Production of compacted granules for detergents

• US 5,318,733 A
• Filed: 04/09/1992
• Issued: 06/07/1994
• Est. Priority Date: 08/09/1989
• Status: Expired due to Fees

• Current Assignee: Henkel KGaA (Henkel AG & Co KGaA)
• Original Assignee: Henkel KGaA (Henkel AG & Co KGaA)
• Inventors: Vogt, Guenther, Raehse, Wilfried, Carduck, Franz-Josef, Jacobs, Jochen, Pawelczyk, Hubert, Smulders, Eduard
• Primary Examiner(s): Kuhns, Allan R.
• Application Number:
  US07/834,251
• Time in Patent Office: 789 Days
• Field of Search: 264/15, 264/118, 264/141, 264/142, 264/143, 264/122, 252/89.1, 252/174, 252/99
• US Class Current: 264/15
• CPC Class Codes: C11D 11/0082 one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
• CPC Class Codes: C11D 17/0047 Detergents in the form of bars or tablets
• CPC Class Codes: C11D 17/0073 Tablets
• CPC Class Codes: C11D 17/065 High-density particulate detergent compositions

Abstract

A process for the production of compacted granules for use in a detergent composition by providing a homogeneous, solid, free-flowing premix to which a plasticizer or lubricant is added, and extruding the mixture through a perforated die under a pressure of from about 25 bar to about 200 bar to form strands of the mixture. The perforated die has an opening width corresponding to a predetermined size of the granules. After emerging from the perforated die, the strands are cut to the predetermined size of the granules by means of a cutting unit. The process enables the preparation of detergent compositions containing increased contents of surfactant components.

Claims

1. A process for the production of compacted granules for use in a detergent composition, comprising providing a homogeneous, solid, granular free-flowing premix containing a plasticizer or lubricant, extruding said premix through a perforated die under a pressure of from about 25 bar to about 200 bar to form plasticized strands of said premix wherein said perforated die has an opening width corresponding to a predetermined size of said granules, and after emerging from said perforated die, cutting said strands to the predetermined size of said granules by means of a cutting unit.

2. A process as in claim 1 wherein said pressure is between about 30 bar and about 200 bar, and said granules have a diameter of from about 0.5 mm to about 5 mm.

3. A process as in claim 1 wherein said plasticizer or lubricant is selected from the group consisting of an anionic surfactant, a nonionic surfactant, a water-soluble, water-emulsifiable or water-dispersible polymer compound, and mixtures thereof.

4. A process as in claim 3 wherein said plasticizer or lubricant is present as an aqueous surfactant paste and is added in a quantity of from about 0.5 to about 10% by weight, based on the weight of said premix.

5. A process as in claim 1 wherein said premix contains up to about 10% by weight of free water, based on the weight of said premix.

6. A process as in claim 1 including homogenizing said premix with a homogenizing unit selected from a granulator, a pelletizing press, a single-screw or twin-screw extruder, and a planetary roll extruder.

7. A process as in claim 6 wherein under the shearing effect of said extruder, compacting said premix at a pressure of from about 50 bar to about 180 bar, plasticizing said premix, extruding said premix to form said strands, size-reducing said strands by means of a rotating chopping blade to spherical or cylindrical granules having a length-to-diameter ration of from about 1:

1 to about 3;

1, and while said granules are still moist and plastic, rounding said granules using a rounding unit while adding thereto a drying powder.

8. A process as in claim 1 wherein said premix contains at least one moisture-binding constituent in anhydrous form, and said granules are at least partly internally dried by binding of the liquid components that are present in said premix, whereby external drying of said granules is shortened or eliminated.

9. A process as in claim 7 including contacting said granules with a temperature-sensitive constituent in the form of separate granules to provide a multiple-granule mixture.