Apparatus and method for continuously mixing fluids

• US 5,382,411 A
• Filed: 01/05/1993
• Issued: 01/17/1995
• Est. Priority Date: 01/05/1993
• Status: Expired due to Term

• Current Assignee: Halliburton Company
• Original Assignee: Halliburton Company
• Inventors: Allen, Thomas E.
• Primary Examiner(s): Warden, Robert J.
• Assistant Examiner(s): Kim, Christopher Y.
• Application Number:
  US08/001,232
• Time in Patent Office: 742 Days
• Field of Search: 422/131, 422/135, 366/2, 366/137, 366/159, 366/165, 366/6, 366/14, 366/15, 366/17, 366/65, 366/66, 366/136, 366/150, 366/181, 366/182, 137/605, 137/625.3, 137/897
• US Class Current: 422/131
• CPC Class Codes: B01F 2101/2805 Mixing plastics, polymer material ingredients, monomers or oligomers
• CPC Class Codes: B01F 23/59 Mixing systems, i.e. flow charts or diagrams
• CPC Class Codes: B01F 25/721 for spraying a fluid on falling particles or on a liquid curtain
• CPC Class Codes: B01F 33/84 Mixing plants with mixing receptacles receiving material dispensed from several component receptacles, e.g. paint tins

Abstract

Apparatus and method of hydrating a particulated polymer and producing a well treatment gel includes a mixer for spraying the polymer with water at a substantially constant water velocity and at a substantially constant water spray pattern at all flow rates of the water. A centrifugal diffuser is connected to the mixer for receiving the mixture, centrifugally diffusing the motive energy of the mixture, and hydrating the mixture into a gel. A centrifugal separator and constant velocity jet pump may be connected between the mixer and the centrifugal diffuser. A dilution valve is connected to the discharge of the centrifugal diffuser for mixing water with the gel at a substantially constant mixing energy at all flow rates of the gel and producing a diluted gel. A viscometer may be connected to the discharge of the dilution valve for measuring the viscosity of the diluted gel and regulating the flow of gel from the centrifugal diffuser to the dilution valve in order to control the viscosity of the diluted gel.

Claims

1. Apparatus for hydrating a particulated polymer and producing a gel, such as a well treatment gel, comprising:

water spraying induction mixing means for spraying the polymer with a water spray and forming a water-polymer mixture having a motive energy; and

a centrifugal diffuser means, connected to the water spraying induction mixing means, for receiving the mixture from the mixing means and passively converting the motion of the mixture into circular motion, thereby centrifugally separating and discharging air from the mixture, centrifugally dissipating the motive energy of the mixture, and hydrating the mixture into a gel.

2. Apparatus of claim 1 wherein:

the water spraying induction mixer sprays the polymer with water at a substantially constant water velocity and at a substantially constant water spray pattern at all flow rates of the water.

3. Apparatus of claim 2 in which the water spraying induction mixing means comprises:

a polymer inlet;

a water inlet surrounding the polymer inlet;

a mixing chamber in fluid communication with the polymer and water inlets;

an outlet for discharging the water-polymer mixture from the mixing chamber;

an orifice plate, located between the water inlet and the mixing chamber, surrounding the polymer inlet, and having a plurality of orifices; and

valve means for opening and closing all of the orifices of the orifice plate simultaneously.

4. Apparatus of claim 3 in which the water spraying induction mixing means comprises:

a spray guide surrounding the polymer inlet and extending between the orifice plate and the mixing chamber and having a plurality of orifices coincident with the orifices of the orifice plate; and

wherein the polymer inlet, water inlet, mixing chamber, outlet, orifice plate, valve plate, and spray guide have a coextensive flow axis along which the polymer flows; and

wherein each orifice of the spray guide has a linear longitudinal axis extending through the spray guide and directed obliquely towards the flow axis and outlet and tangentially to a radial arc about the flow axis, the orifices being thereby directed to create a converging and crisscrossing spray pattern having several focal points along the flow axis.

5. Apparatus of claim 4:

wherein the orifices of the spray guide are directed tangentially at various radial distances from the flow axis and obliquely towards the flow axis at various angles.

6. Apparatus of claim 5:

wherein the orifices of the spray guide are located in opposed pairs, the orifices of each pair being located on opposing sides of the mixing chamber, directed along parallel tangents having the same radial distance from the flow axis, and directed at the same oblique angle toward the flow axis.

