Self-contained cryogenic gas sampling apparatus and method

• US 5,501,080 A
• Filed: 12/14/1994
• Issued: 03/26/1996
• Est. Priority Date: 12/14/1994
• Status: Expired due to Fees

• Current Assignee: Lockheed Idaho Technologies Company
• Original Assignee: Lockheed Idaho Technologies Company
• Inventors: McManus, Gary J., Bird, Susan K., Motes, Billy G., Kotter, Dale K.
• Primary Examiner(s): Capossela, Ronald C.
• Application Number:
  US08/355,689
• Time in Patent Office: 468 Days
• Field of Search: 62/51.1, 62/55.5, 62/235.5, 73/863.11
• US Class Current: 62/55.5
• CPC Class Codes: B01D 8/00 Cold traps; Cold baffles pumps for evacuating by condensing or freezing F04B37/08
• CPC Class Codes: G01N 1/42 Low-temperature sample treatment, e.g. cryofixation
• CPC Class Codes: G01N 2001/2282 with cooling means

Abstract

Apparatus for obtaining a whole gas sample, composed of: a sample vessel having an inlet for receiving a gas sample; a controllable valve mounted for controllably opening and closing the inlet; a valve control coupled to the valve for opening and closing the valve at selected times; a portable power source connected for supplying operating power to the valve control; and a cryogenic coolant in thermal communication with the vessel for cooling the interior of the vessel to cryogenic temperatures.

A method of obtaining an air sample using the apparatus described above, by: placing the apparatus at a location at which the sample is to be obtained; operating the valve control to open the valve at a selected time and close the valve at a selected subsequent time; and between the selected times maintaining the vessel at a cryogenic temperature by heat exchange with the coolant.

Claims

1. Apparatus for obtaining a whole gas sample, comprising:

a sample vessel having an inlet for receiving a gas sample;

a controllable valve mounted in said inlet for controllably opening and closing said inlet;

valve control means coupled to said valve for opening and closing said valve at selected times;

a portable power source connected to said valve control means for supplying operating power to said valve control means;

a cryogenic coolant; and

means containing said coolant and placing said coolant in thermal communication with said vessel for cooling the interior of said vessel to cryogenic temperatures.

2. Apparatus as defined in claim 1 wherein said portable power source is a rechargeable battery.

3. Apparatus as defined in claim 2 further comprising means including a solar cell disposed for converting solar radiation into electricity and connected for recharging said battery.

4. Apparatus as defined in claim 1 wherein said means containing said coolant include a second vessel in which said sample vessel is installed.

5. Apparatus as defined in claim 4 wherein said second vessel is a dry shipper vessel.

6. Apparatus is defined in claim 1 wherein said coolant is liquid nitrogen.

7. Apparatus as defined in claim 1 wherein the gas sample is an environmental air sample.

8. Apparatus as defined in claim 1 wherein said means containing said coolant maintain a constant quantity of coolant in thermal communication with said sample vessel.

9. Apparatus as defined in claim 8 wherein said means containing said coolant comprise a coolant supply container and a coolant flow tube extending around said sample vessel and connected to said coolant supply container for maintaining a flow of coolant from said supply container and around said sample vessel.

10. Apparatus as defined in claim 9 wherein said tube has the form of a multi-turn coil surrounding said sample vessel.

11. A method of obtaining an air sample using the apparatus defined in claim 1 comprising:

placing the apparatus at a location at which the sample is to be obtained;

operating said valve control means to open said valve at a selected time and close said valve at a selected subsequent time; and

between the selected times maintaining said vessel at a cryogenic temperature by heat exchange with said coolant.

12. Apparatus for obtaining a whole gas sample, comprising:

a sample vessel having an inlet for receiving a gas sample;

a controllable valve mounted in said inlet for controllably opening and closing said inlet;

valve control means coupled to said valve for opening and closing said valve at selected times;

a portable power source connected to said valve control means for supplying operating power to said valve control means;

a cryogenic coolant; and

means containing said coolant and placing said coolant in thermal communication with said vessel for cooling the interior of said vessel to cryogenic temperatures, wherein said sample vessel is removable from said means containing said coolant.