Process for making shearform matrix

• US 5,380,473 A
• Filed: 10/23/1992
• Issued: 01/10/1995
• Est. Priority Date: 10/23/1992
• Status: Expired due to Fees

• Current Assignee: Fuisz Technologies Limited (Bausch Health Cos., Inc.)
• Original Assignee: Fuisz Technologies Limited (Bausch Health Cos., Inc.)
• Inventors: Hiscocks, Peter G., Fuisz, Richard C., Bogue, B. Arlie
• Primary Examiner(s): Theisen, Mary Lynn
• Application Number:
  US07/965,804
• Time in Patent Office: 809 Days
• Field of Search: 264/11, 264/12, 264/13, 425/6, 425/7
• US Class Current: 264/11
• CPC Class Codes: A23G 3/10 Candy-pulling machines ; Processes or apparatus for making cotton candy or candy floss
• CPC Class Codes: A23G 3/54 Composite products, e.g. layered, coated, filled
• CPC Class Codes: A61K 9/70 Web, sheet or filament bases ; Films; Fibres of the matrix type containing drug hollow drug-filled fibres A61K9/0092
• CPC Class Codes: B29C 48/00 Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor extrusion blow-moulding B29C49/04

Abstract

The present invention is a unique process and apparatus for making a new matrix material called a shearform matrix which results in transformation of the morphology of a feedstock. The process is characterized by increasing the temperature of a nonsolubilized feedstock carrier to a point where it will undergo internal flow, followed by ejecting a stream of the feedstock and then subjecting it to disruptive fluid shear force which separates it into separate parts or masses which have a transformed morphology. The shearform matrix may include other ingredients such as oleaginous material and actives.

Claims

1. A process for making a shearform matrix comprising:

a) controlledly increasing the temperature of a feedstock which includes a solid non-solubilized carrier material capable of undergoing internal flow in the absence of dissolution to a point where said carrier material will undergo internal flow with the application of disruptive fluid shear force;

b) ejecting said heated feedstock resulting from step (a) as a coherent stream under pressure from at least one orifice; and

c) then subjecting said coherent stream of feedstock to a disruptive fluid shear force which separates said coherent stream of feedstock into multiple discrete and discontinuous parts and transforms the morphology of said feedstock into said shearform matrix.

2. A process according to claim 1 wherein said multiple parts are cooled to a temperature below said internal flow point immediately after contact with said fluid shear forces and separation of said stream into multiple parts.

3. The process of claim 1 wherein an environment is provided for said multiple parts to reform as solid shearform matrix under conditions which permit free-flow until solidification.

4. The process of claim 1 wherein said carrier material selected from the group consisting of saccharide-based materials, thermoplastic polymers, biodegradable polymers, and cellulosics.

5. The process of claim 4 wherein said feedstock further comprises a crystallization control agent.

6. The process of claim 5 wherein said crystallization control agent is an antihumectant.

7. The process of claim 5 wherein said feedstock comprises an oleaginous material selected from the group consisting of vegetable oils, soy bean oil, canola oil, corn oil, sunflower oil, animal fats, tallows, lards, fish oils, crustacean oils, and mixtures thereof.

8. The process of claim 4 wherein said feedstock further comprises an additive selected from the group consisting of bio-affecting agents, dyes, fragrances, crystallization control agents, sweeteners, flavors, and mixtures thereof.

9. The process of claim 1 wherein said temperature is controlledly increased to said internal flow point in the substantial absence of heating beyond said point and with minimum residence time during said controlled temperature increase.

10. The process of claim 9 wherein said feedstock is simultaneously pressurized.

11. The process of claim 9 wherein said controlled temperature increase is provided by passing said feedstock through a feeder chamber having multiple temperature-control zones.

12. The process of claim 11 wherein said feedstock is passed through said multiple zones under conditions which prevent heating substantially beyond said internal point and which minimizes time in said chamber.

13. The process of claim 4 wherein said fluid shear force results from directing a fluid at high velocity at said stream of extrudate.

14. The process of claim 13 wherein said feedstock is sucrose and said fluid is air maintained at a temperature of from about 160°

C. to about 200°

C. and ambient atmosphere has a relative humidity of less than 30% RH.

15. The process of claim 13 wherein said feedstock is maltodextrin and said fluid is air maintained at a temperature of from about 85°

C. to about 180°

C. and ambient atmosphere.

16. The process of claim 4 wherein said fluid shear force results from extruding said feedstock through said nozzle at high velocity against a fluid atmosphere at a condition which provides discrete, discontinuous masses.

17. An apparatus for making a shearform matrix comprising:

means for advancing, and controlledly increasing the temperature of a feedstock which includes a solid non-solubilized carrier material and applied pressure on said solid non-solubilized carrier material to the point where said carrier undergoes internal flow and is simultaneously advanced for ejection;

means for ejecting said feedstock as a coherent stream for shearing said feedstock to provide said shearform matrix, said means for ejecting in a fluid communication with said means for increasing the temperature and pressure and arranged to receive said feedstock material during said internal flow condition; and

means for disruptively shearing said feedstock fixed proximally to said means for ejection and disposed for effecting shear of said coherent stream of feedstock during said internal flow condition into multiple discrete and discontinuous masses whereby said feedstock material is transformed to said shearform matrix.

18. The apparatus of claim 17 wherein said means for increasing the temperature comprises a multiple-zone chamber having selectively heatable zones and a continuous throughput mechanism for advancing said feedstock.

19. The apparatus of claim 18 wherein said throughput mechanism comprises at least one screw mechanism for extruding said feedstock.

20. The apparatus of claim 19 wherein said means is a twin screw extruder having at least four heating zones.

21. The apparatus of claim 20 wherein there are nine heating zones.

22. The apparatus of claim 17 wherein said means for ejecting is a high pressure nozzle.

23. The apparatus of claim 22 wherein said nozzle is a low velocity nozzle which provides a substantially coherent stream of said feedstock at an exit orifice.

24. The apparatus of claim 22 wherein said nozzle is a high velocity nozzle having at least one opening for ejecting feedstock at high velocity.

25. The apparatus of claim 17 wherein said means for shearing said feedstock comprises means for delivering fluid for high velocity against feedstock as it exits said means for ejecting.

26. The apparatus of claim 25 wherein said means for delivering fluid comprises an external atomizing nozzle.

27. The apparatus of claim 24 wherein said means for shearing comprises an environment-maintenance chamber which maintains an environment which induces shear upon collision of said high velocity feedstock against said environment.

28. The apparatus of claim 17 wherein said apparatus comprises means for injecting an additive to said feedstock at a point proximal said means for ejecting said feedstock.