Point of use deionized water purification unit

• US 5,024,766 A
• Filed: 11/09/1988
• Issued: 06/18/1991
• Est. Priority Date: 11/09/1988
• Status: Expired due to Fees

• Current Assignee: Shahzad Mahmud
• Original Assignee: Shahzad Mahmud
• Inventors: Mahmud, Shahzad
• Primary Examiner(s): Cintins, Ivars
• Application Number:
  US07/269,219
• Time in Patent Office: 951 Days
• Field of Search: 210/663, 210/668, 210/669, 210/748, 210/194, 210/196, 210/253, 210/258, 210/259, 210/266, 210/284, 210/900, 210/686, 210/805, 210/806, 210/142, 210/195.1, 210/202
• US Class Current: 210/668
• CPC Class Codes: C02F 1/001 Processes for the treatment of water whereby the filtration technique is of importance C02F1/44 takes precedence; construction of filters in general B01D24/00 - B01D41/00
• CPC Class Codes: C02F 1/008 Control or steering systems not provided for elsewhere in subclass C02F
• CPC Class Codes: C02F 1/32 with ultraviolet light
• CPC Class Codes: C02F 1/325 Irradiation devices or lamp constructions
• CPC Class Codes: C02F 1/42 by ion-exchange ion-exchange in general B01J
• CPC Class Codes: C02F 1/78 with ozone C02F1/4672 takes precedence
• CPC Class Codes: C02F 2001/427 using mixed beds
• CPC Class Codes: C02F 2103/04 for obtaining ultra-pure water
• CPC Class Codes: C02F 2201/326 Lamp control systems
• CPC Class Codes: C02F 2201/782 Ozone generators
• CPC Class Codes: C02F 2209/00 Controlling or monitoring parameters in water treatment
• CPC Class Codes: C02F 2209/006 comprising a software program or a logic diagram
• CPC Class Codes: C02F 2209/05 Conductivity or salinity
• CPC Class Codes: C02F 2209/20 Total organic carbon [TOC]
• CPC Class Codes: C02F 9/20 Portable or detachable small-scale multistage treatment devices, e.g. point of use or laboratory water purification systems
• CPC Class Codes: Y10S 210/90 Ultra pure water, e.g. conductivity water

Abstract

The deionized water purification of this invention is a small compact unit which is inserted between the purified deionized water distribution line in a plant water purification system and the inlet of a point of use apparatus. The small compact modular point of use deionized water purification unit reduces the total organic contaminant loading, the particulate loading, and the ionic contaminants in the purified deionized water from the plant purification system. The purification unit of this invention also includes means for sterilization of the point of use deionized water purification unit and a new technique for preventing damage to the ozone generator used in the sterilization process.

Claims

1. A point of sue water purification apparatus for insertion in a purified water supply line at the location of another apparatus requiring high purity water, the water supply line normally supplying such another apparatus with deionized purified water, said deionized purified water having impurities such as bacteria, particulates, organic carbon contaminants, and a resistivity of about 17-18 megohm-cm, said point of use water purification apparatus comprising:

means, operatively connectable to such a water supply line, for generating a flow of water having an approximately constant pressure, the flow generating means having an inlet and an outlet wherein the inlet receives water from such a water supply line and the approximately constant water pressure is generated at the outlet;

means, operatively connected to said generating means, for reducing organic carbon contaminants and having an inlet and an outlet wherein water received at the inlet of the organic carbon contaminant reducing means from said generating means has a first level of organic carbon contaminants and water at the outlet of the organic contaminant reducing means has a second level of organic carbon contaminants, the second organic carbon contaminants level being less than the first organic carbon contaminants level;

means, operatively connected to the organic carbon contaminant reducing means, for filtering water and having an inlet and an outlet wherein water from said organic carbon contaminant reducing means, received by the inlet of said filtering means, has a first level of particulates and water at the outlet of said filtering means has a second level of particulates which is lower than said first level;

coupling means, operatively connected to said filtering means and operatively connectable to such another apparatus, for providing the water from the filter means to such another apparatus upon demand;

means, operatively coupled to the coupling means, for polishing water and having an inlet and an outlet wherein water from said coupling means is provided to the inlet of the polishing means and the polished water is provided at the outlet of the polishing means;

means, operatively connected to said polishing means, for sterilizing and having an inlet coupled to the outlet of said polishing means and an outlet, said outlet being coupled to the inlet of said generating means to form a recirculation path through said point of use water purification apparatus; and

control means, operatively coupled to said organic carbon contaminant reducing means, to said polishing means and to said sterilization means, for selecting the mode of operation of said point of use water purification apparatus wherein in a first mode of operation, the point of use water purification apparatus provides high purity water to such another apparatus, and in a second mode of operation, said recirculation path through the point of use water purification apparatus is sterilized.

