Method and apparatus for determining the constituents of dairy products

• US 5,258,620 A
• Filed: 10/30/1991
• Issued: 11/02/1993
• Est. Priority Date: 06/15/1990
• Status: Expired due to Fees

• Current Assignee: Snow Brand Milk Products Co. Ltd. (Megmilk Snow Brand Company Limited)
• Original Assignee: Snow Brand Milk Products Co. Ltd. (Megmilk Snow Brand Company Limited)
• Inventors: Watanabe, Mayumi, Kaya, Hidehiko, Sagara, Kazuhiko, Sueyasu, Ryoichi
• Primary Examiner(s): Hannaher, Constantine
• Assistant Examiner(s): Glick, Edward J.
• Application Number:
  US07/773,921
• Time in Patent Office: 734 Days
• Field of Search: 250/339, 250/340, 250/341, 250/343
• US Class Current: 250/339.12
• CPC Class Codes: G01N 21/3577 for analysing liquids, e.g. polluted water
• CPC Class Codes: G01N 21/359 using near infrared light
• CPC Class Codes: G01N 2201/129 Using chemometrical methods
• CPC Class Codes: G01N 33/04 Dairy products
• CPC Class Codes: Y10S 250/91 Food sample analysis using invisible radiant energy source

Abstract

A sample having a specific optical path length of 1 to 15 mm is irradiated with near infrared of two or more wavelengths selected from 700 to 1200 nm to determine constituents of dairy products. Preferably, a pair of specific wavelengths comprise a first wavelength having a high correlation with a target constituent and a second wavelength having a low correlation with the target constituent or comprise wavelengths both having high correlations with the target constitutent. Quantities of near infrared of these two specific wavelengths transmitted by the sample are measured to determine absorbencies and a multiple linear regression equation is used to calculate the constituent on the basis of the absorbencies.

Claims

1. Method for determining the principal constituents of dairy products comprising, providing a sample having a specific optical path length of from 1 to 15 mm, irradiating the sample with near infrared radiation of two or more specific wavelengths within the range of 700 to 1200 nm, measuring the quantities of the near infrared radiation transmitted by the sample and calculating the quantities of the constituents by using a multiple linear regression equation.

2. Method of claim 1, wherein a pair of specific wavelengths are used and a first wavelength thereof has a high correlation with a constituent and a second wavelength thereof has a low correlation with the constituent or both wavelengths have high correlations with the constituent.

3. Method of claim 2, wherein a fat content of the dairy products is determined and an absorption band for C--H bonds of the fat is used as the first wavelength and an absorption band for O--H and N--H bonds is used as the second wavelength.

4. Method of claim 1, wherein a total solid content of the dairy products is determined and two absorption bands highly correlated with fat and protein, respectively, are used.

5. Method of claim 1, wherein an ash content of the dairy products is determined and a pair of wavelengths both being absorbed by N--H groups are used.

6. Apparatus for determining the principal constituents of a dairy product, comprising:

(A) beam means for producing a beam of near infrared radiation;

(B) filter means disposed within said beam so as to produce a filtered beam having at least two specific radiation wavelength ranges within the overall range of 700 to 1200 nm;

(C) a sample means for containing a sample of the dairy product disposed within said filtered beam, said sample means having an optical path for said filtered beam of from 1 to 15 mm in length;

(D) a conversion means for receiving and converting the filtered beam transmitted through said sample means to electrical signals corresponding to absorbencies of the filtered beam by a sample of the dairy product disposed in the sample means;

(E) amplifier means for amplifying said electrical signals to amplified signals;

(F) digitizing means for converting the amplified signals to digital signals; and

(G) digital processing means for processing the digital signals and calculating the quantities of constituents in the dairy product.

7. The apparatus of claim 6 wherein the specific radiation wavelength ranges are within the ranges of 700 to 800 nm, 820 to 950 nm, 960 to 1060 nm and 1070 to 1200 nm.