Automated work station for analyzing soil samples

• US 5,526,705 A
• Filed: 08/05/1994
• Issued: 06/18/1996
• Est. Priority Date: 08/05/1994
• Status: Expired due to Term

• Current Assignee: Blue Leaf IP Incorporated (CNH Industrial N.V.), CNH Industrial America LLC (CNH Industrial N.V.)
• Original Assignee: Tyler Limited Partnership
• Inventors: Bobrov, Vladimier A., Skotnikov, Andrey V.
• Primary Examiner(s): Williams, Hezron E.
• Assistant Examiner(s): LARKIN, DANIEL SEAN
• Application Number:
  US08/286,768
• Time in Patent Office: 683 Days
• Field of Search: 73/863, 73/863.21, 73/863.23, 73/866, 204/400, 422/62, 422/68.1, 422/82.03, 422/82.09, 422/119, 436/31, 436/145, 436/177, 436/178
• US Class Current: 73/863
• CPC Class Codes: G01N 33/24 Earth materials G01N33/42 takes precedence
• CPC Class Codes: G01N 35/02 using a plurality of sample containers moved by a conveyor system past one or more treatment or analysis stations G01N35/0098 and G01N35/0099 take precedence
• CPC Class Codes: Y10T 436/23 Carbon containing
• CPC Class Codes: Y10T 436/25375 Liberation or purification of sample or separation of material from a sample [e.g., filtering, centrifuging, etc.]

Abstract

An apparatus analyzes a plurality of soil samples to determine characteristics of the soil samples. An input portion sequentially provides a plurality of soil samples each having a known solid content. A plurality of vessels are supported for movement with a continuous conveyor relative to the input portion to receive the soil samples. A plurality of testing stations are arranged relative to the continuous conveyor to sequentially access the samples carried by the vessels. The testing stations each test the samples to determine at least one of the characteristics of the samples.

Claims

1. An apparatus for analyzing a plurality of soil samples to determine characteristics of the soil samples, the apparatus comprising:

a sample input section sequentially providing a plurality of soil samples each having a known solid content;

a continuous conveyor;

a plurality of vessels supported for movement with the continuous conveyor relative to the sample input section to receive the soil samples; and

a plurality of testing stations arranged relative to the continuous conveyor to sequentially access the samples carried by the vessels, the testing stations each testing the samples to determine at least one of the characteristics of the samples.

2. The apparatus of claim 1 and further comprising:

a controller operably coupled to the testing stations for determining and processing nutrient information based on the characteristics determined by the test stations.

3. The apparatus of claim 2 wherein the controller periodically calibrates the test stations.

4. The apparatus of claim 2 wherein the sample input section comprises:

an input vessel for receiving soil;

water delivery means for delivering water to the input vessel; and

a mixer coupled relative to the vessel to mix the water and soil to form a slurry.

5. The apparatus of claim 4 wherein the sample input section further comprises:

a doser, coupled to the input vessel, for removing a slurry sample comprising at least a portion of the slurry from the input vessel; and

dry content determining means, coupled to the doser, for receiving the slurry sample from the doser and determining a dry content of the slurry sample.

6. The apparatus of claim 5 wherein the dry content determining means comprises:

a humidity meter for measuring humidity of the slurry sample;

a scale for measuring a weight of the slurry sample; and

wherein the controller is coupled to the humidity meter and the scale and wherein the controller determines a weight of the dry content of the slurry sample.

7. The apparatus of claim 5 wherein the sample input section further comprises:

a filter coupled between the doser and the dry content determining means for filtering the slurry sample before the slurry sample enters the dry content determining means.

8. The apparatus of claim 1 wherein the sample input section comprises:

an opener for receiving sealed packages containing soil and for opening the packages, the input vessel receiving the soil from the opener.

9. The apparatus of claim 1 wherein the testing stations comprise:

a first plurality of test stations, each for determining a nutrient of the soil samples; and

a second plurality of test stations, each for determining a physical characteristic of the soil samples.

10. The apparatus of claim 1 further comprising:

washing means arranged relative to the continuous conveyor for washing the vessels after a last of the testing stations has accessed the sample contained in the vessel.

11. The apparatus of claim 2 wherein the controller determines nutrients to be applied to a field represented by the soil sample.

12. A method of analyzing a plurality of soil samples to determine characteristics of the soil samples, comprising:

receiving a first soil sample;

mixing the soil sample with a liquid to form a slurry;

providing the slurry to a vessel supported for movement with a continuous conveyor;

controlling the continuous conveyor to sequentially move the vessel to a plurality of test stations;

determining a characteristic at each test station; and

repeating the steps of receiving, mixing, providing, controlling and determining for a subsequent soil sample so that a plurality of soil samples are at test stations simultaneously.

13. The method of claim 12 and further comprising, after the step of mixing, determining a dry content of the slurry.

14. The method of claim 13 wherein determining a dry content of the slurry comprises:

determining a humidity of the slurry a plurality of times to obtain a plurality of humidity values;

obtaining a final humidity value based on the plurality of humidity values; and

using the final humidity value in obtaining the dry content of the slurry.

