Multiple solute standard preparation

• US 5,544,684 A
• Filed: 12/08/1994
• Issued: 08/13/1996
• Est. Priority Date: 12/08/1994
• Status: Expired due to Fees

• Current Assignee: The Dow Chemical Company (Dow, Inc.)
• Original Assignee: The Dow Chemical Company (Dow, Inc.)
• Inventors: Robinette, Rex T. III
• Primary Examiner(s): Recla, Henry J.
• Assistant Examiner(s): Douglas, Steven O.
• Application Number:
  US08/352,332
• Time in Patent Office: 614 Days
• Field of Search: 141/9, 141/83, 141/100, 141/104, 141/105, 177/25.14, 177/50, 177/116, 364/567, 364/579, 364/571.05, 364/479, 364/502, 137/98, 137/101.21, 137/101.31
• US Class Current: 141/83
• CPC Class Codes: G01G 17/06 having means for controlling the supply or discharge

Abstract

A method for the automated preparation of a standard solution containing at least two solutes wherein the user of the method adds the solutes to a container according to the respective target weights of the solutes. The ratio between the actual weight of the first solute added and the target weight of the first solute is used to update the target weight of the second solute so that the concentration of the second solute in the standard is closer to its desired concentration.

Claims

1. A method for the preparation of a standard solution containing at least a first solute and a second solute dissolved in a solvent, the solution containing an essentially desired concentration of the first solute and a substantially desired concentration of the second solute, comprising the steps of:

(a) weigh a container to determine the tare weight of the container;

(b) assign a target weight for the solvent;

(c) assign a target weight for the first solute;

(d) assign a target weight for the second solute;

(e) add the first solute to the container;

(f) weigh the container to determine the weight of the first solute added to the container;

(g) determine the ratio of the weight of the first solute added to the container to the target weight for the first solute;

(h) multiply the target weight for the second solute by the ratio of step (g) to obtain an updated target weight for the second solute;

(i) add the second solute to the container;

(j) weigh the container to determine the weight of the second solute added to the container; and

(k) add a weight of the solvent to the container, the weight of the solvent being essentially equal to the quantity of the weight of step (f) divided by the weight of step (c) which quantity is then multiplied by the weight of step (b).

2. The method of claim 1, wherein the weight of step (j) is in the range of from 0.75 to 1.25 of the weight of steep (h).

3. The method of claim 1, wherein the weight of step (j) is in the range of from 0.9 to 1.1 of the weight of step (h).

4. The method of claim 1 wherein the solvent contains an internal standard.

5. The method of claim 2 wherein the solvent contains an internal standard.

6. The method of claim 3 wherein the solvent contains an internal standard.