow fibre modules
• CPC Class Codes: B01D 65/02 Membrane cleaning or sterilisation ; Membrane regeneration

Abstract

In the cleaning and removal of solids from microporous hollow fibre filters by a series of chemical cleaning cycles, the optimum time and pattern of the cleaning cycles is calculated from the rate of diminution in filtrate flow rate and the time and filtrate lost in each cycle.

Claims

1. A method of operating a microporous hollow fibre filter comprising the steps of:

(i) applying a liquid feedstock to be filtered to the outer surface of the filters whereby;

(a) some of the liquid passes through the walls of the fibres to be drawn off as clarified liquid or filtrate from the fibre lumens,

(b) at least some of the solids are retained on or in the fibres with the non-retained solids being removed from the filter with the remainder of the liquid

(ii) discharging the retained solids by applying a pressurised liquid and/or gas backwash,

(iii) calculating from the rate of diminution of flow of filtrate after each application of pressurised liquid and/or gaseous backwash an equation expressing the relationship between filtrate flow and time, and,

(iv) allowing for the time lost in each backwash cycle and the amount of filtrate lost in each backwash cycle,

(v) calculating from the filtrate loss, the time loss and the the relationship between filtrate flow and time, the optimum time and pattern of application of sequential liquid or gaseous backwashes, and,

(vi) effecting the backwash at the optimum time.

2. A method according to claim 1 and including the steps of implementing a chemical cleaning of the fibres after a series of backwashes and calculating from the rate of decrease of peak value of filtrate flow after each backwash cycle and the amount of time and filtrate lost in chemical cleaning, the optimum time for shut down for chemical cleaning.

3. Apparatus for filtering a feedstock and for carrying out a predetermined frequency of liquid and/or gaseous backwashes of the filtering apparatus comprising:

(i) means for applying a feedstock to be filtered to the outside surface of porous hollow fibres contained in a shell or housing, and for withdrawing clarified liquid or filtrate from the lumens of the fibres,

(ii) means for applying through the fibre lumens liquid and/or gaseous backwashes that pass through the walls of the fibres,

(iii) means for measuring the rate of decrease in filtrate flow rate,

(iv) means for calculating the optimal backwash frequency taking account of the rate of decrease in filtrate flow rate, loss of filtrate and time involved in a backwash cycle, and,

(v) means for applying the calculated optimal backwash frequency to the fibres in the filter.

4. Apparatus for automatically applying a predetermined pattern of sequential liquid and gaseous backwashes whilst maintaining a dynamic membrane layer on the surface of the filter fibres, as described above said apparatus comprising:

(i) means for applying a feedstock to be filtered to the outside surface of porous hollow fibres contained in a shell or housing and for withdrawing filtrate from the lumens of the fibres,

(ii) means for applying through the fibre lumens liquid and gaseous backwashes that pass through the walls of the fibres,

(iii) means for automatically applying the predetermined backwash pattern to the fibres in the filter,

(iv) means for detecting the quality of the filtrate and redirecting it back to the feedstock if the quality is unacceptable,

(v) means for measuring the rate of decrease in filtrate flow rate, or flux,

(vi) means for calculating the optimal backwash frequency taking account of the loss of filtrate and time involved in a backwash cycle, and,

(vii) means for applying the calculated optimal backwash frequency to the fibres in the filter.

5. Apparatus for filtering a feedstock and for carrying out liquid and/or gaseous backwash cycles, said apparatus comprising:

(i) means for applying a feedstock to be filtered to the outside surface of porous hollow fibres contained in a shell or housing, and for withdrawing clarified liquid or filtrate from the lumens of the fibres,

(ii) means for applying through the fibre lumens liquid and/or gaseous backwashes that pass through the walls of the fibres,

(iii) means for determining the instantaneous filtrate flow rate at any point in time,

(iv) means for measuring the integrated filtrate flux over time since the last backwash or chemical cleaning cycle,

(v) means for applying a backwash cycle to the fibres when the integrated filtrate flux equals the instantaneous filtrate flux multiplied by the sum of the period of time elapsed since the last backwash plus the time taken for the backwash cycle.