2. The point of use water purification apparatus of claim 1 wherein the generating means comprises a centrifugal booster pump.

3. The point of use water purification apparatus of claim 2 wherein the centrifugal booster pump provides a water pressure at the pump outlet of approximately about 17-32 psig at a flow of approximately 40-75 gpm.

4. The point of use water purification of claim 3 wherein the flow is approximately 75 gpm.

5. The point of use water purification apparatus of claim 4 wherein the centrifugal booster pump is constructed of polyvinylidene fluoride.

6. The point of use water purification apparatus of claim 1 wherein the means for reducing organic carbon contamination comprises an ultraviolet lamp unit.

7. The point of use water purification apparatus of claim 6 wherein the ultraviolet lamp unit generates radiation having about a 185 nanometer wavelength.

8. The point of use water purification apparatus of claim 6 wherein the ultraviolet lamp unit reduces the organic carbonic contaminants for flows through the lamp unit of about 40-100 gpm.

9. The point of use water purification apparatus of claim 1 wherein the means for filtering water comprises a filter housing containing about 0.2 micron filters.

10. The point of use water purification apparatus as in claim 9 wherein the filters are ozone resistant.

11. The point of use water purification apparatus of claim 1 wherein the means for polishing water comprises two polishers connected in parallel wherein each polisher contains resins such that said polishers are operative for flow through said polishers of approximately 25-35 gpm.

12. The point of use water purification apparatus as in claim 11 wherein each polisher is a mixed bed polisher.

13. The point of use water purification apparatus as in claim 12 wherein the bed of each polisher contains approximately about 60-70% anion resin and about 30-40% cation resin.

14. A point of use water purification apparatus as in claim 13 wherein the mixed ion bed polisher contains about 70% anion resins and about 30% cation resins.

15. The point of use water purification apparatus as in claim 1 wherein the sterilizing means further comprises:

means for regulating water pressure having an inlet and an outlet wherein the inlet of the water pressure regulating means comprises the inlet of the sterilizing means and the outlet of the water pressure regulating means comprise the outlet of the sterilizing means; and

means, operatively connected in parallel with the water pressure regulating means, for induction of a sterilizing agent wherein the sterilizing agent is introduced into the means for induction at a first pressure and the means for regulating water pressure drops the water pressure in said water purification apparatus so that the water pressure in said induction means is less than the first pressure.

16. The point of use water purification apparatus as in claim 15 wherein the sterilizing agent comprises ozone.

17. The point of use water purification apparatus as in claim 16 wherein the sterilizing means further comprises:

controllable means, connectable to a source of oxygen and operatively coupled to the induction means, for generating ozone wherein the controllable ozone generating means changes oxygen from such a source of oxygen to ozone and provides the ozone to said induction means.

18. The point of use water purification apparatus as in claim 17 further comprising:

a first controllable valve coupled between the outlet of the second coupling means and the inlet of the polishing means;

a second controllable valve coupled between the outlet of said second coupling means and the inlet of the means for regulating water pressure; and

a third controllable valve in parallel with the organic carbon contaminant reducing means wherein said control means is operatively connected to the first, second and third controllable valves and the means for generating ozone and

in said first mode of operation of the point of use water purification apparatus, the control means closes the second and third controllable valves, opens the first controllable valve and disables the means for generating ozone, and

in said second mode of operation, the control means closes the first controllable valve, opens the second and third controllable valves and enables the ozone generator.

19. A method for purifying water having about a 17-18 megohm-cm resistivity in a point of use water supply line comprising the steps of:

(a) removing organic contaminants from said water;

(b) filtering the water after removal of the organic contaminants; and

(c) providing the filtered water to a point of use apparatus.

20. The method of claim 19 further comprising the step of:

recycling unused filtered water through steps (a)-(c).

21. The method of claim 19 further comprising the step of polishing the water after removal of organic contaminants.