Method for coating continuous tow

• US 5,164,229 A
• Filed: 07/08/1991
• Issued: 11/17/1992
• Est. Priority Date: 07/08/1991
• Status: Expired due to Fees

• Current Assignee: United States Of America As Represented By The Secretary Of The Air Force
• Original Assignee: United States Of America As Represented By The Secretary Of The Air Force
• Inventors: Hay, Randall S.
• Primary Examiner(s): Beck, Shrive
• Assistant Examiner(s): Bareford, Katherine A.
• Application Number:
  US07/726,485
• Time in Patent Office: 498 Days
• Field of Search: 427/434.7, 427/434.6, 427/314, 427/372.2, 427/226, 118/405
• US Class Current: 427/226
• CPC Class Codes: B05C 3/12 for treating work of indefinite length
• CPC Class Codes: B05D 7/20 to wires for insulating electric cables H01B13/16
• CPC Class Codes: C04B 14/46 Rock wool ; Ceramic or silicate fibres C04B14/40, C04B14/42 take precedence
• CPC Class Codes: C04B 41/009 characterised by the material treated
• CPC Class Codes: C04B 41/4505 characterised by the method of application
• CPC Class Codes: C04B 41/4535 applied as a solution, emulsion, dispersion or suspension
• CPC Class Codes: C04B 41/455 the coating or impregnating process including a chemical conversion or reaction
• CPC Class Codes: C04B 41/4584 Coating or impregnating of particulate or fibrous ceramic material C04B20/10, C04B35/628 take precedence
• CPC Class Codes: C04B 41/5025 with ceramic materials copper oxide or solid solutions thereof C04B41/5074
• CPC Class Codes: D06B 3/045 in a tube or a groove

Abstract

A method for coating continuous tow which comprises the steps of: (a) transporting a tow through a coating composition to provide a coated tow having a layer of uncured coating thereon, (b) transporting the coated tow through a liquid which is immiscible with the coating composition and (c) curing the coating on the tow to provide a coated tow having a layer of cured coating on the individual filaments thereof, wherein the tow has contact only with the coating composition and the immiscible liquid between the uncoated state of the tow prior to coating step (a) and the cured, coated state of the tow subsequent to curing step (c).

Claims

1. A method for coating fibers in a continuous tow which comprises the steps of:

(a) transporting a tow through an inorganic aqueous coating solution to provide a coated tow having a layer of uncured coating thereon,

(b) transporting the coated tow through a hydrocarbon liquid which is immiscible with the coating solution and

(c) calcining the coating on the tow to provide a coated tow having a layer of cured coating on the individual filaments thereof,

wherein the tow has contact only with the coating solution and the immiscible liquid between the uncoated state of the tow prior to coating step (a) and the cured, coated state of the tow subsequent to calcining step (c).

2. The method of claim 1 wherein said tow comprises a plurality of fibers selected from the group consisting of carbon, graphite, silica, silicon carbide, silicon nitride, silicon carbide-coated boron, boron carbide-coated boron, silicon-coated silicon carbide, alumina, mullite, yttrium-aluminum oxides, beryllium-titanium composites, and boron-aluminosilicate.

3. The method of claim 2 further comprising the step of heat treating said tow at a temperature of about 500°

C. to 1000°

C. prior to said coating step (a).

4. A method for coating fibers in a continuous tow which comprises the steps of:

(a) transporting a tow through an aqueous ceramic-forming solution to provide a coated tow having a layer of uncured coating thereon,

(b) transporting the coated tow through a hydrocarbon liquid which is immiscible with the coating solution and

(c) curing the coating on the tow to provide a coated tow having a layer of cured coating on the individual filaments thereof,

wherein the tow has contact only with the coating solution and the immiscible liquid between the uncoated state of the tow prior to coating step (a) and the cured, coated state of the tow subsequent to curing step (c),

wherein said tow comprises a plurality of fibers selected from the group consisting of carbon, graphite, silica, silicon carbide, silicon nitride, silicon carbide-coated boron, boron carbide-coated boron, silicon-coated silicon carbide, alumina, mullite, yttrium-aluminum oxides, beryllium-titanium composites, and boron-aluminosilicate, and

wherein said ceramic-forming solution is selected from the group consisting of silicates, aluminates, yttriates, titanates, zirconates, and combinations thereof.