Film testing

• US 5,517,860 A
• Filed: 02/03/1995
• Issued: 05/21/1996
• Est. Priority Date: 02/03/1995
• Status: Expired due to Term

• Current Assignee: Axalta Coating Systems Ip Co Llc (Axalta Coating Systems Ltd.)
• Original Assignee: E. I. du Pont de Nemours and Company (Corteva, Inc.)
• Inventors: Lin, Li, Johnson, Melvin H.
• Primary Examiner(s): Chilcot, Richard
• Assistant Examiner(s): NOORI, MAX H
• Application Number:
  US08/382,815
• Time in Patent Office: 473 Days
• Field of Search: 73/7, 73/78, 73/789, 73/790, 73/791, 73/795
• US Class Current: 73/789
• CPC Class Codes: G01B 7/16 for measuring the deformation in a solid, e.g. by resistance strain gauge
• CPC Class Codes: G01L 5/0038 applying a pushing force
• CPC Class Codes: G01N 2203/0278 Thin specimens
• CPC Class Codes: G01N 2203/0282 Two dimensional, e.g. tapes, webs, sheets, strips, disks or membranes
• CPC Class Codes: G01N 3/08 by applying steady tensile or compressive forces G01N3/28 takes precedence
• CPC Class Codes: G01N 3/20 by applying steady bending forces G01N3/26, G01N3/28 take precedence

Abstract

Measurement of stress-strain relationships in thin films using substantially flat, parallel test surfaces with minimal width.

Claims

1. In a testing apparatus comprising means for determining the stress-strain relationship in a film of polymeric material to produce an electronic signal, and means for converting the electronic signal to visual or graphic form, the improvement wherein the means for determining the stress-strain relationship comprises:

(a) first and second substantially flat test surfaces between which the film is placed for testing, the flat test surfaces each having a substantially linear configuration and in substantially complete alignment and wherein the width of each test surface is at least equal to the thickness of the film and no greater than twice the thickness of the film;

(b) means for positioning the test surfaces substantially parallel to each other; and

(c) means for moving one of the test surfaces with respect to the second test surface;

wherein the means for positioning at least one of the test surfaces is a double cantelever structure onto which one test surface is attached.

2. An apparatus of claim 1 wherein each test surface has a surface variation of less than about 30 nm.

3. An apparatus of claim 2 wherein each of the test surfaces comprises a single crystal.

4. An apparatus of claim 3 wherein at least one of the test surfaces consists essentially of silicon.

5. In a method for determining the stress-strain relationship in a film of polymeric material to produce at least one electronic signal reflecting the resistance of a sample to compressive deformation, and converting the electronic signal to visual or graphic form, the improvement wherein the stress-strain relationship comprises:

(a) placing the film between first and second substantially flat test surfaces for testing, the flat test surfaces each having a substantially linear configuration and wherein the width of each test surface is at least equal to the thickness of the film and no greater than twice the thickness of the film;

(b) positioning the test surfaces substantially parallel to each other; and

(c) moving one of the test surfaces toward second test surface to compress the film; and

(d) measuring the force required to compress the film

wherein the test surfaces are positioned substantially parallel by means of a double cantelever structure onto which one test surface is attached.

6. A method of claim 5 wherein each test surface has a surface variation of less than about 30 nm.