Injection septum with dust wiper

• US 5,531,810 A
• Filed: 09/21/1994
• Issued: 07/02/1996
• Est. Priority Date: 09/21/1994
• Status: Expired due to Fees

• Current Assignee: Merlin Instrument Company
• Original Assignee: Merlin Instrument Company
• Inventors: Fullemann, James S.
• Primary Examiner(s): SPITZER, ROBERT H
• Application Number:
  US08/310,276
• Time in Patent Office: 650 Days
• Field of Search: 96/101-107, 210/198.2, 215/247, 215/292, 215/307, 215/310
• US Class Current: 96/105
• CPC Class Codes: G01N 30/18 using a septum or microsyringe
• CPC Class Codes: G01N 35/1079 with means for piercing stoppers or septums

Abstract

A cap assembly for a gas chromatography injection port includes a two-piece septum. The two-piece septum includes a syringe seal for sealing an injection needle and a duckbill seal for sealing the injection port when the needle is not inserted. The syringe seal includes three annular ribs in its aperture. At the aperture base is a sealing rib that provides the main sealing function for the syringe seal. Just above the sealing rib is a stress-relief rib. At the top of the aperture is a wiping rib. The wiping rib wipes dust on the needle exterior so that it does not enter the aperture. Dust entering the aperture can be retained in the relatively large dust pocket between the wiping rib and the strain-relief rib. The septum is held in place by a septum nut that has a recess above the wiping rib for holding dust removed from the needle by the wiping rib. A washer in the recess prevents the syringe seal from deforming into the recess. The septum nut includes a guide aperture section that aligns the syringe needle with the apertures of the syringe seal and the duckbill seal. The septum nut is made of anodized aluminum to provide ready machinability for formation of the guide aperture section and sufficient hardness to resist damage inflicted by the syringe needle.

Claims

1. A septum assembly for permitting injection of a fluid by extension of a needle therethrough, said needle having a needle diameter, said septum comprising:

an elastic duckbill seal having a duckbill aperture with a duckbill perimeter, said perimeter being at least as great as said needle diameter, said duckbill seal contacting and generally conforming to the cross section of said needle when said needle extends completely through said duckbill aperture, said duckbill aperture closing when said needle is withdrawn therefrom;

an elastic syringe seal having a generally annular aperture of varying diameter, said syringe seal mating with said duckbill seal so that said annular aperture and said duckbill aperture are aligned, said syringe seal having

annular wipe, seal, and alignment elements, the diameters of said annular aperture at each of said elements being less than said needle diameter when said needle is not inserted therethrough, said wipe element being at an insertion end of said annular aperture, said seal element being at an opposite end of said aperture, said alignment element being between said wipe element and said seal element, said alignment element being closer to said seal element than to said wipe element, and

annular wipe and seal pockets, the diameters of said annular aperture at each of said pockets being greater than said needle diameter when said needle is inserted through said annular aperture, said wipe pocket being between said wipe element and said alignment element, said seal pocket being between said seal element and said alignment element.

2. A septum assembly as recited in claim 1 further comprising a septum nut, said septum nut having threads for mating with a gas chromatography injection port, said septum nut being configured to mate with the mated combination of said duckbill seal and said syringe seal, said septum nut having a guide aperture aligned with said annular aperture and said duckbill aperture, said guide aperture having a cylindrical section with an inner diameter between 100% and 130% of said needle diameter, the height of said cylindrical section being at least twice its diameter.

3. A septum assembly as recited in claim 2 wherein said septum nut is of anodized aluminum.

4. A septum assembly as recited in claim 2 wherein said septum nut and said syringe seal are co-shaped so as to define near said wipe element a cavity for gathering particles removed from said needle by said wipe element, the volume not occupied by said septum of said cavity when said needle is inserted being at least the cube of said needle diameter.

5. A septum assembly as recited in claim 2 further comprising a washer disposed between said septum nut and said syringe seal so as to prevent protrusion of said syringe seal into said volume.