Method for determining physical properties

• US 5,040,734 A
• Filed: 02/28/1990
• Issued: 08/20/1991
• Est. Priority Date: 09/22/1987
• Status: Expired due to Term

• Current Assignee: BP PLC
• Original Assignee: BP PLC
• Inventors: Collins, Patrick, Belchamber, Ronald M.
• Primary Examiner(s): Gorski, Joseph M.
• Application Number:
  US07/492,261
• Time in Patent Office: 538 Days
• Field of Search: 241/30, 241/33, 241/34, 241/36, 267/908
• US Class Current: 241/30
• CPC Class Codes: B02C 25/00 Control arrangements specially adapted for crushing or disintegrating
• CPC Class Codes: G01N 2291/02408 Solids in gases, e.g. particle suspensions
• CPC Class Codes: G01N 29/046 using the echo of particles imparting on a surface; using acoustic emission of particles investigating concentration of particle suspensions G01N15/06; devices for measuring flow of solids in suspension G01F1/74

Abstract

A method for the determination of the value of a property of the material within a mill during the comminution of solid material within the mill comprises the steps of:

(a) detecting the noise intensity of milling by means of an analog electrical signal, the intensity of which is proportional to the intensity of the noise in the audio frequency range,

(b) converting the analog signal to a digital signal,

(c) passing the digital signal through a digital band-pass filter to select at least two frequency bands, and

(d) analyzing the data from the bands by means of a multivariate statistical technique to obtain the value of the property. The method is particularly suitable for determining the particle size distribution of material being ground in a ball mill.

Claims

1. A non-intrusive method for determining a number of inter-related values of physical properties of material within a mill during comminution of the material within the mill wherein the method comprises the steps of:

(a) detecting an acoustic frequency distribution of milling, in the audio frequency range by utilizing a sound transducer, providing output from said transducer as an analogue electrical signal, the intensity of signal is proportional to the intensity of audio frequency range sound,

(b) converting the analogue signal to a digital signal,

(c) passing the digital signal through a digital band-pass filter and selecting at least two frequency bands from the audio frequency range of said digital signal passing through said band-pass filter,

(d) averaging power in each of the bands for a specified period of time, and

(e) analysing the averaged power in the bands by utilizing a multivariate statistical technique, thereby obtaining the values of the physical properties.

2. The method according to claim 1 wherein the sound transducer is a microphone.

3. The method according to claim 1 where the properties are selected from the group consisting of particle size distribution of solid particles, pulp density being milled and pulp volume during milling.

4. The method according the claim 1 including amplifying the analogue electrical signal.

5. The method according to claim 1 including passing the analogue electrical signal through a band-pass filter.

6. The method according to claim 5 including removing frequencies above 10 KHz from the audio frequency range of said digital signal passing through said band-pass filter.

7. The method according to claim 5 including removing frequencies below 50 Hz from the audio frequency range of said digital signal passing through said band-pass filter.

8. The method according to claim 5 wherein the band-pass filter is capable of selecting from 2 to 24 desired frequency bands.

9. The method according to claim 1 wherein the multivariate statistical technique is a method of principal components analysis.

10. The method according to claim 1 wherein the multivariate statistical technique is a method of partial least squares.

11. The method according to claim 1 including performing each step on-line.