7. Apparatus of claim 1, comprising:

separating means, connected to the mixing means, for receiving the water-polymer mixture and separating air therefrom; and

a pump, connected to the separating means, for imparting motive energy to the mixture and moving the mixture from the separating means to the centrifugal diffuser means.

8. Apparatus of claim 7 in which the separating means comprises:

a centrifugal separator means, connected to an outlet of the mixing means, for receiving the mixture from the mixing means and passively converting the motion of the mixture into circular motion, thereby centrifugally separating air from the mixture, and providing a flow path for the discharge of the mixing means which does not significantly restrict air flow through the mixing means.

9. Apparatus of claim 8 in which the centrifugal separator means includes:

a separator chamber having an upper end, a lower end, and an outside wall having an about cylindrical inside surface;

a tangential inlet at the upper end of the chamber for receiving and directing the mixture from the mixing means into a circumferential flow path around the inside surface of the outside wall of the separator chamber; and

a tangential lower outlet at the lower end of the chamber for receiving and discharging the circumferentially flowing mixture from the chamber.

10. Apparatus of claim 9:

wherein the upper inlet of the separator chamber is skewed toward the lower end of the chamber in order to direct the circumferential flow of the mixture in a downward spiral toward the lower end of the chamber.

11. Apparatus of claim 1:

wherein the mixing means is further defined as creating a suction at the polymer inlet whereby polymer is pulled into the mixing means.

12. Apparatus of claim 11, comprising:

a polymer supply located at a lower elevation than the polymer inlet of the mixing means; and

a conduit connected between the polymer supply and the polymer inlet.

13. Apparatus of claim 12 in which the polymer supply comprises:

a metering feeder for metering a predetermined quantity of polymer to the conduit.

14. Apparatus of claim 7 in which the pump comprises:

injection means for injecting water into the mixture at a substantially constant velocity at all flow rates of the mixture.

15. Apparatus of claim 14 in which the injection means comprises:

a water injection conduit, located between the separating means and the diffuser means, having an orifice for injecting water into the mixture;

a valve, movably positioned in the orifice, for varying the size of the orifice; and

actuator means, connected to the valve, for moving the valve and controlling the size of the orifice in response to changes in the flow rate of the mixture from the separating means.

16. Apparatus of claim 1 in which the centrifugal diffuser means comprises:

an inner chamber having an upper end;

a lower end;

an outside wall having an about cylindrical inside surface;

a tangential upper inlet at the upper end of the inner chamber for receiving and directing the mixture discharged from the mixing means into a circumferential flow path around the inside surface of the inner chamber; and

a lower outlet at the lower end of the chamber for discharging the mixture from the inner chamber; and

an outer chamber surrounding the inner chamber, the outer chamber having an upper end;

a lower end;

an outside wall having an about cylindrical inside surface; and

an outlet at the upper end of the outer chamber;

the lower end of the outer chamber receiving the mixture discharged from the inner chamber so that the mixture flows upward from the lower end to the outlet of the outer chamber.

17. Apparatus of claim 16 in which the outlet of the inner chamber comprises:

a guide vane extending from the outlet into the inner chamber for guiding the circumferentially flowing mixture out of the inner chamber so that the mixture flows circumferentially around the inside surface of the outer chamber'"'"'s outside wall.

18. Apparatus of claim 16:

wherein the upper inlet of the inner chamber is skewed toward the lower end of the inner chamber in order to direct the circumferential flow of the mixture in a downward spiral toward the lower end of the chamber.

19. Apparatus of claim 16 in which the centrifugal diffuser means comprises:

a hydration tank having a wall surrounding the outer chamber for receiving and hydrating the mixture discharged from the outer chamber.

20. Apparatus of claim 19:

wherein the outside wall of the outer chamber extends from the lower end of the outer chamber upward to an elevation lower than the inlet of the inner chamber and lower than the upper elevation of the hydration tank wall, the upper end of the outer chamber being open above the outside wall so that the upper end of the outside wall forms the outlet of the outer chamber; and

wherein the inner chamber has a plurality of outlets so that the mixture flows centrifugally from the inner chamber and around the inside surface of the outer chamber'"'"'s outside wall, the mixture thereby flowing circumferentially upward through the outer chamber and over the outer chamber'"'"'s outside wall into the hydration tank.

