Method and apparatus for inspecting liquid-filled containers

• US 5,523,560 A
• Filed: 12/07/1994
• Issued: 06/04/1996
• Est. Priority Date: 02/01/1991
• Status: Expired due to Term

• Current Assignee: Novo Nordisk A/S
• Original Assignee: Novo Nordisk A/S
• Inventors: Martinussen, Tommy, Nielsen, Gert, Manique, Flemming
• Primary Examiner(s): ALLEN, STEPHONE B
• Application Number:
  US08/350,757
• Time in Patent Office: 545 Days
• Field of Search: 250/223 B, 250/227.11, 250/573, 250/576, 356/341, 356/342, 356/344, 356/237, 356/239, 356/240, 356/427, 356/343, 209/526, 209/577
• US Class Current: 250/223.00B
• CPC Class Codes: G01N 2033/0081 containers; packages; bottles
• CPC Class Codes: G01N 21/9027 in containers after filling

Abstract

The present invention relates to a method and apparatus for inspecting entities comprising liquid-filled containers for one or more test parameters of the liquid, the container, or both, by rotating and axially line scanning said entities and comparing said scans electronically, after which entities exhibiting one or more unacceptable test parameters are identified and separated from entities exhibiting acceptable test parameters.

Claims

1. A method for inspecting an entity comprising a liquid-filled container for one or more test parameters of the liquid, the container, or both, wherein the entity is irradiated by irradiating means, rotated and axially line scanned along a line parallel with the axis of rotation by detecting means detecting radiation reflected, diffracted, or scattered from the entity, the inspection comprising at least one sequence of:

a) rotating the entity according to a predetermined rate profile having one or more periods of constant angular velocities, line scanning the container axially during the periods of constant angular velocities, and comparing pixel values of said line scans with set references; and

b) rotating the entity according to a predetermined rate profile comprising rates of rotation causing the liquid to circulate and foreign bodies having densities higher than the liquid to accumulate at the container wall, bringing the container to a standstill with the liquid rotating, line scanning the entity axially before the rotation of the liquid is substantially reduced, digitally filtering the pixel values of said line scans, and comparing the filtered values with predetermined references.

2. A method according to claim 1, wherein the periods of constant angular velocity generally occur at rotation rates below 2000 rpm.

3. A method according to claim 2, wherein the constant angular velocity is about 1200 rpm.

4. A method according to claim 1, wherein the detection of foreign bodies in the liquid having densities larger than that of the liquid is performed while the liquid is rotating at a rate from about 10000 rpm to about 2000 rpm.

5. A method according to claim 4, wherein the liquid is rotating at a rate about 8000 rpm.

6. A method according to claim 1, wherein the total inspection time including the scanning, is less that 1000 ms.

7. A method according to claim 5, wherein the total inspection times, including the scanning, is about 250 ms.

8. A method according to claim 1, wherein said entity is irradiating with electromagnetic radiation and the transmitted, reflected, diffracted or scattered radiation is detected at an angle from about 90 to about 180 degrees relative to the incident radiation taken about the axis of rotation.

9. A method according to claim 8, wherein the transmitted, reflected, diffracted or scattered radiation is detected at an angle of 120°

relative to the incident radiation taken about the axis of rotation.

10. A method according to claim 1, wherein the entity is irradiated with electromagnetic radiation, and the radiation reflected, diffracted or scattered into the direction opposite the incident radiation is detected as retroreflected radiation.

11. A method according to claim 10, wherein said retro-reflected radiation is reflected out of the incidentdirection by means of a semi-transparent and reflecting mirror.

12. A method according to claim 8, wherein said transmitted, reflected, diffracted or scattered radiation is detected by a linear array of radiation detectors and stored digitally, preferably in a frame store memory and a matrix filter.

13. A method according to claim 1, wherein one or more test parameters of the liquid is selected from the group consisting of:

type of liquid, including clear solution, emulsion, and suspension;

liquid specification, including amount and intended content, concentration of components, color, transmittance, and mixer ball; and

foreign matter, including foreign liquids and bodies, suspended particles, impurities and undesired flocculation, growth of crystals and biological organisms.

14. A method according to claim 1, wherein one or more test parameters of the container is selected from a group consisting of:

container specification, including shape, bottom cap, labels, bar code, plunger fill level, color and transmittance;

container defects, including flaws, cracks, air bubbles and particles entrapped in the container wall, and weakenings; and

container contamination, including dirt and dust, material entrapped between the plunger and container wall.

15. A method according to claim 1, wherein an inspected entity exhibiting one or more unacceptable test parameters of the liquid, the container, or both, is identified and separated from containers exhibiting acceptable test parameters.

16. An apparatus for inspecting an entity comprising liquid-filled container for one or more test parameters of the liquid, the container (10), or both, by rotating, irradiating, and axially line scanning said entity and comparing said scans electronically, comprising rotating means (705) for rotating the entity according to a predetermined rate profile having one or more periods of constant angular velocities, and for rotating the entity to another predetermined rate profile comprising rates of rotation causing the liquid to circulate and foreign bodies having densities deities higher than the liquid to accumulate at the container wall and of bringing the container to a standstill, irradiating means (611-614), detection means (631-632), and electronic digital filtering comparison means (708-726).

17. An apparatus according to claim 16, wherein said rotation means (705) comprises a programmable stepper motor, preferably a low inertia stepper motor, programmed to provide a predefined rate profile over the total time of inspection and to stop the rotation generally in less than 500 ms, preferably in less than 100 ms, particularly in the range 20-80 ms.

18. An apparatus according to claim 16, wherein said irradiating means (611-614) comprises:

a) a dc-powered light source (611), or a synchronized stroboscopic light source, preferably a stabilized tungsten light source;

b) an IR-filter (612) removing radiation having a wavelength longer than approximately 1000 nm; and

c) fiber optical light guides (613), preferably glass fibers, arranged in a long narrow line (614) of width approximately 1.0 mm and of a length corresponding to the full axial length of the container.

19. An apparatus according to claim 16, wherein said detection means (631-632) comprises an optical lens (631) imaging the transmitted or scattered radiation, from preferably a narrow, e.g. 50 μ

m wide, vertical line segment of the container, onto a linear array (632) of imaging photo detectors containing anywhere from 32 to 10000 elements.

20. An apparatus according to claim 19, wherein the linear array of imaging photo detectors is a linear CCD- or PCCD-array having 1024 pixels of 14×

14 μ

m.

21. An apparatus according to claim 20, wherein said detection means further comprises means line scanning the pixels of the CCD- or PCCD-array serially.

22. An apparatus according to claim 20, wherein each pixel is accessed every 200 μ

s.

23. An apparatus according to claim 20, wherein said detection means further comprises means for transforming analog pixel values to digital values.

24. An apparatus according to claim 16, wherein said electronic digital comparison means comprises a digital matrix filter and/or a frame store memory.

25. An apparatus according to claim 16, further comprising means of identifying and means of separating containers having one or more unacceptable test parameters of the liquid, the container, or both, from containers having acceptable test parameters.