Method and apparatus for sampling the gaseous content of a liquid

• US 5,090,256 A
• Filed: 11/27/1989
• Issued: 02/25/1992
• Est. Priority Date: 04/26/1989
• Status: Expired due to Term

• Current Assignee: Geoservices Equipements (SLB)
• Original Assignee: Geoservices (SLB)
• Inventors: Issenmann, Olivier
• Primary Examiner(s): RAEVIS, ROBERT R
• Application Number:
  US07/441,546
• Time in Patent Office: 820 Days
• Field of Search: 73/153, 73/863.23, 73/863.24, 73/864.34, 73/864.81, 73/863.21, 175/40, 175/50, 175/48, 175/66, 175/206, 166/250, 166/264, 166/265
• US Class Current: 73/863.23
• CPC Class Codes: E21B 21/01 Arrangements for handling drilling fluids or cuttings outside the borehole, e.g. mud boxes
• CPC Class Codes: E21B 21/067 Separating gases from drilling fluids
• CPC Class Codes: E21B 49/005 Testing the nature of borehole walls or the formation by using drilling mud or cutting data
• CPC Class Codes: G01N 1/14 Suction devices, e.g. pumps; Ejector devices
• CPC Class Codes: G01N 1/2294 Sampling soil gases or the like
• CPC Class Codes: G01N 1/24 Suction devices G01N1/22 - G01N1/2294 take precedence
• CPC Class Codes: G01N 2001/2267 separating gas from liquid, e.g. bubbles
• CPC Class Codes: G01N 33/2823 Raw oil, drilling fluid or polyphasic mixtures

Abstract

A method and apparatus for sampling the gaseous content of a liquid laden with solids initially involves sampling the liquid as close as possible to the source of the liquid. A strainer housing having a strainer plate for filtering out debris in the liquid is connected to a suction pump for sucking the liquid into the housing and to the pump. The pump delivers the sampled liquid to a degassing device mounted on a frame with the pump. The degassing device agitates the liquid to liberate gases suspended therein. The gases are then collected from the degassing device so that the gases may be analyzed. A motor mechanism on the frame drives the pump, a rotating agitator in the degassing device and a rotating scraper on the exterior of the strainer plate simultaneously. This method and apparatus are particularly applicable to the sampling of drilling mud from an oil well exploration site for purposes of analyzing the hydrocarbon content of the drilling mud.

Claims

1. An apparatus for sampling the gaseous content of a liquid laden with solids, comprising:

a support frame;

a degassing device mounted on said support frame for degassing sample liquid received therein to obtain a sample of gas of the sample liquid, said degassing device comprising a degassing container having an inlet connection for receiving sample liquid therethrough, a rotary degassing agitator, a discharge nozzle for discharging degassed sample liquid, and means for conducting sample gas from said degassing device for delivery to an analyzing device; and

means for collecting sample liquid from a stream of the liquid and delivering substantially all of the sample liquid to said degassing container, said means for collecting and delivering comprising a pump mounted on said support frame having an input connection and an output connection, a flexible suction tube connected to said input connection, and a motor means mounted on said support frame for driving said pump, said output connection being fluidly connected to said inlet connection of said degassing container, and said rotary degassing agitator being driven by said motor means driving said pump.

2. The apparatus as set forth in claim 1, wherein said support frame comprises a support plate and a plurality of support legs connected thereto, said degassing container being connected to the underside of said support plate.

3. The apparatus as set forth in claim 2, wherein:

said degassing container is removably mounted on the underside of said support plate; and

said degassing container has a peripheral collar thereon and an O-ring seal on said collar for sealing contact with said support plate.

4. The apparatus as set forth in claim 2, wherein said motor means comprises a motor mounted on the top side of said support plate.

5. The apparatus as set forth in claim 1, wherein said means for collecting and delivering further comprises:

a suction strainer device connected to a suction end of said flexible suction tube.

6. The apparatus as set forth in claim 5, wherein said suction strainer device comprises:

a hollow strainer housing connected to said flexible suction tube;

a strainer plate on a suction side of said hollow strainer housing; and

means for continuously scraping the exterior side of said strainer plate when said pump is operating to suction sample fluid through said hollow strainer housing and said flexible suction tube.

