Differential dielectric analyzer

• US 5,309,110 A
• Filed: 03/04/1992
• Issued: 05/03/1994
• Est. Priority Date: 03/04/1992
• Status: Expired due to Term

• Current Assignee: Perkin-Elmer Llc (Revvity, Inc.)
• Original Assignee: The Perkin-Elmer Corporation (Thermo Fisher Scientific Incorporated)
• Inventors: McKinley, Kerry, O'Neill, Michael J.
• Primary Examiner(s): Wieder, Kenneth A.
• Assistant Examiner(s): BROWN, GLENN WARNER
• Application Number:
  US07/845,994
• Time in Patent Office: 790 Days
• Field of Search: 324/649, 324/650, 324/651, 324/662, 324/663, 324/671, 324/674, 324/681, 324/683, 324/685, 324/686, 324/690
• US Class Current: 324/674
• CPC Class Codes: G01R 27/2641 of plate type, i.e. with the sample sandwiched in the middle

Abstract

An apparatus for analyzing the dielectric properties of a sample. A thin planar sample having a hole therein is positioned over two bottom electrodes having the hole over one of the bottom electrodes. An oscillator provides a first signal to one of the bottom electrodes and a second signal 180° out of phase with the first signal to the second bottom electrode. A differential signal is obtained on the top electrode representative of the dielectric properties of the sample with the elimination of edge effects. A phase sensitive demodulator synchronized with the oscillator extracts the two components of the conductance and susceptance of the sample. A position sensor measures the thickness of the sample and is used to calculate the dielectric constant of the sample. Thereby, an accurate measurement of the dielectric properties of the sample is obtained without a complicated structure in order to eliminate edge effects.

Claims

1. An apparatus for analyzing the dielectric properties of a sample comprising:

a substrate;

a first bottom electrode mounted on said substrate;

a second bottom electrode mounted on said substrate;

a top electrode;

oscillator means, coupled to said first and second bottom electrodes, for driving said first and second bottom electrodes, said second electrode being driven out of phase relative to said first electrode;

demodulator means, coupled to said top electrode, for extracting a signal representative of the conductance of the sample and a signal representative of the susceptance of the sample;

calculator means, coupled to said oscillator means and said demodulator means, for calculating desired dielectric properties of the sample; and

display means, coupled to said calculator means, for displaying desired dielectric properties of the sample.

2. An apparatus for analyzing the dielectric properties of a sample as in claim 1 wherein:

said second electrode is driven 180°

out of phase relative to said first electrode.

3. An apparatus for analyzing the dielectric properties of a sample as in claim 2 wherein:

said first and second bottom electrodes have equal surface areas.

4. An apparatus for analyzing the dielectric properties of a sample as in claim 1 wherein:

the surface area of said top electrode is at least as large as the combined surface areas of said first and second bottom electrodes.

5. An apparatus for analyzing the dielectric properties of a sample as in claim 1 wherein:

said oscillator means is variable.

6. An apparatus for analyzing the dielectric properties of a sample as in claim 5 wherein:

said oscillator means has a variable frequency range between 0.001 Hz and 100 kHz.

7. An apparatus for analyzing the dielectric properties of a sample as in claim 6 wherein:

said calculator means further comprises means for calculating the dielectric properties of the sample as a function of frequency.

8. An apparatus for analyzing the dielectric properties of a sample as in claim 1 further comprising:

position sensor means, associated with either said top electrode or said substrate, for determining the thickness of the sample placed therebetween.

9. An apparatus for analyzing the dielectric properties of a sample as in claim 8 wherein:

said calculator means further comprises means for calculating the dielectric constant of the sample.

10. An apparatus for analyzing the dielectric properties of a sample comprising:

a substrate;

a first bottom electrode mounted on said substrate;

a second bottom electrode mounted on said substrate;

a top electrode;

oscillator means, coupled to said first and second bottom electrodes, for driving said first and second bottom electrodes, said second electrode being driven out of phase relative to said first electrode;

demodulator means, coupled to said top electrode, for extracting a signal representative of the conductance of the sample and a signal representative of the susceptance of the sample;

calculator means, coupled to said oscillator means and said demodulator means, for calculating desired dielectric properties of the sample;

display means, coupled to said calculator means, for displaying desired dielectric properties of the sample; and

heater means, coupled to said substrate, for heating the sample over a range of temperatures.

11. An apparatus for analyzing dielectric properties comprising:

a substrate;

a first bottom electrode mounted on said substrate;

a second bottom electrode mounted on said substrate adjacent said first bottom electrode, said second bottom electrode having a top surface area equal to a top surface area of said first bottom electrode;

a top electrode positioned above said first and second bottom electrodes having a bottom surface area at least as large as the combined top surface areas of said first and second bottom electrode;

a planar sample to be analyzed, said sample having a hole therein, said sample positioned between said top electrode and said first and second bottom electrodes such that the hole is positioned completely over one of said first or second bottom electrodes;

oscillator means, coupled to said first and second bottom electrodes, for applying a first signal to said first bottom electrode, and a second signal 180°

out of phase with said first signal to said second bottom electrode; and

phase sensitive demodulator means, coupled to said top electrode and said oscillator means, for obtaining a first component in phase with said first signal representative of the conductance of said sample and a second component 90°

out of phase with said first signal representative of the susceptance of the sample.

12. An apparatus for analyzing dielectric properties as in claim 11 further comprising:

position sensor means, coupled either to said top electrode or said substrate for determining the thickness of said sample; and

calculator means, coupled to said position sensor means and said phase sensitive demodulator means, for calculating the dielectric constant of said sample.

13. An apparatus for analyzing dielectric properties as in claim 12 further comprising:

a heater element attached to said substrate; and

heater control means, coupled to said heater element and said calculator means, for controlling the temperature of said sample.

14. An apparatus for analyzing dielectric properties as in claim 13 further comprising:

display means, coupled to said calculator means, for displaying selected dielectric properties of said sample.