Apparatus and method for the analysis of particle characteristics using monotonically scattered light

• US 5,471,299 A
• Filed: 07/29/1994
• Issued: 11/28/1995
• Est. Priority Date: 02/21/1992
• Status: Expired due to Term

• Current Assignee: The secretary of state for defence in her Britannic Majesty's Government of the United Kingdom of Great Britain And Northern Ireland
• Original Assignee: The secretary of state for defence in her Britannic Majesty's Government of the United Kingdom of Great Britain And Northern Ireland
• Inventors: Hirst, Edwin, Kaye, Paul H.
• Primary Examiner(s): Rosenberger, Richard A.
• Assistant Examiner(s): VIERRA EISENBERG, JASON D
• Application Number:
  US08/256,983
• Time in Patent Office: 487 Days
• Field of Search: 356/336-338, 356/340-343
• US Class Current: 356/336
• CPC Class Codes: G01J 2001/448 Array [CCD]
• CPC Class Codes: G01J 2001/4493 with image intensifyer tube [IIT]
• CPC Class Codes: G01N 15/1427 with the synchronisation of components, a time gate for operation of components, or suppression of particle coincidences
• CPC Class Codes: G01N 15/1436 the optical arrangement forming an integrated apparatus with the sample container, e.g. a flow cell
• CPC Class Codes: G01N 15/1459 the analysis being performed on a sample stream
• CPC Class Codes: G01N 2015/0046 in gas, e.g. smoke
• CPC Class Codes: G01N 2015/1402 Data analysis by thresholding or gating operations performed on the acquired signals or stored data
• CPC Class Codes: G01N 2015/144 Imaging characterised by its optical setup
• CPC Class Codes: G01N 2021/4714 Continuous plural angles

Abstract

An apparatus for the analysis of individual particle characteristics from an aerosol or other suspension of particles, of the type having a scattering chamber (15) with an ellipsoidal reflector (17) and an orifice leading to a rear chamber (20), and a monochromatic light source (10) adapted to transmit a collimated beam of light (11) along the main axis of the reflector (17) to impinge on a stream of the particles reflector (17), has an optical system (17, 32, 33, 34) arranged to collect light back-scattered from a particle, through a solid angle of at least 3π, pass the light to a a ccd video recorder (36) having a two dimensional array of a multitude of sensors.

The recorder (36) is associated with a data processor (37) and with an imaging screen (35) positioned such that rays of light scattered from the particle and imaged thereon by the optical system (17, 32, 33, 34) are monotonically ordered with respect to the angle of scattering of the rays from the particle.

Claims

1. Apparatus for analysis of individual particle characteristics from an aerosol or other suspension of particles in a particle stream, said apparatus including:

a scattering chamber including an optical system having an ellipsoidal reflector with an orifice therein leading to a rear chamber;

a monochromatic light source adapted to transmit a collimated beam of light along a main axis of the reflector;

means for directing said particle stream in a stream of finite thickness containing said particles through the beam of light at substantially a main focus of the reflector;

an optical system comprising a means for collecting scattered light from a solid angle of at least 3π

around a region where the particle stream crosses the light beam;

a detector having a two dimensional array of a multitude of sensors for forming an image from light scattered from a particle in the particle stream and collected by the optical system;

and a data processor for comparing parameters of the image with parameters stored in a memory to determine a characteristic of the particle;

the detector is associated with an imaging screen positioned behind a secondary focus of the reflector said optical system, said light source, and said means for directing, in combination, comprising a means for providing monotonically ordered scattered rays of light at said imaging screen such that, whatever part of the finite thickness of the particle stream occupied by the particle when it passes through the beam of light, rays of light scattered from the particle and imaged thereon by the optical system are monotonically ordered with respect to the angle of scattering of the rays from the particle so that the image recorded on the imaging screen is substantially independent of position of the particle in the particle stream.

2. Apparatus as claimed in claim 1 wherein the detector is a charged couple device (ccd) video camera.

3. Apparatus as claimed in claim 1 wherein the imaging screen is an image intensifier.

4. Apparatus as claimed in claim 1 further including trigger means for triggering the detector to store the image.

5. Apparatus as claimed in claim 4 wherein the trigger means includes sensor means for sensing scattered light not collected by the optical system and thereby determining presence of a particle in the beam of light.

6. Apparatus as claimed in claim 5 wherein the sensor means comprises a photomultiplier tube onto which is focussed scattered rays which pass through the orifice in the optical system into the rear chamber.

7. Apparatus as claimed in claims 4 wherein the trigger means includes a controller having an output to the detector.

8. Apparatus as claimed in claim 4 wherein the trigger means include means for triggering the detector only when a single particle is in the beam.

9. Apparatus as claimed in claim 1 wherein the rear chamber contains a second video camera to record scattered light not collected by the optical means.

10. Apparatus as claimed in claim 1 wherein the parameters compared relate to entire images.

11. Apparatus as claimed in claims 1 wherein the parameters compared relate to parts of images.

12. Apparatus as claimed in claim 1 wherein the parameters compared relate to resolving diffraction or interference maxima and minima.

13. Apparatus as claimed in claim 1 wherein the multitude of sensors are arrayed in a configuration of substantially 32 by 32 pixels.

14. Apparatus as claimed in claim 1 wherein the multitude of sensors are arrayed in a shape according to an expected image.

15. A method as claimed in claim 1 wherein said particle stream is an gaseous particle stream.

16. A method of analysing individual particle characteristics from an aerosol or other suspension of particles includes the steps of:

directing a particle stream of finite thickness containing said particles through a scattering chamber;

the scattering chamber including an optical system having an ellipsoidal reflector having a main focus and a secondary focus and with an orifice therein leading to a rear chamber;

a monochromatic light source adapted to transmit a collimated beam of light along a main axis of the reflector;

means for directing the particle stream through the beam of light at substantially the main focus of the reflector;

collecting by means of an optical system scattered light from a solid angle of at least 3π

around a region where the particle stream crosses the light beam;

the scattering chamber is associated with a detector having a two dimensional array of a multitude of sensors arranged to form an image from light scattered from a particle in the particle stream and collected by the optical system;

recording said image in said detector and passing information to a data processor, the data processor being adapted to compare parameters of the image with parameters stored in a memory to determine the nature of the particle;

the detector is associated with an imaging screen positioned behind the secondary focus of the reflector wherein the directing step includes locating said scattering chamber relative to said imaging screen such that, whatever part of the finite thickness of the particle stream occupied by the particle when it passes through the beam of light, rays of light scattered from the particle and imaged thereon by the optical system are monotonically ordered with respect to the angle of scattering of the rays from the particle so that the image recorded on the imaging screen is substantially independent of position of the particle in the particle stream.

17. A method as claimed in claim 16 wherein the detector is triggered to store an image by a triggering system including sensor means for sensing scattered light not collected by the optical system.

18. A method as claimed in claim 16 wherein said particle stream is an gaseous particle stream.