Method for making optical probe

• US 5,397,411 A
• Filed: 12/19/1991
• Issued: 03/14/1995
• Est. Priority Date: 05/22/1990
• Status: Expired due to Term

• Current Assignee: Bruce A. Mckinley, Camino Neurocare, Inc.
• Original Assignee: Optex Biomedical, Inc.
• Inventors: Costello, David J., Schlain, Leslie A., Singh, Raghuvir, Salter, James R., Kosa, Nadhir B.
• Primary Examiner(s): Thurlow, Jeffery
• Assistant Examiner(s): VARGOT, MATHIEU D
• Application Number:
  US07/810,479
• Time in Patent Office: 1,181 Days
• Field of Search: 264/1.4, 264/1.5, 264/1.7, 264/22, 264/263, 264/101, 264/103, 264/162, 264/511, 264/254, 264/261, 264/265, 264/278, 264/292, 264/339, 264/2.6, 128/632, 128/634, 128/637, 385/12, 385/13, 156/172, 156/173, 156/196, 156/206, 156/154, 156/273.5, 156/275.3, 425/3, 425/508, 425/510, 425/392
• US Class Current: 156/154
• CPC Class Codes: G01N 2021/7706 Reagent provision
• CPC Class Codes: G01N 2021/7793 Sensor comprising plural indicators
• CPC Class Codes: G01N 21/7703 using reagent-clad optical fibres or optical waveguides using measurement of total internal reflection or attenuated total reflection G01N21/552; optical fibres or waveguides per se G02B
• CPC Class Codes: G02B 6/04 formed by bundles of fibres G02B6/24 takes precedence
• CPC Class Codes: G02B 6/362 Vacuum holders for optical elements
• CPC Class Codes: G02B 6/40 having fibre bundle mating means
• CPC Class Codes: Y10T 436/204998 Inorganic carbon compounds
• CPC Class Codes: Y10T 436/207497 Molecular oxygen

Abstract

A method for making an optical fiber bundle which, in one aspect, includes bending each of a plurality of optical fibers to form a bend therein and then suspending the fibers over a suspension member; holding the fibers taut under tension; applying potting material to the fiber bends and curing it; and removing the fibers from the suspension member.

Claims

1. Method for making an optical fiber bundle, the method comprising

bending each of a plurality of optical fibers to form a fiber bend,

suspending the plurality of fibers at the fiber bends over a suspension member,

holding the fibers taut under tension to maintain the fiber bends,

applying first potting encapsulating material to a portion of the fibers adjacent the fiber bends,

curing the first potting encapsulating material,

after removing the plurality of fibers from the suspension member applying second potting encapsulating material to the fiber bends, and

curing the second potting encapsulating material.

2. The method of claim 1 wherein sufficient potting encapsulant material is applied so that there is at least about 0.0014 inches of cured potting material between the exterior surface of each fiber and an exterior surface of the optical fiber bundle.

3. The method of claim 1 wherein the suspension member is a circular first spider having a central opening traversed by a plurality of spokes secured to the first spider, only one fiber section disposed between each pair of spokes.

4. The method of claim 1 wherein the suspension member is a circular first spider having a central opening and one spoke traversing the opening and secured to the first spider, the fiber bends disposed over the spoke so that no two fiber bends touch each other.

5. The method of claim 1 wherein weight means attached to the fibers provide tension of the fibers and a vacuum chuck disposed beneath the suspension member receives and holds the ends of the optical fibers.

6. The method of claim 1 including heat treating the fiber bends with hot air prior to applying potting encapsulating material to the fiber bends to relieve internal stresses in the optical fibers so that their tendency to un-bend is reduced.

7. The method of claim 1 wherein the potting encapsulating material is cured with intermittent pulses of ultraviolet radiation.

8. The method of claim 7 wherein pulsed application of curing ultraviolet radiation is effected by alternately moving a shutter between the fibers and a source of the ultraviolet radiation.

9. The method of claim 1 including also suspending a thermocouple on the suspension member with two thermocouple leads attached thereto and extending therefrom along with ends of the optical fibers.

10. The method of claim 9 wherein the thermocouple is disposed more centrally in the bundle than are the fibers.

11. The method of claim 1 including also

electrostatically neutralizing the fibers to facilitate the handling of them.

12. The method of claim 4 including also

passing the fibers through a spider member disposed beneath the suspension member to further maintain them in position.

13. The method of claim 12 wherein the spider member is a second circular spider having a central opening traversed by a plurality of spokes secured to the second spider, only one fiber section disposed between each pair of spokes.

