Material and splint for orthopaedical, surgical and veterinary use and method of making same
First Claim
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1. A method for the production of a deformable material for orthopaedical, surgical, veterinary and technical applications, based upon poly-ε
- -caprolactone, wherein equimolecular weight amounts of ε
-caprolactone, polyurethane prepared of polyoxypropylene glycol and toluene-di-isocyanate, and ethylene-butylene-styrene-copolymer are reacted together under heating, and with reflux cooling of vapours during said reaction, triallylcyanurate in an amount of 0.3 to 3.5% wt./wt. and slowly oleic acid-imide in an amount of about 1% wt./wt. of the total mass are added, and the reaction product is cooled down, washed and granulated, and brought into the desired surgical or technical shape by injection moulding or extrusion, followed by irradiation with gamma rays of up to 2.5 Mrad, to obtain a solid flexible shape of flexibility and elasticity, as required for practical use.
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Abstract
A thermoplastic material, mainly to be used for splints and supports in orthopaedical, surgical and veterinary practice, is proposed for the fixation of body parts, the material including a copolymer of ε-caprolactone, polyurethane, and ethylene-butylene-styrene mixed with triallylcyanurate and oleic acid-imide, the copolymer mixture being gamma irradiated after processing, such that a degree of cross-linking of the molecules and a partially crystalline configuration results in a molded material with reproducible flexibility, elasticity and reciprocal stretch properties.
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5 Claims
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1. A method for the production of a deformable material for orthopaedical, surgical, veterinary and technical applications, based upon poly-ε
- -caprolactone, wherein equimolecular weight amounts of ε
-caprolactone, polyurethane prepared of polyoxypropylene glycol and toluene-di-isocyanate, and ethylene-butylene-styrene-copolymer are reacted together under heating, and with reflux cooling of vapours during said reaction, triallylcyanurate in an amount of 0.3 to 3.5% wt./wt. and slowly oleic acid-imide in an amount of about 1% wt./wt. of the total mass are added, and the reaction product is cooled down, washed and granulated, and brought into the desired surgical or technical shape by injection moulding or extrusion, followed by irradiation with gamma rays of up to 2.5 Mrad, to obtain a solid flexible shape of flexibility and elasticity, as required for practical use. - View Dependent Claims (2, 3, 4, 5)
- -caprolactone, wherein equimolecular weight amounts of ε
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