Process and apparatus for controlling and metering the pneumatic transfer of solid particulates

• US 5,464,591 A
• Filed: 02/08/1994
• Issued: 11/07/1995
• Est. Priority Date: 02/08/1994
• Status: Expired due to Fees

• Current Assignee: David B. Bartholic
• Original Assignee: David B. Bartholic
• Inventors: Bartholic, David B.
• Primary Examiner(s): McMahon, Timothy M.
• Assistant Examiner(s): BHAT, NINA NMN
• Application Number:
  US08/193,456
• Time in Patent Office: 637 Days
• Field of Search: 422/142, 422/144, 422/145, 422/146, 422/147, 415/1, 208/127, 208/161, 208/86, 208/88
• US Class Current: 422/142
• CPC Class Codes: B01J 8/001 Controlling catalytic processes B01J8/1809 takes precedence
• CPC Class Codes: B01J 8/0015 Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
• CPC Class Codes: B01J 8/26 with two or more fluidised beds, e.g. reactor and regeneration installations
• CPC Class Codes: C10G 11/187 Controlling or regulating

Abstract

The method of controlling the flow of a fluidizable particulate solid, e.g., FCC catalyst, which comprises: (a) passing a fluidized stream of the particulate solid downwardly from a source of the particulate solid, e.g., an FCC regenerator, in a first conduit to a junction with a second conduit where the solid particulate is mixed with a stream of a fluid transport medium from a third conduit; (b) passing a stream of the resulting mixed solid particulate/transport medium upwardly in the second conduit at an angle less than 90° from the first conduit for a distance at least as great as the diameter of the first conduit at the junction into a fourth conduit; (c) transporting the particulate solid/fluid transport medium stream in the fourth conduit to a desired location; and (d) controlling the mass flow of the particulate solid in the fourth conduit by setting the flow rate of the transport medium in the third conduit. By determining the temperatures of the particulate solid in the first conduit, the transport medium in the third conduit and the particulate solid transport medium mixture, the mass flow of the particulate solid in the fourth conduit may be controlled by setting the flow rate of the transport medium in the third conduit. Apparatus for carrying out the method is also included.

Claims

1. The method of controlling the flow of a fluidized particulate solid used in the processing of a hydrocarbon feedstock, which comprises:

(a) passing a fluidized stream of said particulate solid downwardly from a pressurized source of said particulate solid in a first conduit to a junction with a second conduit where said solid particulate is mixed with a stream of a fluid transport medium from a third conduit;

(b) passing a stream of the resulting mixed solid/particulate transport medium upwardly in the second conduit from the first conduit for a distance at least as great as the diameter of the first conduit at said junction to a fourth conduit;

(c) transporting the particulate solid/fluid transport medium stream in the fourth conduit to a desired location;

(d) determining the temperature of the particulate solid in the first conduit;

(e) determining the temperature of the transport medium in the third conduit;

(f) determining the temperature of the solid particulate/transport medium mixture; and

(g) setting the flow rate of the transport medium in the third conduit to produce a target mass flow of the particulate solid in the fourth conduit determined in accordance with the following equation;

space="preserve" listing-type="equation">Mp=Mm·

Cm·

(T46-T40)/Cp·

(T36-T46)

where;

Mp represents the target mass flow of the particulate solid in the fourth conduit,

Mm represents the mass flow of the transport medium in the third conduit,

Cp represents the heat capacity of the particulate solid,

Cm represents the heat capacity of the transport medium,

T46 represents the temperature of the particulate solid in the fourth conduit,

T40 represents the temperature of the transport medium in the third conduit,

T36 represents the temperature of the particulate solid in the first conduit.

2. The method of claim 1, further including passing a second stream of a fluid transport medium through a fifth conduit into said fourth conduit to increase the velocity and lower the density of the particulate solid/transport medium therein.

3. The method of controlling the flow of a fluidized particulate solid used in the processing of a hydrocarbon feedstock, which comprises:

(a) passing a fluidized stream of said particulate solid downwardly from a source of said particulate solid in a first conduit to a junction with a second conduit where said solid particulate is mixed with a stream of a fluid transport medium from a third conduit;

(b) passing a stream of the resulting mixed solid particulate/transport medium upwardly in the second conduit at an angle less than 90°

from the first conduit for a distance at least as great as the diameter of the first conduit at said junction into a fourth conduit;

(c) transporting the particulate solid/fluid transport medium stream in the fourth conduit to a desired location; and

(d) controlling the mass flow of the particulate solid in said fourth conduit by setting the flow rate of said transport medium in said third conduit.

4. The method of claim 3, further including passing a second stream of a fluid transport medium through a fifth conduit into said fourth conduit to increase the velocity and lower the density of the particulate solid/transport medium therein.

5. The method of claim 4, wherein a stream of said fluid transport medium supplied by a sixth conduit is split by a three-way control valve to pass a first portion thereof into said third conduit and a second portion thereof into said fifth conduit.

