Method and apparatus for testing the integrity of filter elements

• US 5,417,101 A
• Filed: 06/09/1992
• Issued: 05/23/1995
• Est. Priority Date: 06/10/1991
• Status: Expired due to Term

• Current Assignee: Pall Corporation (Danaher Corporation)
• Original Assignee: Pall Corporation (Danaher Corporation)
• Inventors: Weich, Gerhard
• Primary Examiner(s): Williams, Hezron E.
• Assistant Examiner(s): LARKIN, DANIEL SEAN
• Application Number:
  US07/895,841
• Time in Patent Office: 1,078 Days
• Field of Search: 73/38, 73/40
• US Class Current: 73/38
• CPC Class Codes: B01D 2201/0446 suspended from plates at the upper side of the filter elements
• CPC Class Codes: B01D 2201/0469 Filter tubes connected to collector tubes
• CPC Class Codes: B01D 2201/088 Arrangements for killing microorganisms
• CPC Class Codes: B01D 2201/287 Filtering elements with a vertical or inclined rotation or symmetry axis
• CPC Class Codes: B01D 29/114 arranged for inward flow filtration B01D29/15, B01D29/33 take precedence
• CPC Class Codes: B01D 29/52 in parallel connection
• CPC Class Codes: B01D 29/603 by flow measuring
• CPC Class Codes: B01D 29/92 for discharging filtrate
• CPC Class Codes: B01D 29/96 in which the filtering elements are moved between filtering operations; Particular measures for removing or replacing the filtering elements; Transport systems for filters B01D29/09, B01D29/70 take precedence
• CPC Class Codes: B01D 65/104 Detection of leaks in membrane apparatus or modules

Abstract

A method and apparatus for testing the integrity of filter elements is provided. The filter assembly comprises a plurality of filter elements which are subdivided into a plurality of sections. By measuring the gas flow rate under known pressure conditions through all of the sections or a selected portion of the sections, defective filter elements can be isolated in a systematic manner.

Claims

1. A method of testing the integrity of filter elements in a filter assembly comprising a plurality of filter elements which are subdivided into a plurality of sections, said method comprising the steps:

a) wetting a filter material of said plurality of filter elements;

b) subjecting the filter elements with wetted filter material to a gas pressure;

c) measuring a bulk gas flow rate through the wetted filter material of all of said plurality of filter elements;

d) determining whether the measured bulk gas flow rate deviates from a first desired flow rate by an amount within a first preset range, wherein a deviation within said preset range indicates that all filter elements are intact;

e) closing gas passage through at least one section of filter elements containing a portion of said plurality of filter elements;

f) measuring a bulk gas flow rate through the wetted filter material of filter elements disposed in remaining sections open to gas passage;

g) determining whether the measured bulk gas flow rate of step f) deviates from a second desired flow rate corresponding to the number of filter elements disposed in remaining sections open to gas passage by an amount within a second preset range, wherein a deviation of the measured bulk gas flow rate of step f) from a second desired flow rate within the second preset range indicates that one or more of the filter elements in said at least one section of step e) is not intact.

2. Method of claim 1, wherein when the measured bulk gas flow rate of step f) exceeds said second desired flow rate by an amount greater than allowed by said second preset range, the steps e), f) and g) are repeated while closing the gas passage in step e) for other sections of said plurality of filter elements until a deviation is found in step g) indicating a single section of filter elements in which at least one filter element is not intact.

3. Method of claim 1 wherein said gas pressure is in the range of 50 to 6000 mbar.

4. Method of claim 1 wherein said gas pressure is held at a constant value.

5. Method of claim 1 wherein said gas is air.

6. Method of claim 1 wherein said filter elements have been subjected to a sterilization at preselected temperatures prior to said integrity testing.

7. A filter assembly for carrying out the method of claim 1 comprising:

a plurality of filter elements divided into a plurality of sections, each section containing a portion of said plurality of filter elements;

a plurality of outlet headers, each one of said plurality of headers being connected to a respective one of the plurality of sections, said headers communicating with individual outlet openings of the filter elements;

a plurality of valves, each one of said plurality of valves coupled to a corresponding outlet conduit.

8. The filter assembly of claim 7, wherein said plurality of filter elements are arranged in a vessel.

9. Filter assembly of claim 7 wherein each of said sections of filter elements connected to each of said outlet headers comprises in the range of 2 to 15 filter elements.

10. A filter assembly according to claim 7 wherein each of said sections of filter elements connected to each of said outlet headers comprises in the range of 3 to 7 filter elements.

11. A method of testing the integrity of filter elements in a filter assembly comprising a plurality of filter elements which are subdivided into a plurality of sections, said method comprising:

a) subjecting the filter elements to a gas pressure;

b) measuring a parameter indicative of integrity of the plurality of filter elements;

c) determining whether the measured parameter deviates from a first desired parameter by an amount within a first preset range, wherein a deviation within the preset range indicates that the filter elements are intact;

d) closing gas passage through at least one section of filter elements;

e) measuring a parameter indicative of integrity of the filter elements disposed in remaining sections open to gas passage; and

f) determining whether the measured parameter of step e) deviates from a second desired parameter corresponding to the number of filter elements disposed in remaining sections open to gas passage by an amount within a second preset range, wherein a deviation of the measured parameter of step e) from a second desired parameter within the second preset range indicates that one or more of the filter elements in said at least one section of step d) is not intact.

12. A method of testing the integrity of filter elements as claimed in claim 11 wherein the parameter indicative of integrity of the plurality of filter elements includes a bulk gas flow rate through the filter elements.

13. A method of testing the integrity of filter elements as claimed in claim 11 further comprising:

g) continuing to close gas passage through said at least one section and closing gas passage through another section when the measured parameter of step e) deviates from the a second desired parameter by an amount outside of the second preset range.

14. A method of testing the integrity of filter elements as claimed in claim 13 further comprising repeating steps e), f) and g) until the measured parameter of step e) deviates from the second desired parameter by an amount within the second preset range.