Method for preparing improved lithium-silicate glare-reducing coating for a cathode-ray tube

• US 4,965,096 A
• Filed: 08/25/1988
• Issued: 10/23/1990
• Est. Priority Date: 08/25/1988
• Status: Expired due to Term

• Current Assignee: RCA Licensing Corporation
• Original Assignee: RCA Licensing Corporation
• Inventors: Bartch, Donald W., Deal, Samuel B.
• Primary Examiner(s): Morgenstern, Norman
• Assistant Examiner(s): King, Roy V.
• Application Number:
  US07/236,403
• Time in Patent Office: 789 Days
• Field of Search: 427/165, 427/164, 427/64, 427/314, 427/168, 427/110, 427/353, 427/354, 427/380, 427/226, 313/479, 313/478, 428/428
• US Class Current: 427/165
• CPC Class Codes: C03C 17/25 by deposition from the liquid phase
• CPC Class Codes: C03C 2217/23 Mixtures
• CPC Class Codes: C03C 2218/113 by sol-gel processes
• CPC Class Codes: H01J 29/24 Supports for luminescent material
• CPC Class Codes: H01J 29/896 Anti-reflection means, e.g. eliminating glare due to ambient light
• CPC Class Codes: H01J 9/20 Manufacture of screens on or from which an image or pattern is formed, picked up, converted or stored; Applying coatings to the vessel

Abstract

An antistatic, glare-reducing coating, as for the surface of the viewing surface of a CRT is prepared by (a) warming a glass support surface above room temperature, (b) coating a surface of the warm support with an aqueous solution containing a lithium-stabilized silica sol and an inorganic metallic compound, and drying the deposited coating, (c) heating the glass support surface and the coating to a temperature of about 65° C. for about 30 seconds, and (d) washing and then drying the coating.

Claims

1. A method for preparing an optical viewing screen having a glare-reducing viewing surface comprising

(a) warming a glass support to a temperature of about 50°

C.,

(b) coating a surface of said warm support with an aqueous solution containing lithium-stabilized silica sol, and drying the deposited coating,

(c) exposing said surface of said support and said deposited coating to a heat source for about 30 seconds to raise said surface and said deposited coating to a temperature of about 65°

C.,

(d) washing said dry coating with water, and

(e) drying said coating.

3. The method defined in claim 1 wherein, at step (a), said glass support is heated to temperatures of about 48°

to 50°

C.

2. A method for preparing an optical viewing screen having an antistatic, glare-reducing viewing surface for a cathode-ray tube comprising

(a) warming a glass faceplate to a temperature of about 50°

C.,

(b) coating an exterior surface of said warm faceplate with an aqueous solution containing lithium-stabilized silica sol and an inorganic metallic compound selected from the group consisting of palladium sulfate, tin sulfate, tin chloride and gold chloride present in a concentration within the range of 0.005 to 0.02 weight percent for imparting antistatic characteristics to said coating, and drying the deposited coating,

(c) reheating the exterior surface of said faceplate and said deposited coating to a temperature of about 65°

C. for 30 seconds without substantially heating the body of said faceplate,

(d) washing said dry coating with water, and

(e) drying said coating.

4. The method defined in claim 2 wherein, at step (a), said glass faceplate is heated to temperatures of about 48°

to 50°

C.

5. A method for preparing an optical viewing screen having an antistatic, glare-reducing viewing surface for a cathode-ray tube comprising

(a) warming a glass faceplate of said tube to about 48°

to 50°

C.,

(b) coating an exterior surface of said warm faceplate with an aqueous solution containing lithium-stabilized silica sol and a palladium compound in a concentration within the range of 0.005 to 0.02 weight percent for imparting an antistatic characteristic to said coating, and drying the deposited coating,

(c) reheating the exterior surface of said faceplate for about 30 seconds to a temperature of about 65°

C. without substantially heating the body of the faceplate,

(d) washing said dry coating with water, and

(e) drying said coating.