6. The method of claim 5, wherein said fluid transport medium is passed from said fifth conduit into said fourth conduit at a point upstream of the point at which said solid particulate/transport medium is passed into said fourth conduit.

7. The fluidized process of claim 3, wherein said improvement further comprises:

(a) determining the temperature of the particulate solid in the first conduit;

(b) determining the temperature of the transport medium in the third conduit;

(c) determining the temperature of the solid particulate/transport medium mixture; and

(d) setting the flow rate of the transport medium in the third conduit to produce a target mass flow of the particulate solid in the fourth conduit determined in accordance with the following equation;

space="preserve" listing-type="equation">Mp=Mm·

Cm·

(T46-T40)/Cp·

(T36-T46)

where;

Mp represents the target mass flow of the particulate solid in the fourth conduit,

Mm represents the mass flow of the transport medium in the third conduit,

Cp represents the heat capacity of the particulate solid,

Cm represents the heat capacity of the transport medium,

T46 represents the temperature of the particulate solid in the fourth conduit,

T40 represents the temperature of the transport medium in the third conduit,

T36 represents the temperature of the particulate solid in the first conduit.

8. The fluidized process of claim 7, further including measuring a selected parameter of said process or characteristic of said particulate solid transported, and re-setting the flow rate of the transport medium in the third conduit in response to variations in the selected parameter.

9. The fluidized process of claim 8, wherein said process is a fluidized catalytic cracking process and said selected parameter or characteristic is at least one of carbon monoxide in the regenerator flue gas, sulfur oxides in the regenerator flue gas, bottoms product yield, equilibrium catalyst activity, gasoline fraction octane or transported particulate solid temperature.

10. Apparatus useful for controlling the flow of a fluidized particulate solid to be transported in a unit for the processing of a hydrocarbon feedstock, which apparatus comprises:

(a) a downwardly extending first conduit having upper and lower ends, the upper end thereof being connectable to a source of said particulate solid;

(b) a second conduit having upper and lower ends, the lower end thereof being connected to the lower end of said first conduit to place said first and second conduits in flow communication, said second conduit having a length extending upwardly from its junction with said first conduit for a distance at least as great as the diameter of the lower end of said first conduit;

(c) a third conduit having first and second ends, said first end being connectable to a source of a fluid transport medium and said second end being connected to said junction to place said third conduit in flow communication with said first and second conduits; and

(d) a fourth conduit having a first end and a second end and being in flow communication with said second conduit for receiving a stream of said particulate solid and said transport medium, the second end of said fourth conduit being connectable to a vessel for receiving the transported particulate solid.

11. The apparatus of claim 10, further including a fifth conduit having a first end and a second end, the second end thereof being connected to and in flow communication with the first end of said fourth conduit, and the first end thereof being connectable to said source of transport fluid.

12. The apparatus of claim 11, wherein the upper end of said second conduit is connected to said fourth conduit at a point intermediate the first and second ends thereof.

13. The apparatus of claim 11, further including a three-way control valve having a first port connected to the first end of said third conduit and second port connected to the first end of said fifth conduit, and a sixth conduit connecting a third port of said three-way valve to said source of transport medium.

14. The apparatus of claim 13, further including valve means in said sixth conduit between said three-way valve and said source of transport medium for controlling the flow of said transport medium in said sixth conduit to said three-way valve.

15. The apparatus of claim 14, further including means for measuring the temperature of each of said particulate solid in said first conduit, said transport medium in said sixth conduit and said particulate solid/transport medium stream in said fourth conduit, means for measuring the mass flow of said transport medium in said sixth conduit;

flow control means connected to said sixth conduit for controlling the flow of said transport medium therein;

computer/controller means for receiving signals from each of said temperature measuring means and said mass flow measuring means and outputting a signal to said three-way control valve to control the operation thereof.

16. The apparatus of claim 10, wherein the length of said second conduit is at least 5 times the diameter of the lower end of said first conduit.

17. The apparatus of claim 10, wherein said angle formed by said first and second conduits is from about 30°

to about 60°

.

18. The apparatus of claim 17, wherein said angle is less than about 45°

.

19. The apparatus of claim 10, wherein during use said source of particulate solid supplies said solid to said first conduit at a pressure greater than the pressure in said fourth conduit.

20. The apparatus of claim 10, further including means for measuring the temperature of each of said particulate solid in said first conduit, said transport medium in said third conduit and said particulate solid/transport medium stream in said fourth conduit, means for measuring the mass flow of said transport medium in said third conduit;

flow control means connected to said third conduit for controlling the flow of said transport medium therein;

computer/controller means for receiving signals from each of said temperature measuring means and said mass flow measuring means and for outputting a signal to said flow control means to control the operation thereof.

21. The apparatus of claim 20, further including means for measuring a selected parameter at a control point (a) in said vessel for receiving the transported solid or (b) in a process employing said particulate solid and transmitting a signal to said computer/controller means.