Sample introduction for spectrometers

• US 5,256,374 A
• Filed: 03/29/1991
• Issued: 10/26/1993
• Est. Priority Date: 04/04/1990
• Status: Expired due to Fees

• Current Assignee: Her Majesty The Queen In Right of Canada As Represented By The Minister of National Defence, Technology Marketing Division Canmet
• Original Assignee: Her Majesty The Queen In Right of Canada As Represented By The Minister of National Defence
• Inventors: Guevremont, Roger, De Silva, K. Nimalasiri
• Primary Examiner(s): Housel, James C.
• Assistant Examiner(s): WALLENHORST, MAUREEN
• Application Number:
  US07/677,095
• Time in Patent Office: 942 Days
• Field of Search: 422/63, 422/67, 422/68.1, 422/80, 422/103, 422/70, 436/52, 436/181, 436/50, 436/155, 436/171, 250/288, 73/864.81
• US Class Current: 422/80
• CPC Class Codes: G01N 21/714 Sample nebulisers for flame burners or plasma burners nebulizers per se B05B
• CPC Class Codes: Y10T 436/115831 Condition or time responsive
• CPC Class Codes: Y10T 436/117497 with a continuously flowing sample or carrier stream
• CPC Class Codes: Y10T 436/25875 Gaseous sample or with change of physical state

Abstract

A system for introducing a sample to an analyzing device, such as a spectrometer, wherein the flow rate of gas to the analyzing device is maintained substantially constant and uncontaminated during sample changeover. The system includes a flow controller and flow control paths arranged to avoid having any flow diverting valves or direction change in the analyte flow path.

Claims

1. A system for introducing a sample to an analyzing device comprising:

a sample chamber having openable access means for receiving a sample, said sample chamber also having an inlet and outlet;

means for atomizing the sample within the sample chamber;

a flow combining portion connected with the outlet of the sample chamber, said flow combining portion further having an inlet for receiving a carrier gas and an outlet for connection to an analyzing device;

sampler gas supply means connected with the inlet of the sample chamber for transporting the sample from the sample chamber through the flow combining portion and to the analyzing device; and

flow control means responsive to the opening of the access means of the sample chamber for increasing the input of the carrier gas to the flow combining portion when the access means of the sample chamber is opened, such that the flow rate of gas to the analyzing device is maintained substantially constant while a portion of the carrier gas flows back through the outlet of the sample chamber to purge ambient air, said flow control means being disposed external to the flow path of the sample extending from the sample chamber to the analyzing device.

2. The system of claim 1 wherein the flow control means comprises a first gas controller providing a continuous substantially constant basal flow rate of carrier gas, and a second gas controller providing an additional gas flow rate of carrier gas corresponding to the flow lost while the access means of the sample chamber is open.

3. The system of claim 2 wherein the flow control means further comprises a gas controller for controlling the flow rate of sampler gas.

4. The system of claim 1 wherein the flow combining portion comprises an outer annular passageway for the carrier gas surrounding an upper portion of the outlet of the sample chamber such that the carrier gas exits the outlet of the flow combining portion in the form of a sheath about the sample and sampler gas.

5. The system of claim 1 wherein the flow combining portion defines an outer annular passageway surrounding an upper portion of the outlet of the sample chamber and wherein the inlet of the flow combining portion is connected generally tangentially to said outer annular passageway to provide spiral flow of the carrier gas within the flow combining portion.

6. The system of claim 1 having flow passageways extending from the sample chamber, through the flow combining portion and to the analyzing device that are disposed in a substantially straight path for providing a substantially straight obstruction free path for a sample passing between the sample chamber and the analyzing device.