7. The apparatus as set forth in claim 6, wherein said means for continuously scraping comprises:

a rotating scraper rotatably mounted on the exterior of said strainer plate; and

rotary driving means connected to said rotating scraper and drivably connected to said means for driving said pump.

8. The apparatus as set forth in claim 7, wherein:

said hollow strainer housing is cylindrical on the interior thereof;

said rotary driving means extends through said housing; and

a radial agitator blade is mounted on said rotary driving means in said strainer housing so as to rotate with said rotating scraper and agitate sample liquid in said housing.

9. The apparatus as set forth in claim 7, wherein:

said rotary driving means comprises a shaft extending through said hollow strainer housing and connected to said rotating scraper, and a bowden wire connected between said shaft and said means for driving said pump.

10. The apparatus as set forth in claim 7, wherein a capped nut and a spring are disposed on the exterior of said hollow strainer housing for biasing said rotating scraper against said strainer plate.

11. The apparatus as set forth in claim 6, wherein:

said strainer plate and at least a portion of said means for continuously scraping are made of the same material, said material having a hardness sufficient, according to the Mohs scale, to resist abrasion by any solids in the sample liquid.

12. The apparatus as set forth in claim 11, wherein said material comprises tungsten carbide.

13. The apparatus as set forth in claim 1, wherein:

said means for conducting sample gas from said degassing device comprises a gas evacuation tube disposed on an upper portion of said degassing container for connection to an analyzing device.

14. The apparatus as set forth in claim 13, wherein:

a lateral portion of said degassing container has said discharge nozzle thereon.

15. The apparatus as set forth in claim 14, wherein:

said degassing container has two radial deflectors therein above said rotary degassing agitator, an inner collar defining a circular opening between said motor and said rotary degassing agitator, and a rotary disk above said radial deflectors rotatably mounted with said rotary degassing agitator;

said radial deflectors are disposed below said inner collar; and

said inner collar circular opening has a diameter at most equal to the diameter of said rotary disk.

16. An apparatus for sample the gaseous content of a liquid laden with solids, comprising:

a support frame;

a degassing device mounted on said support frame for degassing sample liquid received therein to obtain a sample of gas of the sample liquid, said degassing device comprising a degassing container having an inlet connection for receiving sample liquid therethrough, a rotary degassing agitator, a discharge nozzle for discharging degassed sample liquid, and means for conducting sample gas from said degassing device for delivery to an analyzing device; and

means for collecting sample liquid from a stream of the liquid and delivering substantially all of the liquid to said degassing container, said means for collecting and delivering comprising a pump mounted on said support frame having an input connection and an output connection, a flexible suction tube connected to said input connection, and a motor means mounted on said support frame for driving said pump, said output connection being fluidly connected to said inlet connection of said degassing container, and said flexible suction tube having a hollow strainer housing connected thereto, said hollow strainer housing having a strainer plate on a suction side thereof and a means for continuously scraping the exterior side of said strainer plate when said pump is operating to suction sample fluid through said hollow strainer housing and said flexible suction tube, said means for continuously scraping being driven by said motor means driving said pump.

17. The apparatus as set forth in claim 16, wherein said means for continuously scraping comprises:

a rotating scraper rotatably mounted on the exterior of said strainer plate; and

rotary driving means connected to said rotating scraper and drivably connected to said motor means driving said pump.

18. The apparatus as set forth in claim 17, wherein:

said hollow strainer housing is cylindrical on the interior thereof;

said rotary driving means extends through said housing; and

a radial agitator blade is mounted on said rotary driving means in said strainer housing so as to rotate with said rotating scraper and agitate sample liquid in said housing.

19. The apparatus as set forth in claim 18, wherein:

said strainer plate and at least a portion of said means for continuously scraping are made of the same material, said material having a hardness sufficient, according to the Mohs scale, to resist abrasion by any solids in the sample liquid.

20. The apparatus as set forth in claim 19, wherein said material comprises tungsten carbide.

21. The apparatus as set forth in claim 20, wherein a capped nut and a spring are disposed on the exterior of said hollow strainer housing for biasing said rotating scraper against said strainer plate.

22. The apparatus as set forth in claim 21, wherein:

said rotary driving means comprises a shaft extending through said hollow strainer housing and connected to said rotating scraper, and a bowden wire connected between said shaft and said means for driving said pump.