Method and apparatus using molecular sieves for freeze drying

• US 5,035,065 A
• Filed: 12/06/1989
• Issued: 07/30/1991
• Est. Priority Date: 06/03/1988
• Status: Expired due to Fees

• Current Assignee: Martin C. Parkinson
• Original Assignee: Martin C. Parkinson
• Inventors: Parkinson, Martin C.
• Primary Examiner(s): Makay, Albert J.
• Assistant Examiner(s): SOLLECITO, JOHN M
• Application Number:
  US07/446,616
• Time in Patent Office: 601 Days
• Field of Search: 34/5, 34/92, 55/389, 55/73
• US Class Current: 34/92
• CPC Class Codes: F26B 21/083 by using sorbent or hygroscopic materials, e.g. chemical substances, molecular sieves
• CPC Class Codes: F26B 5/06 the process involving freezing

Abstract

An apparatus and method is described for sequestering sublimating water vapor with molecular sieves during freeze drying. Long mesh columns of sieves permit unimpeded sublimating water vapor flow while efficiently adsorbing sublimating water vapor at high flow rates, and also allow efficient sieve desorption during regeneration.

Claims

1. A freeze drying apparatus utilizing molecular sieve to sequester sublimating water vapor, which comprises:

(A) A drying chamber;

(B) A water vapor condenser having means for vapor communication with said drying chamber;

(C) Said condenser contained a quantity of said molecular sieve held within a mesh column;

(D) Said condenser containing a quantity of said molecular sieve held within a solid wall container;

(E) Said solid wall container being connected in series between said mesh column and a source of vacuum;

(F) Said condenser having means for connecting said condenser to said source of vacuum;

(G) Said mesh column of molecular sieve and said solid wall container of said molecular sieve being positioned in said condenser so that when said condenser is connected to said source of vacuum, and said means for vapor communication is providing vapor communication between said condenser and said drying chamber, said sublimating water vapor is subject to impedance to the flow of said sublimating water vapor due to the presence of said solid wall container of said molecular sieve, and, as a result of said impedance, larger amounts of said sublimiting water vapor is absorbed by said sieve in said mesh column.

2. A freeze drying apparatus according to claim 1, further comprising a small quantity of said molecular sieve within said solid wall container, said small quantity of said sieve being small in comparison to the total quantity of said sieve held within said mesh column.