Apparatus for testing membrane filter integrity

• US 5,353,630 A
• Filed: 04/30/1993
• Issued: 10/11/1994
• Est. Priority Date: 05/01/1992
• Status: Expired due to Fees

• Current Assignee: Filtec, USF Filtration and Separations Group, Inc. (Siemens AG)
• Original Assignee: Filtec, Memtec Japan Limited
• Inventors: Soda, Fusao, Sawa, Hidenobu
• Primary Examiner(s): Williams, Hezron E.
• Assistant Examiner(s): ROSKOS, JOSEPH
• Application Number:
  US08/056,252
• Time in Patent Office: 529 Days
• Field of Search: 73/38
• US Class Current: 73/38
• CPC Class Codes: B01D 65/102 Detection of leaks in membranes
• CPC Class Codes: G01N 15/0826 and measuring fluid flow rate, i.e. permeation rate or pressure change
• CPC Class Codes: G01N 2015/086 of films, membranes or pellicules

Abstract

A membrane filter integrity test system includes a large volume mass-flow controller for rapidly supplying a larger amount of fluid to a primary side of a membrane filter under test, a small volume mass-flow controller for supplying a relatively small amount of fluid to the primary side of the membrane filter. The operation of the large volume mass-flow controller is stopped when the pressure at the primary side of said membrane filter reaches a predetermined level. This predetermined pressure is detected by a pressure sensor which senses the pressure at the primary side of the membrane filter. The pressure sensor responsively generates a detection signal corresponding to the sensed pressure at the primary side of the membrane filter. A main controller responsive to the detection signal from the pressure sensor controls the small volume mass-flow controller in a negative feedback loop manner for controlling the supply of fluid to the primary side of the membrane filter so that the pressure on the primary side of the filter is maintained at the predetermined value.

Claims

1. An apparatus for testing the perfection of a membrane filter, said apparatus comprising:

a large-flow controller for supplying a primary side of said membrane filter rapidly with a larger amount of a fluid;

a pressure detecting sensor for detecting the pressure at said primary side of said membrane filter and for responsively generating a detection signal;

a small-flow controller for supplying the primary side of said membrane filter with a smaller amount of said fluid;

a switching member for forming a fluid path for said fluid from said large-flow controller and said small-flow controller to said membrane filter, said switching member disconnecting said fluid path and forming an exhaust path for withdrawing said fluid in said primary side of said membrane filter

a main control unit responsive to the detection signal from said pressure detecting sensor to stop the operation of said large-flow controller when the pressure at the primary side of said membrane filter reaches a predetermined level, the main control unit then controlling said small-flow controller in a proportional/integral control manner to compensate the pressure decrease caused by said membrane filter to maintain said predetermined level, said main controller monitoring the amount of fluid flowing from said small-flow controller to said membrane filter to determine diffusion flow in said membrane filter.

2. The apparatus of claim 1, wherein said fluid is a gas and each of said large-flow controller and said small-flow controller comprises:

a housing having an inlet and an outlet;

a manifold within said housing through which a main stream of fluid flows;

a capillary through which a secondary stream of fluid flows from an upstream side of said manifold to a downstream side of said manifold; and

two thermal resistance wires mounted at two spaced positions along said capillary,

wherein a temperature difference in the secondary flow at the two positions where the thermal resistance wires are located is sensed by a resistance change in the thermal resistance wires in order to determine the gas flow through the large-flow controller and the small-flow controller.

3. The apparatus of claim 2 further comprising a register which stores flow data from the main control unit, wherein the main control unit changes the flow data in the register depending on the gas pressure on the primary side of the membrane filter detected by the pressure detecting sensor.

4. The apparatus of claim 3, wherein each of said large-flow controller and said small-flow controller further including:

a bridge circuit connected to the ends of the thermal resistance wires which detects the difference of the resistance value in the thermal resistance wires and generates a corresponding electric output signal;

an amplifier which amplifies the output signal from the bridge circuit to output an amplified signal;

a comparator circuit which receives the amplified signal from the amplifier and also a reference signal from the register;

a valve which opens or closes a gap provided in proximity to said outlet; and

a solenoid for actuating said valve,

wherein the comparator circuit compares the amplified signal with the reference signal and generates an electric current to the solenoid which actuates the valve to compensate for the difference between the two input signals of the comparator circuit.

5. A method for testing the integrity of a membrane filter, said method comprising the steps of:

supplying a fluid to a membrane filter test system through an inlet valve;

allowing said fluid to contact a primary side of said filter until completely wetted;

closing said valve to shut off said supply of fluid;

draining said fluid from the system;

supplying a gas to said membrane filter test system through a second inlet valve on the primary side of the filter;

monitoring a pressure on the primary side of said filter with a sensor which generates a pressure signal;

transmitting the pressure signal to a main controller;

commencing a first gas flow to the primary side of the membrane filter through a large-flow controller;

stopping said first gas flow by actuating a valve within said large-flow controller based on instructions from the main controller when a predetermined pressure on the primary side of said membrane is reached;

delivering a second gas flow to the primary side of the membrane filter through a small-flow controller;

maintaining a predetermined pressure in the primary side of the membrane filter during the test by metering flow through said small-flow controller based on a feedback loop comprised of said sensor, said main controller and said small-flow controller.

6. The method of claim 5, wherein a bubble point test is conducted, the bubble point test comprising the steps of:

diverting an outlet flow line from a secondary side of said filter to a reservoir of liquid;

transmitting said pressure signal to an output recorder for creating a record of the time-varying pressure signal;

increasing the pressure on the primary side of said membrane filter by actuating said small-flow controller past a point at which bubbles are apparent in the reservoir;

comparing said pressure-signal record with the time when bubbles were apparent to determine the bubble point of said filter.