Method and apparatus for dissolving a treating material

• US 5,419,355 A
• Filed: 11/12/1993
• Issued: 05/30/1995
• Est. Priority Date: 11/12/1993
• Status: Expired due to Fees

• Current Assignee: OLIN Corporation
• Original Assignee: OLIN Corporation
• Inventors: Brennan, James P., Telese, Rocco
• Primary Examiner(s): Schwadron, Martin P.
• Assistant Examiner(s): Lee, Kevin L.
• Application Number:
  US08/151,328
• Time in Patent Office: 564 Days
• Field of Search: 137/268, 137/1, 422/261, 422/264, 422/282, 422/283, 239/310
• US Class Current: 137/1
• CPC Class Codes: B01F 21/22 using additional holders in conduits, containers or pools for keeping the solid material in place, e.g. supports or receptacles
• CPC Class Codes: C02F 1/688 Devices in which the water progressively dissolves a solid compound
• CPC Class Codes: C02F 1/76 with halogens or compounds of halogens C02F1/4674 takes precedence
• CPC Class Codes: Y10T 137/0318 Processes
• CPC Class Codes: Y10T 137/4891 With holder for solid, flaky or pulverized material to be dissolved or entrained

Abstract

An apparatus and method for dissolving a chlorine containing treating material such as calcium hypochlorite in which water is fed to a container preferably in the form of a column containing the treating material. The water is caused to cyclically rise in the container to a predetermined height to dissolve a portion of the material and then discharge to a storage container to empty the material containing container. The height at which the water rises within the container, the cross-sectional area of the container and the length of time the liquid is in contact with the material during the cycle is set to produce a solution having a concentration of from between about 2 to about 18% available chlorine at a feed rate of at least about 2 lbs/hr available chlorine. The cyclical action is preferably achieved through the use of a siphon tube connected to the material holding container and through which the fluid in the container is discharged. The ratio of the internal cross-section area of the column to the internal cross-sectional area of the siphon tube is less than 700 and preferably in the range of 500 to 100.

Claims

1. An apparatus for dissolving a chlorine-containing solid treating material to provide a solution into a system to be treated, comprising:

(a) a container for holding said chlorine-containing solid treating material;

(b) an inlet line for supplying a fluid to said container;

(c) a siphon comprising a siphon tube connected to a point on said container or said inlet line and being a generally inverted U-shape of a predetermined height above the base of said container, but less than the overall height of said container;

said siphon tube constructed to (1) permit said fluid in said container to cyclically rise in said container to said predetermined height while in contact with said treating material, thereby solubilizing at least a portion of said treating material and forming a solution, and (2) then cyclically discharge said solution to empty the container of the solution, wherein the ratio of internal cross-section of the container to the internal cross-sectional area of the syphon tube being 700;

1 or less.

2. The apparatus of claim 1 wherein said ratio of cross-sectional areas is from about 500:

1 to about 100;

1.

3. The apparatus of claim 1 wherein said container is a column and said predetermined height of said siphon tube is such that the fluid can rise in said container to a height greater than the greatest internal diameter of said column.

4. The apparatus of claim 1 further including an adjustable flow control valve in said inlet line to provide a constant flow rate of fluid to said container.

5. The apparatus of claim 1 wherein said treating material is calcium hypochlorite.

6. The apparatus of claim 1 wherein said predetermined height and said internal cross-sectional area of said container and said siphon tube and said flow rate of fluid into the container are selected to produce a solution having a concentration of about 2 to about 18% available chlorine and a feed rate of at least 2 pounds per hour of available chlorine.

7. The apparatus of claim 1 wherein said input line contains a drain valve.

8. A method for dissolving a chlorine containing solid soluble treating material to provide a solution for dispensing into a system to be treated comprising:

(a) providing a container for holding a quantity of treating material;

(b) providing a source of fluid to said container;

(c) providing a siphon comprising a siphon tube and causing the fluid to cyclically rise in said container to a predetermined height in contact with the treating material contained therein thereby solubilizing at least a portion of said treating material and forming a solution, and then discharging said solution through the siphon tube into a storage container; and

(d) selecting the internal cross-sectional area of the container and the internal cross-sectional area of the siphon tube such that the ratio of these container area to the siphon tube area is 700;

1 or less.

9. The method of claim 8 further including selecting the height at which the fluid-rises in the material-containing container and the internal cross-sectional areas of the column and siphon tube such that a solution is produced having a concentration of from about 2 to about 18% available chlorine and a feed rate of at least about 1 pounds per hour of available chlorine.

10. The method of claim 8 wherein said fluid reaches said predetermined height and said solution is discharged at least once an hour.

11. The method of claim 8 wherein said fluid reaches said predetermined height and said solutions discharged at least once every half hour.

12. The method of claim 8 wherein said fluid reaches said predetermined height and said solution is discharged once every 1 to 15 minutes.

13. The method of claim 8 wherein the time at which no fluid is in contact with said treating material in said container during the filling and discharge cycle is one minute or less.

14. A method of dissolving a chlorine containing solid soluble treating material to provide a solution containing available chlorine comprising:

(a) providing a container for holding said treating material;

(b) causing fluid cyclically to flow into said container to contact a portion of said treating material in the container to cause the material to dissolve and then discharge the resulting solution into a storage chamber; and

(c) controlling (i) the height of the fluid in the container while in contact with said treating material before the fluid is discharged and (ii) the length of time the fluid remains in contact with the material to thereby provide a solution having a concentration of between about 2 to about 18% available chlorine at a feed rate of at least about 2 pounds per hour available chlorine.