Two continuous filtration system for supplying filtrate to automatic analyzers

• US 5,505,854 A
• Filed: 09/09/1994
• Issued: 04/09/1996
• Est. Priority Date: 09/09/1994
• Status: Expired due to Fees

• Current Assignee: Electric Power Research Institute
• Original Assignee: Electric Power Research Institute
• Inventors: King, Thomas, Meserole, Frank, Moser, Robert E., Richardson, Carl, Maller, Gordon, Hanley, Timothy, Maybach, Gerard B., Glover, Robert L.
• Primary Examiner(s): Drodge, Joseph W.
• Application Number:
  US08/302,432
• Time in Patent Office: 578 Days
• Field of Search: 210/96.1, 210/108, 210/333.01, 210/335, 210/321.69, 210/411, 210/427, 210/636, 210/739, 210/798, 210/902, 210/500.35, 210/96.2, 210/143, 210/650, 95/8, 95/13, 423/243.08, 423/243.09, 55/270, 422/62, 436/177
• US Class Current: 210/739
• CPC Class Codes: B01D 2321/04 Backflushing
• CPC Class Codes: B01D 61/146 comprising multiple ultrafiltration steps
• CPC Class Codes: B01D 63/08 Flat membrane modules
• CPC Class Codes: B01D 65/02 Membrane cleaning or sterilisation ; Membrane regeneration
• CPC Class Codes: B01D 65/08 Prevention of membrane fouling or of concentration polarisation
• CPC Class Codes: G01N 1/4077 by other techniques involving separation of suspended solids
• CPC Class Codes: Y10T 436/25375 Liberation or purification of sample or separation of material from a sample [e.g., filtering, centrifuging, etc.]

Abstract

A continuous filtration system for supplying an uninterrupted supply of filtrate from a solids-containing industrial process suitable for use by on-line automatic analyzers is provided. The continuous filtration system, which is particularly useful for filtering flue gas desulfurization process slurry to produce a solids-free filtrate for autoanalysis, includes a pair of filters connected in series which concurrently receive a tangential flow of slurry into the filter head that is discharged perpendicularly through a filtrate head. An automatic flushing system is provided to keep the filter membranes free of solid particles. An optional autoanalyzer for unfiltered slurry may also be included in the system.

Claims

1. A continuous filtration system for producing an uninterrupted supply of a solids-free filtrate from a solids-containing industrial process slurry for the automatic on-line analysis of components of the filtrate by an automatic analyzer system, wherein said continuous filtration system comprises:

(a) a supply of a solids-containing slurry to be filtered;

(b) a pair of filter elements fluidically connected together in series and selectively fluidically connected and disconnected to the supply of slurry and fluidically connected to a source of water;

(c) a filtrate outlet connected to the filter elements and selectively fluidically connected and disconnected to an automatic analyzer system for analysis of said filtrate;

(d) a control system controllable to automatically and selectively disconnect the filter elements from the slurry supply and the automatic analyzer system and to direct water from the water source through said filter elements from the filtrate outlet toward the slurry supply and then from the water source through the filter elements toward the filtrate outlet in response to a predetermined signal corresponding to the performance of a predetermined number of analyses performed in the analyzer system and then to automatically m-connect the filter elements to the slurry supply and the filtrate outer to the analyzer system; and

(e) a drain fluidically connected to the automatic analyzer system and the water source to direct excess fluids away from the filter elements and the analyzer system.

2. The continuous filtration system described in claim 1, wherein each of said pair of filter elements includes:

(a) a housing supporting a slurry head spaced toward the slurry supply from a filtrate head;

(b) a planar filter membrane positioned between the slurry head and the filtrate head;

(c) a slurry inlet in the slurry head oriented to direct a flow of slurry into the filter element tangential to the filter membrane; and

(d) a filter outlet in the filtrate head oriented to direct a flow of filtrate out of the filter element perpendicular to the filter membrane and into a plurality of filtrate collection channels.

3. The continuous filtration system described in claim 2, wherein said control system includes:

(a) an autoflush control system electronically connected to a circuit box connected to said automatic analyzer system, said autoflush control system being connected to said slurry supply and to said water source;

(b) a plurality of valves located in the fluid connections between said slurry supply, said water source, said filtrate outlet and said analyzer system, wherein said valves are actuatable by said autoflush control system to selectively direct fluid flow in response to said predetermined signal after said predetermined number of analyses have been performed; and

(c) a data acquisition system input/output link electronically connected to said autoflush control system.

4. The continuous filtration system described in claim 3, wherein said system further includes an automatic flushing system to remove solid particles from said filter membranes, said automatic flushing system comprising an autoflush controller electronically connected to said autoflush control system, to said data acquisition system input/output link and to said plurality of valves, said source of water, and said filtrate outlet, wherein said autoflush controller receives said predetermined signal and actuates said valves to prevent slurry flow through said filter elements and to cause water from said source of water to flow into said filter elements through said filtrate outlet and out said slurry inlets and then through said slurry inlets and out said filtrate outlet to said drain.

5. The continuous filtration system described in claim 4, further including an automatic analysis system fluidically connected directly to said slurry supply and fluidically connected to a slurry outlet.

