Use of capillary-membrane sampling device to monitor oil-drilling muds

• US 5,469,917 A
• Filed: 12/14/1994
• Issued: 11/28/1995
• Est. Priority Date: 12/14/1994
• Status: Expired due to Term

• Current Assignee: Fia Solutions, Inc.
• Original Assignee: Duane K. Wolcott
• Inventors: Wolcott, Duane K.
• Primary Examiner(s): Schoeppel, Roger J.
• Application Number:
  US08/355,493
• Time in Patent Office: 349 Days
• Field of Search: 166/250, 166/264, 175/59, 175/60, 73/23.35, 73/23.26, 73/23.38, 73/23.41, 73/23.42
• US Class Current: 166/250.01
• CPC Class Codes: E21B 49/005 Testing the nature of borehole walls or the formation by using drilling mud or cutting data
• CPC Class Codes: G01N 1/34 Purifying; Cleaning processes or apparatus for extracting or separating nucleic acids from biological samples C12N15/1003
• CPC Class Codes: G01N 2030/025 Gas chromatography
• CPC Class Codes: G01N 2030/146 using membranes
• CPC Class Codes: G01N 33/2823 raw oil, drilling fluid or polyphasic mixtures hydrocarbon content of earth materials G01N33/241; prospecting G01V; drilling per se E21B

Abstract

A method for monitoring oil-drilling mud. A supported capillary membrane (SCMS) device having a support member, a capillary membrane permeable to hydrocarbons, and flights on the surface of the support member within which the capillary member is supported is disposed in a stream returning mud from a drill hole to the surface of an oil well. A stream of inert gas is passed through the SCMS device, thereby entraining hydrocarbon vapors in the gas stream and providing a sample of the hydrocarbons associated with the oil-drilling mud. The hydrocarbon-laden gas stream is input to an analytical instrument such as a gas chromatograph capable of identifying and quantitatively determining the concentrations of the hydrocarbons.

Claims

1. A method for monitoring oil-drilling mud, which comprises the steps of:

(a) providing a device comprising a support member, a capillary membrane permeable to hydrocarbons, and flights on the surface of the support member within which the capillary member is supported;

(b) disposing the device in a stream returning mud from a drill hole to the surface of an oil well;

(c) passing a stream of inert gas through the capillary membrane, thereby entraining hydrocarbon vapors in the gas stream; and

(d) inputting the gas stream containing the entrained hydrocarbon vapors to an analytical instrument capable of identifying and quantitatively determining the concentrations of the hydrocarbons.

2. The method of claim 1, wherein the device is disposed in the mud-return stream at the surface of the well.

3. The method of claim 1, wherein the device is disposed in the mud-return stream below ground in the well near a drill head.

4. The method of claim 3, further comprising the steps of:

(e) providing a flow controller to control the flow of gas through the device;

(f) disposing the flow controller in the well near the device;

(g) providing a gas-sensing unit for the identification and quantitative determination of the hydrocarbons entrained by the inert gas;

(h) disposing the gas-sensing unit in the well near the device;

(i) providing electronic hardware to process data from the gas-sensing unit and the flow controller;

(j) disposing the electronic hardware in the well near the device;

(k) programming the electronic hardware to process data from the gas-sensing unit and the flow controller;

(l) providing hydraulic generator vanes to provide power for the operation of the gas-sensing unit and the electronic hardware; and

(m) disposing the hydraulic generator vanes in the mud-return flow stream in the well near the device.

5. A method for sampling hydrocarbons associated with oil-drilling mud, the method comprising the steps of:

(a) providing a device comprising a support member, a capillary membrane permeable to hydrocarbons, and flights on the surface of the support member within which the capillary member is supported;

(b) disposing the device in a stream returning mud from a drill hole to the surface of an oil well; and

(c) passing a stream of inert gas through the capillary membrane, thereby entraining hydrocarbon vapors in the gas stream and obtaining a sample of the hydrocarbons associated with the oil-drilling mud.

6. The method of claim 5, wherein the device is disposed in the mud-return stream at the surface of the well.

7. The method of claim 5, wherein the device is disposed in the mud-return stream below ground in the well near a drill head.