Method for reducing thickness of a titanium foil or thin strip element

• US 5,226,989 A
• Filed: 12/16/1991
• Issued: 07/13/1993
• Est. Priority Date: 12/16/1991
• Status: Expired due to Fees

• Current Assignee: Engineered Materials Solutions, Inc. (Wickeder Westfalenstahl GmbH /Private Group/)
• Original Assignee: Texas Instruments, Inc.
• Inventors: Sukonnik, Israil
• Primary Examiner(s): Roy, Upendra
• Application Number:
  US07/809,689
• Time in Patent Office: 575 Days
• Field of Search: 148/669, 148/670, 148/671, 148/650, 148/657
• US Class Current: 148/670
• CPC Class Codes: B21B 1/36 by cold-rolling
• CPC Class Codes: B21B 1/40 for rolling foils which present special problems, e.g. because of thinness
• CPC Class Codes: B21B 13/147 Cluster mills, e.g. Sendzimir mills, Rohn mills, i.e. each work roll being supported by two rolls only arranged symmetrically with respect to the plane passing through the working rolls
• CPC Class Codes: B21B 15/0085 Joining ends of material to continuous strip, bar or sheet
• CPC Class Codes: B21B 2015/0057 Coiling the rolled product
• CPC Class Codes: B21B 3/00 Rolling materials of special alloys so far as the composition of the alloy requires or permits special rolling methods or sequences ; Rolling of aluminium, copper, zinc or other non-ferrous metalsaltering special metallurgical properties of alloys, other than structure consolidation or mechanical properties resulting therefrom C21D, C22F
• CPC Class Codes: B21B 45/004 Heating the product
• CPC Class Codes: B21B 9/00 Measures for carrying out rolling operations under special conditions, e.g. in vacuum or inert atmosphere to prevent oxidation of work; Special measures for removing fumes from rolling mills

Abstract

Leaders are attached to opposite ends of a titanium foil or thin strip element and are partially coiled on respective reels spaced at opposite sides of a cluster rolling mill to transfer the titanium element back and forth between the reels to move the element between pressure rolls of the mill a plurality of times and under forward and back tension in air at room temperature to initially reduce the element thickness enough to permit the element to be coiled on the reels and then to partially coil the element on the reels to further reduce element thickness. Iron aluminide material is interleaved with a loose coil of the element and the element is heated in a protective atmosphere to stress relieve and partially recrystallize the element material between the reductions in thickness.

Claims

1. A method for reducing thickness of a titanium alloy foil or thin strip element having low ductility comprising the steps of providing an element of titanium alloy material having selected length and width and relatively much smaller thickness, advancing the element between a pair or pressure rolls at room temperature while applying a forward tension force to the element and a back tension force to the element, and compressing two opposite surfaces of the element between the rolls to reduce the thickness of the element free of cracking of the element.

2. A method according to claim 1 wherein the element material is selected from the group of titanium intermetallic compounds and high strength titanium alloys consisting of alpha/alpha-2 titanium aluminide intermetallic compounds, alpha-2 titanium aluminide intermetallic compounds, superalpha-2 titanium aluminide intermetallic compounds, near alpha aluminide high strength titanium alloys, alpha/beta aluminide high strength titanium alloys, and beta aluminide high strength titanium alloys, the element is advanced between the pair of pressure rolls at room temperature a plurality of times while applying a forward tension force to the element and a back tension force to the element each time, and compressing the two opposite surfaces of the element between the rolls to reduce the thickness of the element each time.

3. A method according to claim 2 wherein the element is heated to stress relieve and at least partially recrystallize the element material at least one time after the two opposite surfaces of the element are compressed between the rolls to reduce the thickness of the element.

4. A method according to claim 3 wherein the element is heated to stress relieve and at least partially recrystallize the element material a plurality of times after respective compressions of the two opposite surfaces of the element between the rolls to reduce the thickness of the element, and the element is cooled to room temperature before any subsequent compression of the two opposite surfaces of the element between the rolls to reduce the thickness of the element.

