Method and apparatus for using stochastic excitation and a superconducting quantum interference device (SAUID) to perform wideband frequency response measurements

• US 5,343,147 A
• Filed: 09/08/1992
• Issued: 08/30/1994
• Est. Priority Date: 09/08/1992
• Status: Expired due to Fees

• Current Assignee: Quantum Magnetics, Inc. (GE Aerospace)
• Original Assignee: Quantum Magnetics, Inc. (GE Aerospace)
• Inventors: Sager, Ronald E., Simmonds, Michael B.
• Primary Examiner(s): Strecker, Gerard R.
• Assistant Examiner(s): EDMONDS, WARREN
• Application Number:
  US07/941,527
• Time in Patent Office: 721 Days
• Field of Search: 324/201, 324/202, 324/205, 324/239, 324/243, 324/248, 324/260, 324/261, 324/262, 324/301, 324/302, 324/71.6, 324/318, 307/306, 505/841-846, 505/702, 505/705, 338/325, 338/224, 338/259
• US Class Current: 324/239
• CPC Class Codes: G01R 33/0358 coupling the flux to the SQUID gradiometer coils G01R33/022; coils with superconductive winding H01F6/06
• CPC Class Codes: G01R 33/326 involving a SQUID
• CPC Class Codes: G01R 33/4616 using specific RF pulses or specific modulation schemes, e.g. stochastic excitation, adiabatic RF pulses, composite pulses, binomial pulses, Shinnar-le-Roux pulses, spectrally selective pulses not being used for spatial selection
• CPC Class Codes: Y10S 505/846 using superconductive quantum interference device, i.e. squid

Abstract

A stochastic excitation, SQUID detection system for determining the frequency response of a sample. A pair of counterwound detection coils are adjacent to an excitation coil. The sample is selectively placed in one of the detection coils for taking measurements. The SQUID sensor is a broadband, high sensitivity device which enables the frequency response of the sample to be determined over a wide bandwidth with a single measurement.

Claims

1. A method for obtaining wideband frequency response measurements from a sample, the method comprising the steps of:

applying to the sample a stochastic magnetic excitation field whereby the frequency components of the excitation field which coincide with the resonant frequencies of the nuclear magnetic moments in the staple generate an oscillating magnetic field in and around the sample;

sensing the oscillating magnetic field around the sample by means of the current induced in a detection coil closely adjacent to the sample;

coupling the sensed oscillating current to a SQUID by means of a superconducting input coil in a SQUID sensor; and

providing the SQUID output signals, which include the characteristic frequency responses from the sample in a superconductive modulation coil, to measurement and analysis apparatus to thereby obtain the frequency response measurements.

2. The method recited in claim 1, wherein the detection coil comprise a pair of counterwound coils connected across the superconducting input coil.

3. The method recited in claim 1, and comprising the further step of converting the signals from the SQUID to an indication signal for analysis.

4. The method recited in claim 1, and comprising the further step of applying a DC magnetic field to the sample while the frequency response measurements are being performed.

5. The method recited in claim 4, wherein the strength of the DC magnetic field applied to the sample is selectively controllable whereby the frequency response of the sample is measured as a function of the magnetic field.

6. The method recited in claim 5, wherein the DC magnetic field is parallel to the excitation field applied to the sample.

7. The method recited in claim 5, wherein the DC magnetic field is perpendicular to the excitation field applied to the sample.

8. The method recited in claim 1, and comprising the further step of subjecting the sample to varying temperatures while the measurements are being performed, whereby the frequency response of the sample is measured as a function of temperature.

9. Apparatus for obtaining frequency response measurements from a sample, said apparatus comprising:

a stochastic signal source;

an excitation coil connected to said stochastic signal source, the sample being positioned with respect to said excitation coil so that the magnetic field of said excitation coil is applied to the sample, thereby causing the sample to generate an oscillating magnetic field;

detection coil means adjacent to the sample such that the oscillating magnetic field from the sample inductively couples to said detection coil, thereby causing currents to flow in said detection coil;

a superconducting input coil connected to said detection coil means such that the currents flowing in said detection coil also flow in said input coil; and

a SQUID sensor, said input coil being coupled to said SQUID sensor such that the currents flowing in said input coil cause said SQUID sensor to generate an output voltage where the frequency response of the sample is contained in the oscillating output voltage.

10. The apparatus recited in claim 9, wherein said detection coil means comprises a pair of series connected coils which are counterwound with respect to each other and balanced with respect to said excitation coil so that when no sample is present, a signal from the excitation coil produces substantially no signal in the SQUID detector.

11. The apparatus recited in claim 9, and further comprising means for applying a DC magnetic field to the sample to enable the frequency response of the sample to be measured as a function of the magnetic field.

12. The apparatus recited in claim 11, wherein said DC magnetic field is parallel to the excitation field.

13. The apparatus recited in claim 11, wherein the DC magnetic field is perpendicular to the excitation field.

14. The apparatus recited in claim 9, and further comprising means for applying a selectively variable temperature to the sample to enable the frequency response of the sample to be measured as a function of temperature.

15. The apparatus recited in claim 9, and further comprising means for converting the SQUID output signals to indication signals for analysis.