Gas analyzer for molten metals

• US 5,495,746 A
• Filed: 07/18/1994
• Issued: 03/05/1996
• Est. Priority Date: 08/30/1993
• Status: Expired due to Fees

• Current Assignee: Geoffrey K. Sigworth
• Original Assignee: Geoffrey K. Sigworth
• Inventors: Sigworth, Geoffrey K.
• Primary Examiner(s): Williams, Hezron E.
• Assistant Examiner(s): Politzer, Jay L.
• Application Number:
  US08/276,457
• Time in Patent Office: 596 Days
• Field of Search: 73/19.01, 73/19.07
• US Class Current: 73/19.07
• CPC Class Codes: G01N 1/125 adapted for sampling molten metals
• CPC Class Codes: G01N 33/2025 Gaseous constituents
• CPC Class Codes: G01N 7/10 by allowing diffusion of components through a porous wall and measuring a pressure or volume difference

Abstract

Disclosed is a probe for determining the gas content of molten metal. The probe comprises a porous filter head permeable to gas and impermeable to the molten metal and a small diameter tube having an upper portion and a lower portion, the tube attached to the filter head at the lower portion. A device for drawing a vacuum on the tube and a device for measuring gas pressure in the tube is provided.

Claims

1. A hollow probe for immersion in a molten metal for determining the gas content thereof by drawing a vacuum on the probe and permitting gas to permeate from the molten metal and equilibrate in the probe wherein gas pressure can be measured to determine the gas pressure in the molten metal, the probe comprising:

(a) a porous filter head permeable to gas in said molten metal and impermeable to said molten metal;

(b) a small diameter metal tube having an upper portion and a lower portion, the tube attached to said filter head at the lower portion; and

(c) said tube attached at said upper portion to means for drawing a vacuum on said tube and means for measuring gas pressure in said tube.

2. The probe in accordance with claim 1 wherein said small diameter tube has a ceramic coating thereon resistant to attack by molten metal.

3. The probe in accordance with claim 1 wherein said small diameter tube has an inside diameter in the range of 0.01 to 0.08 inch.

4. The probe in accordance with claim 1 wherein said small diameter tube is fabricated from copper.

5. The probe in accordance with claim 1 wherein said small diameter tube is fabricated from steel.

6. The probe in accordance with claim 1 wherein said small diameter tube is fabricated from stainless steel.

7. The probe in accordance with claim 1 wherein said lower portion of said tube has a cylindrical shaped lower section and said filter head has a cylindrical recessed section for fitting snugly to said cylindrical shoulder section.

8. The probe in accordance with claim 1 wherein said porous filter head is fabricated from a material selected from at least one of the group consisting of carbon, silicon nitride, titanium diboride, silicon carbide, alumina, zirconia, titania and mullite.

9. The probe in accordance with claim 1 wherein said porous filter head is fabricated from carbon and said tube is fabricated from steel.

10. The probe in accordance with claim 9 wherein the lower portion of said small diameter tube has a coating which prevents chemical reaction between the small diameter steel tube and the porous carbon filter head.

11. A hollow probe for immersion in a molten metal for determining the gas content thereof by drawing a vacuum on the probe and permitting gas to permeate from the molten metal and equilibrate in the probe wherein gas pressure can be measured to determine the gas pressure in the molten metal, the probe comprising:

(a) a porous carbon filter head permeable to gas in said molten metal and impermeable to said molten metal;

(b) a small diameter steel tube having an upper portion and a lower portion, the tube;

(i) attached to said carbon filter head at the lower portion, and

(ii) having at its lower portion a coating that prevents chemical reaction between said steel tube and said porous carbon filter head; and

(c) said tube attached at said upper portion to means for drawing a vacuum on said tube and means for measuring gas pressure in said tube.