6. The continuous filtration system described in claim 2, wherein said slurry heads have a substantially rectangular configuration and are formed of polypropylene.

7. The continuous filtration system described in claim 2, wherein said filtrate heads have a substantially circular configuration and are formed of an acrylic plastic.

8. The continuous filtration system described in claim 7, wherein said filtrate heads include a plurality of concentric channels and collection vanes integrally formed in said filtrate heads and spaced outwardly from respective filter outlets.

9. The continuous filtration system described in claim 1, wherein said industrial process is a wet lime or limestone slurry flue gas desulfurization process.

10. A continuous filtration system for producing an uninterrupted supply of a solids-free filtrate from a wet lime or limestone slurry flue gas desulfurization process slurry for the on-line automatic analysis of selected process indicators of tho flue gas desulfurization process, said continuous filtration system comprising:

(a) a source of flue gas desulfurization process slurry to be analyzed;

(b) a pair of filter elements fluidically connected together in series and fluidically connected to the source of slurry wherein each of said filter elements includes;

(i) a housing supporting a slurry head spaced toward the slurry source from a filtrate head;

(ii) a planar filter membrane positioned between the slurry head and the filtrate head;

(iii) a slurry inlet head oriented to direct a flow of slurry into the filter element tangential to the filter membrane; and

(iv) a filtrate outlet in the filtrate head oriented to direct a flow of filtrate out of the filter clement perpendicular to the filter membrane fluidically connected to an automatic analyzer system;

(c) a source of water fluidically connected to the filter elements;

(d) a control system controllable to automatically and selectively fluidically isolate the falter elements from the slurry source, the water source and the automatic analyzer system and to direct water from the water source through said filter elements from the filtrate outlets to the slurry source and then from the water source through the filter elements toward the filtrate outlets in response to a predetermined signal corresponding to a selected number of analyses having been performed by the automatic analyzer system; and

(e) a drain fluidically connected to the automatic analyzer system and the water source to direct excess fluids away from the filter elements and the automatic analyzer system.

11. The continuous filtration system described in claim 10, wherein said control system includes:

(a) an autoflush control system electronically connected to said automatic analyzer system, to said slurry source and to said water source;

(b) a plurality of valves located in the fluid connections between said slurry source, said water source, said filtrate outlets and said analyzer system, wherein said valves are actuatable by said autoflush control system to selectively direct fluid flow in response to said predetermined signal; and

(c) a data acquisition system input/output link electronically connected to said autoflush control system.

12. The continuous filtration system described in claim 11, wherein said system further includes an automatic flushing system to remove solid particles from said filter membranes, said automatic flushing system comprising:

(a) an autoflush controller electronically connected to said autoflush control system, to said data acquisition system input/output link and to said plurality of valves;

(b) said source of water; and

(c) said filtrate outlets, wherein said autoflush controller receives said predetermined signal and actuates said valves to prevent slurry flow through said filter elements and to cause water from said source of water to flow into said filter elements through said filtrate outlets and out said slurry inlets and through said slurry inlets and out said filtrate outlets to said drain.

13. The continuous filtration system described in claim 12, further including an automatic analysis system fluidically connected directly to said slurry source and fluidically connected to a slurry outlet.

14. The continuous filtration system described in claim 10, wherein said slurry heads have a substantially rectangular configuration and are formed of polypropylene.

15. The continuous filtration system described in claim 10, wherein said filtrate heads have a substantially circular configuration and are formed of an acrylic plastic.

16. The continuous filtration system described in claim 15, wherein said filtrate heads include a plurality of concentric channels and collection vanes integrally formed in said filtrate heads and spaced outwardly from respective filtrate outlets.

17. A method for automatically producing a supply of slurry filtrate from a wet lime or limestone slurry flue gas desulfurization process for the analysis of selected flue gas desulfurization process indicators including the steps of:

(a) concurrently directing a flow of flue gas desulfurization process slurry tangentially through a pair of filter membranes connected in series to produce a slurry filtrate;

(b) directing the slurry filtrate to at least one automatic analyzer, analyzing the filtrate as required and obtaining signals corresponding to numbers of analyses performed, and transmitting said signals to an autoflush control system;

(c) when a predetermined number of signals corresponding to a selected number of analyses performed on the slurry filtrate have been transmitted to said autoflush control system, selectively actuating a plurality of valves to prevent slurry flow through said filter membranes and to cause service water to flow perpendicularly through said membranes in a direction opposite the slurry flow during step (a);

(d) permitting the service water to flow through said membranes for a predetermined time and then deactuating said valves to cause slurry flow through said filter membranes to produce slurry filtrate for analysis by said at least one automatic analyzer; and

(e) repeating steps (a) through (d) as necessary to obtain required information from the analysis.

18. The method described in claim 17, wherein said method further includes the steps of concurrently directing a flow of unfiltered flue gas desulfurization process slurry to an automatic analyzer, conducting a selected analysis on said unfiltered slurry, transmitting signals corresponding to the data obtained to an autoflush control system, and directing the used unfiltered slurry to a slurry outlet.