21. Apparatus of claim 19:

wherein the hydration tank has a floor extending below the inner and outer chambers, the inner and outer chambers being supported above the tank floor; and

wherein the hydration tank has an outlet in the floor below the inner and outer chambers for discharging the gel from the tank.

22. Apparatus of claim 16 in which the inner chamber comprises:

a cylindrical post of smaller diameter than the inner chamber and extending from about the center of the lower end of the chamber towards the upper end of the inner chamber in order to create an annular flow path and retard the flow of the mixture through the inner chamber and to reduce vortexing.

23. Apparatus of claim 1, comprising:

dilution means, having a gel inlet connected to an outlet of the centrifugal diffuser and a water inlet, for maintaining a substantially constant differential pressure between the water inlet and the gel inlet and for mixing water with the gel and producing a diluted gel.

24. Apparatus of claim 23, comprising:

a water supply, the water being at a higher pressure than the gel in order to provide a differential pressure mixing energy; and

wherein the dilution means is further defined as injecting water from the water supply into the gel and as adjusting the flow rate of the water injected into the gel in response to changes in the flow rate of the gel from the centrifugal diffuser such that the gel and water are mixed at about the same mixing energy at all flow rates of the gel.

25. Apparatus of claim 24 in which the dilution means comprises:

a mixing chamber having a water inlet, a gel inlet, and an outlet for discharging the diluted gel; and

a valve, movably disposed between the water inlet and the mixing chamber, for regulating the size of an orifice between the water inlet and the mixing chamber and thereby regulating the flow of water from the water inlet into the mixing chamber;

the valve having a first surface exposed to the water pressure in the water inlet and a second surface exposed to the gel pressure in the gel inlet so that changes in the water pressure or gel pressure move the valve and change the size of the orifice and thereby maintain a substantially constant differential pressure between the water pressure in the water inlet and the gel pressure in the gel inlet.

26. Apparatus of claim 25 in which the valve comprises:

a first conduital member connected to the first and second surfaces of the valve and telescopingly engaged with a second conduital member such that the first and second conduital members surround the mixing chamber and define a flow passageway from the gel inlet to the outlet with the water inlet surrounding the first and second conduital members; and

wherein at least one of the conduital members includes a plurality of orifices positioned around the mixing chamber so that movement of the first conduital member varies the size of the orifices between a fully opened size and a fully closed size.

27. Apparatus of claim 23, comprising:

a viscometer, connected to an outlet of the dilution means, for measuring the viscosity of the diluted gel and producing a viscosity signal; and

control means for receiving the viscosity signal and adjusting the flow of gel from the centrifugal diffuser to the dilution means and thereby adjust the viscosity of the diluted gel to a desired viscosity.

28. Apparatus of claim 27:

wherein the control means is further defined as comparing the viscosity signal to a setpoint signal indicative of the desired viscosity of the diluted gel and generating a control signal indicative of the flow of gel from the centrifugal diffuser to the dilution means necessary to achieve the desired viscosity; and

in which the apparatus comprises a metering pump, connected between the centrifugal diffuser and the dilution means, for receiving the control signal and pumping a correlating flow of gel from the centrifugal diffuser to the dilution means.

29. Apparatus for hydrating a particulated polymer and producing a gel, such as a well treatment gel, comprising:

water spraying induction mixing means for mixing the polymer with water to form a water-polymer mixture;

separating means, connected to the mixing means, for receiving the water-polymer mixture and separating air therefrom;

a pump, connected to the separating means, for imparting motive energy to the mixture and pumping the mixture from the separating means; and

a centrifugal diffuser means, connected to the pump, for receiving the mixture discharged from the pump and passively converting the motion of the mixture into circular motion, thereby centrifugally dissipating the motive energy of the mixture, centrifugally separating air from the mixture, and flowing the mixture in a first-fluid-in, first-fluid-out flow regime in order to hydrate the polymer into a gel.

30. Apparatus for hydrating a particulated polymer and producing a gel, such as a well treatment gel, comprising:

water spraying induction mixing means for mixing the polymer with a water spray and

discharging a water-polymer mixture having a motive energy from the outlet of the mixing means;

a centrifugal separator means, connected to the outlet of the mixing means, for receiving the mixture and passively converting the motion of the mixture into circular motion, thereby centrifugally separating air from the mixture and providing a flow path for the discharge of the mixing means which does not significantly restrict air flow through the mixing means; and

a pump, connected to an outlet of the centrifugal separator, for pumping the centrifugally separated mixture to a hydration tank.