5. A method for reducing thickness of a titanium foil alloy or thin strip element having low ductility comprising the steps of providing an element of titanium alloy material having selected length and width and relatively much smaller thickness, advancing the element between cluster roll means at room temperature while applying a forward tension force to the element and a back tension force to the element, and compressing two opposite surfaces of the element between the rolls to reduce the thickness of the element free of cracking of the element.

6. A method for reducing the thickness of a titanium foil or thin strip element comprising the steps of providing an element of titanium material having selected length and width and relatively a much smaller thickness, attaching leaders to respective ends of the length of the element, advancing the element between a pair of pressure rolls of a cluster mill at room temperature a plurality of times in an air atmosphere while applying a forward tension force to the element by pulling on one of the leaders and applying a back tension force to the element by partially restraining advance of the other leader, compressing two opposite surfaces of the element between the rolls to reduce the thickness of the element by at least 15 percent each time, and heating the element to stress relieve and at least partially recrystallize the element material a plurality of times after respective compressions of the two opposite surfaces of the element to reduce the thickness of the element, the element being cooled to room temperature before any subsequent compression of the two opposite surfaces of the element between the rolls to reduce the thickness of the element free of cracking of the element.

7. A method according to claim 6 wherein the element material is selected from the group of titanium intermetallic compounds and high strength titanium alloys consisting of an alpha/alpha-2 titanium aluminide intermetallic compound having a composition by weight percent of 8.5 percent aluminum, 5 percent niobium, 1 percent molybdenum, 1 percent zirconium, 1 percent vanadium and the balance titanium, an alpha-2 titanium aluminide intermetallic compound having a composition by weight percent of 14 percent aluminum, 21 percent niobium and the balance titanium, a superalpha-2 titanium aluminide intermetallic compound having a composition by weight percent of 14 percent aluminum, 20 percent niobium, 3-2 percent molybdenum, 2 percent vanadium, and the balance titanium, an orthorhombic superalpha-2 titanium aluminide intermetallic compound having a composition by weight percent of 11 percent aluminum, 38 percent niobium, 3.8 percent vanadium and the balance titanium, a near alpha aluminide high strength titanium alloy having a composition by weight percent of 6 percent aluminum, 3 percent in, 4 percent zirconium and the balance titanium, an alpha/beta aluminide high strength titanium alloy having a composition by weight percent of 6 percent aluminum, 4 percent vanadium and the balance titanium, and a beta aluminide high strength titanium alloy having a composition by weight of 3 percent aluminum, 3 percent niobium, 15 percent molybdenum and the balance titanium.

8. A method according to claim 6 wherein the element is coiled loosely in interleaved relation with a coil of iron aluminide material during heating thereof to stress relieve and at least partially recrystallize the element material.

9. A method according to claim 6 wherein the leaders each comprise titanium metal lap welded by resistance welding to the element.

10. A method according to claim 7 wherein the leaders are partially coiled on respective reels and the reels are rotated in a first direction to pay out and take-up the respective leaders at relatively different rates for advancing the element in the first direction between the rolls while applying the forward and back tension to the element at least one of the times while the two opposite surfaces of the element are compressed between the rolls to reduce the thickness of the element.

11. A method according to claim 8 wherein the element is coiled loosely in interleaved relation with a coil of iron aluminide material during heating thereof to stress relieve and at least partially recrystallize the element material.

12. A method according to claim 10 wherein the reels are rotated in an opposite direction to pay out and take up the respective leaders at relatively different rates for advancing the element in the opposite direction between the rolls while applying the forward and back tension to the element at least one of the times while the two opposite surfaces of the element are compressed between the rolls to reduce the thickness of the element.

13. A method according to claim 12 wherein the element is provided with a selected initial thickness larger than is coilable on the reels and is reduced at least to a lesser thickness coilable on the reels, and the reels are spaced to permit elongation of the element with reduction of the element to the lesser thickness free of coiling of the element on the reels.

14. A method according to claim 13 wherein the element is at least partially coiled on at least one of the reels in advancing the element in at least one of the directions after reduction of the element to the lesser thickness.

15. A method according to claim 14 wherein a plurality of lengths of titanium foil or thin strips are initially secured together in sequential relation to each other for forming the element.