15. The method of claim 14 wherein the humidity is determined by taking measurements with a humidity meter and wherein the method comprises:

rinsing the humidity meter between measurements of slurries formed with different soil samples.

16. The method of claim 12 wherein determining a characteristic comprises:

agitating the slurry;

measuring sedimentation in the slurry by measuring light transmission characteristics of the slurry; and

determining particle size of particles in the slurry based on the light transmission characteristics.

17. An apparatus for analyzing a plurality of soil samples to determine characteristics of the soil samples, the apparatus comprising:

a sample input section providing a plurality of soil samples each having a known solid content;

a conveyor;

a plurality of vessels supported for movement with the conveyor relative to the sample input section to receive the soil samples;

a plurality of accessing members arranged relative to the conveyor to sequentially access the samples carried by the vessels, the accessing members each accessing the samples so the samples can be tested to determine at least one of the characteristics of the samples; and

wherein the plurality of vessels and the plurality of accessing members are movable relative to one another so that the plurality of vessels are advancable with the conveyor without interfering with the plurality of accessing members.

18. The apparatus of claim 17 further comprising:

a movable support member coupled to the plurality of accessing members moving the plurality of accessing members out of interference with the plurality of vessels so the plurality of vessels can be advanced by the conveyor.

19. The apparatus of claim 17 further comprising:

a second set of accessing members arranged relative to the conveyor and to the plurality of accessing members so that any of the plurality of accessing members are replaceable by corresponding ones of the second set of accessing members to sequentially access the samples carried by the vessels when any of the plurality of accessing members malfunctions.

20. An apparatus for analyzing a plurality of soil samples to determine characteristics of the soil samples, the apparatus comprising:

a sample input section sequentially providing a plurality of soil samples each having a known solid content;

a conveyor;

a plurality of vessels supported for movement with the conveyor relative to the sample input section to receive the soil samples; and

a plurality of testing stations arranged relative to the conveyor to sequentially access the samples carried by the vessels, the testing stations each testing the samples to determine at least one of the characteristics of the samples, the testing stations comprising;

a carbon content analyzer including an acid introducer introducing an acid into a vessel containing the soil sample, a gas collector collecting gas produced by the acid and soil sample;

volume determining means for determining a volume of the gas produced; and

means for determining carbon content based on the volume of gas produced.

21. The apparatus of claim 20 wherein the gas collector comprises:

a container coupled to the vessel containing the soil sample and the acid and being filled to a reference level with liquid;

a reservoir providing the liquid to the container such that when gas enters the container from the vessel, the gas forces at least a portion of the liquid back into the reservoir; and

wherein the volume determining means determines the volume of the gas collected based on an amount the fluid has dropped from the reference level.

22. The apparatus of claim 21 wherein the volume determining means comprises:

a pump for pumping liquid back into the container to the reference level; and

means for determining a volume of the liquid pumped back into the container to return the liquid to the reference level to obtain the volume of gas collected.

23. The apparatus of claim 22 wherein the acid comprises hydrochloric acid and wherein the gas comprises carbonic acid gas.

24. The apparatus of claim 22 wherein the volume determining means comprises:

a liquid sensitive electrode arranged relative to the container to provide a signal indicating when the liquid is at the reference level.

25. An apparatus for analyzing a plurality of soil samples to determine characteristics of the soil samples, the apparatus comprising:

a sample input section sequentially providing a plurality of soil samples each being mixed into a soil slurry having a known solid content;

a conveyor;

a plurality of vessels supported for movement with the conveyor relative to the sample input section to receive the soil samples;

a plurality of testing stations arranged relative to the conveyor to sequentially access the samples carried by the vessels, the testing stations each testing the samples to determine at least one of the characteristics of the samples, the testing stations comprising;

a nutrient analyzer including at least one ion-selective electrode, and means for removing a portion of an extraction from the slurry in a vessel and generating an extraction flow, the ion-selective electrode being positioned in the flow and generating a signal indicative of a nutrient in the flow.

26. The apparatus of claim 25 wherein the nutrient analyzer comprises:

a plurality of ion-selective electrodes positioned in the flow to provide a plurality of signals indicative of a plurality of nutrients in the flow.

27. The apparatus of claim 25 wherein the means for removing a portion of the extraction from the slurry comprises:

a selectively pressurized conduit coupled to the vessel; and

a ceramic filter filtering the slurry removed from the vessel.

28. The apparatus of claim 27 and further comprising:

means for providing a back pressure across the ceramic filter to clean the filter between soil samples.

29. The apparatus of claim 25 wherein the ion-selective electrode provides a signal indicative of at least one of the group consisting of NO3, NH4, K, P, Ca, Mg.

30. The apparatus of claim 26 and further comprising means for determining the nutrients based on interference effects of the nutrients indicated by the signals provided by the plurality of ion-selective electrodes.

31. The apparatus of claim 25 and further comprising:

means for evaporating a portion of the extraction; and

means for increasing ion concentration in the extraction by adding a buffer.

32. The apparatus of claim 31 wherein the buffer comprises:

an MES buffer having a pH of approximately 6.15.