Metal coating method

• US 5,032,421 A
• Filed: 08/21/1990
• Issued: 07/16/1991
• Est. Priority Date: 08/21/1990
• Status: Expired due to Term

• Current Assignee: AMP Incorporated (Johnson Controls International plc)
• Original Assignee: AMP Incorporated (Johnson Controls International plc)
• Inventors: Sampath, Walajabad S., Wilbur, Paul J., Subramanian, Nagarajan, Sarma, Srinivasan V.
• Primary Examiner(s): PIANALTO, BERNARD D
• Application Number:
  US07/570,481
• Time in Patent Office: 329 Days
• Field of Search: 427/38, 427/39, 427/124, 427/42, 427/125, 427/251, 427/255.5, 427/255.7, 427/261, 427/287, 427/290, 427/295, 427/319, 427/321, 427/327
• US Class Current: 427/535
• CPC Class Codes: C23C 14/022 by means of bombardment with energetic particles or radiation
• CPC Class Codes: C23C 14/568 Transferring the substrates through a series of coating stations C23C14/562 takes precedence

Abstract

This invention includes a method featuring steps having a transport (64, 68) to carry metal articles (10, 14) through a vacuum chamber (62, 66, 90) containing a plasma cleaning station (32) followed by exposure to an evaporant of metal (42) generated by an E-Beam (50) caused to condense on the articles in high vacuum. A channel structure (51) is provided to cause selective condensation upon the surface of said articles. The apparatus includes several stations (101, 102, 103) to provide multiple coatings on one or both sides of an article to be coated.

Claims

1. A method of coating metallic articles utilizing an essentially dry process which comprises the steps of:

a. cleaning a selected area of an article by abrasion to remove macro particles, scales and the like,

b. exposing said area to a plasma of above a 1-2 Key energy level in the presence of an argon environment,

c. preheating said area to a temperature above 230 degrees Celsius,

d. producing an evaporant of a metal to be coated upon said area by evaporation through bombardment by an electron beam directed against the said metal in a vacuum on the order of greater than 10^-4 Torr,

e. transporting said article in said area within said evaporant at a distance on the order of between 1 and 7 inches whereby said evaporant condenses on the said area to coat said area,

f. adjusting the rate of transport to effect the thickness of said coating as desired.

2. The method of claim 1 characterized in that the step of producing an evaporant further includes channeling said evaporant to limit exposure to said area or parts of the said area.

3. The method of claim 2 wherein said step of channeling includes the provision of additional step of heating the means of channeling.

4. The method of claim 1 wherein there is further included a series of coating steps incorporating said steps as recited in order providing a first barrier coating followed by a second finish coating of different materials.

5. The method of claim 1 wherein the said step of coating the said material is followed by a second step of coating a different material over said first material by a separate second step of evaporation.

6. The method of claim 1 when said material of said coating is chosen from the materials of gold, nickel, tin, tin lead, copper, zinc, palladium, silver, ruthenium, platinum and alloys thereof.

7. The method of claim 1 wherein the said step of producing an evaporant includes the step of causing said E-Beam to scan the said material whereby to control the characteristics of evaporation.

8. The method of claim 1 characterized in that there is the additional step of controlling the movement of the said article and area to adjust the thickness of coating thereof.

9. The method of claim 1, wherein there is included the further step of supplying said article in the form of a strip and moving said strip through said various method steps.

10. The method of claim 1 wherein there is further included the step of providing a plurality of steps in producing a variety of evaporants from a variety of metals to be coated upon a plurality of areas of said article.