Freeze drying apparatus with additional condensation surface and refrigeration source

• US 4,949,473 A
• Filed: 07/29/1988
• Issued: 08/21/1990
• Est. Priority Date: 07/29/1987
• Status: Expired due to Term

• Current Assignee: Finn-Aqua Santasalo-Sohlberg GmbH (GEA Group AG)
• Original Assignee: Leybold Aktiengesellschaft
• Inventors: Steinkamp, Heinrich
• Primary Examiner(s): Bennet, Henry A.
• Assistant Examiner(s): SOLLECITO, JOHN M
• Application Number:
  US07/226,536
• Time in Patent Office: 753 Days
• Field of Search: 34/5, 34/15, 34/92, 62/332, 62/333, 62/514, 62/45, 62/54
• US Class Current: 34/92
• CPC Class Codes: F26B 5/06 the process involving freezing

Abstract

A freeze drying apparatus includes a vacuum chamber, an evacuation system, and an additional condensation surface which may serve as a fail-safe condensation surface. The additional condensation surface is connected by way of a valve with a reservoir container containing a low boiling point coolant, such as liquid nitrogen. If, due to a malfunction, the pumping power of the evacuation system fails, the valve is opened so that the additional condensation surface takes over the pumping work for the commodity charge positioned in the vacuum chamber. The additional condensation surface may be positioned in a condenser of the evacuation system, in the vacuum chamber, or in a separate chamber connected to the vacuum chamber.

Claims

1. A freeze drying apparatus, comprising:

a vacuum chamber;

an evacuation system comprised of a condenser and a vacuum pump connected by a conduit including a second valve, and a refrigeration machine, wherein the condenser has at least one condensation surface supplied by the refrigeration machine and wherein the condenser is connected to the vacuum chamber by a conduit including a third valve;

a reservoir container containing a coolant which is a liquid having a low boiling point; and

an additional condensation surface which is connected to the reservoir container by a conduit including a first valve and which is disposed in the condenser.

2. The freeze drying apparatus according to claim 1, wherein the first valve, the second valve, and the third are equipped with electrical or electropneumatic actuating devices in such a manner that, upon a malfunction or loss of current, the second valve takes on its closed position and the first valve and the third valve take on their open positions or retain their open positions.

3. The freeze drying apparatus according to claim 1, wherein the reservoir container for the coolant has associated means for generating an increased pressure within the reservoir container.

4. The freeze drying apparatus according to claim 1, wherein the coolant in the reservoir container is liquid nitrogen.

5. A freeze drying apparatus, comprising:

a vacuum chamber;

an evacuation system comprised of a condenser and a vacuum pump connected by a conduit including a second valve, wherein the condenser is connected to the vacuum chamber by a conduit including a third valve;

a reservoir container containing a coolant which is a liquid having a low boiling point; and

an additional condensation surface which is disposed in a chamber which is interconnected by a conduit to the vacuum chamber, and which is connected to the reservoir container by a conduit including a first valve.

6. A freeze drying apparatus, comprising:

a vacuum chamber;

an evacuation system comprised of a condenser and a vacuum pump connected by a conduit including a second valve, wherein the condenser is connected to the vacuum chamber by a conduit including a third valve;

a reservoir container containing a coolant which is a liquid having a low boiling point; and

an additional condensation surface which is connected to the reservoir container by a conduit including a first valve,

wherein the first valve and the third valve are equipped with electrical or electropneumatic actuating devices in such a manner that, upon a malfunction or loss of current, the first valve takes on its open position and the third valve takes on its closed position.