14. The method of claim 1 including also

emplacing a movable shield about the fibers during curing of potting encapsulating material.

15. Method for making an optical fiber bundle, the method comprising

bending each of a plurality of optical fibers to form a fiber bend in each fiber,

suspending the plurality of fibers over a first circular spider having a central opening traversed by a plurality of spokes, the spokes secured to the first circular spider, one fiber section disposed between each pair of spokes,

with the ends of the fibers distant from the fiber bends received in and held by a clamping means for holding the fibers taut under tension,

applying first potting encapsulating material to a portion of the fibers adjacent the fiber bends,

curing the first potting encapsulating material with intermittent pulses of ultraviolet radiation,

removing the plurality of fibers from the first circular spider and from the clamping means,

applying second potting encapsulating material to the fiber bends, and

curing the second potting encapsulating material.

16. Method for making an optical fiber sensor probe, the method comprising

bending each of a plurality of optical fibers to form a fiber bend in each fiber,

suspending the plurality of fibers over a suspension means secured to a probe fabrication apparatus,

with the ends of the fibers distant from the fiber bends received in and held by a clamping means for holding the fibers taut under tension, the clamping means secured to the probe fabrication apparatus,

applying first potting encapsulating material to a portion of the fibers adjacent the fiber bends,

curing the first potting encapsulating material with intermittent pulses of ultraviolet radiation,

removing the plurality of fibers from the suspension means and from the clamping means,

applying second potting encapsulating material to the fiber bends,

curing the second potting encapsulating material,

forming gaps in each of the fibers for receiving and holding a chemical indicator which reacts to a particular chemical,

coating the fibers and the gaps with protective coating material,

emplacing chemical indicator material in each gap, and

applying a semi-permeable membrane material over each gap, the membrane material permitting the passage therethrough of only the particular chemical to which the chemical indicator in the gap reacts.

17. The method of claim 16 wherein the gaps are formed by ablating optical fiber and cured potting encapsulant material with an excimer laser.

18. The method of claim 17 wherein the gaps are five-walled openings.

19. The method of claim 17 wherein the gaps are longitudinally spaced apart from each Other by at least 665 microns.

20. The method of claim 18 wherein the gaps are between 85 and 115 microns long, about 130 to about 160 microns wide, and between 130 and 160 microns deep and two faces of a fiber are exposed in each gap.

21. The method of claim 17 wherein each gap is at least 2240 microns distant from an end tip of the probe.

22. The method of claim 16 wherein the suspension means comprises

a micro hook for each fiber, each micro hook supporting an individual fiber at its fiber bend, the micro hooks extending from micro hook holders.

23. The method of claim 22 wherein the micro hooks are disposed so that no two fiber bends are in contact.

24. The method of claim 16 wherein the clamping means comprises for each individual fiber a first sheet magnet connected to a magnet mount member and a second sheet magnet emplaceable on the first sheet magnet, the magnet mount member movable and the fiber being held between the two magnets so that the fibers supports the weight of the two magnets and the magnet mount member.

25. The method of claim 23 wherein portions of the fibers adjacent the fiber bends are held apart by fiber holders connected to the probe fabrication apparatus so that these portions are not in contact.

26. The method of claim 25 wherein the micro hooks are sized and disposed, the fiber holders are sized and disposed, the fibers are of such a diameter, and potting encapsulant material is applied so that the resulting probe is substantially circular and its diameter ranges between about 600 microns and about 730 microns.

27. The method of claim 16 wherein sufficient potting encapsulant material is used so that there is at least about 0.0014 inches of cured potting encapsulant material between and exterior surface of each fiber and an exterior surface of the probe.

28. The method of claim 16 including also suspending a thermocouple on the suspension means with two thermocouple leads attached thereto and extending therefrom along with ends of the optical fibers.

29. The method of claim 28 wherein the thermocouple is disposed more centrally in the probe than are the optical fibers.

30. The method of claim 16 including also

electrostatically neutralizing the fibers to facilitate the handling of them.

31. The method of claim 16 wherein the gaps are longitudinally spaced apart from each other by at least 665 microns.

32. The method of claim 16 wherein the gaps are between 85 and 115 microns long, about 130 to about 160 microns wide, and between 130 and 160 microns deep and two fiber faces of a fiber are exposed in each gap.

33. The method of claim 16 wherein each gap is at least 2240 microns distant from an end tip of the probe.

34. The method of claim 23 including also

applying heat to the micro hook holders, micro hooks, and fiber bends by blowing hot air at about 80°

C. on them to relieve internal stresses in the fiber bends and reduce their tendency to spring back.