Method and apparatus for dry particle analysis

• US 5,579,107 A
• Filed: 05/25/1995
• Issued: 11/26/1996
• Est. Priority Date: 05/25/1995
• Status: Expired due to Fees

• Current Assignee: Horiba Instruments Incorporated (Horiba Limited)
• Original Assignee: Horiba Instruments Incorporated (Horiba Limited)
• Inventors: Wright, Craig, Torgerson, Curt
• Primary Examiner(s): Rosenberger, Richard A.
• Application Number:
  US08/451,023
• Time in Patent Office: 551 Days
• Field of Search: 356/335, 356/336, 356/338, 356/339, 356/438, 356/440, 73/865.5, 73/24.03.24.06, 73/864.81, 241/39
• US Class Current: 356/336
• CPC Class Codes: G01N 1/286 involving mechanical work, e.g. chopping, disintegrating, compacting, homogenising microtomes G01N1/06; pulverising in general B02C; mixing in general B01F
• CPC Class Codes: G01N 15/0205 by optical means
• CPC Class Codes: G01N 2001/2866 Grinding or homogeneising

Abstract

A dry particle analyzer includes a vibrating sieve cup drizzling particles downwardly with first, second, and third sheath air flows being provided to separate the particles from boundary walls and to form the drizzling particles into a columnated flow for optical analysis. The particles drop vertically as a drizzle with gravitational assistance from a bulk sample to an analysis chamber. Along the way to the analysis chamber, the particles are subjected to an interval of high air flow shear, and to high turbulence of the air flow to break up agglomerations of particles.

Claims

1. A dry particle analyzer comprising:

means for drizzling particles from a bulk sample thereof, means for providing a downward flow of first sheath ambient air around said drizzling particles in a flow regime of laminar bulk flow with a surrounding viscous boundary layer, means for suddenly changing the flow regime of said drizzling particles and first sheath air to a flow regime with a surrounding second sheath of high velocity air causing high shear and acceleration of said drizzling particles and first sheath air flow and with admixture of said second sheath air, means for columnating and decelerating said particles and said admixture of first sheath air and second sheath air, means for providing a downward and columnar flow of third sheath ambient air around said columnated drizzled particles and first and second air flows admixed together and substantially in velocity union therewith, and means defining a vertically downwardly extending optical analysis cell passage receiving the unified downward flow of drizzled particles and admixed first and second sheath air surrounded by said third sheath air for columnated downward flow therein, whereby the drizzled particles flow downwardly continuously from said bulk sample and through said analysis cell passage.

2. The dry particle analyzer of claim 1 wherein said means for providing a downward flow of first sheath ambient air around said drizzling particles in a flow regime of laminar bulk flow with a surrounding viscous boundary layer includes a sieve cup providing a downward gravitational drizzle of particles in response to agitation thereof, and a conduit receiving said downward gravitational drizzle of the particles along with a surrounding flow of ambient air as said first sheath air flow.

3. The dry particle analyzer of claim 2 further including means for creating a sub-ambient pressure within said conduit to induce said surrounding flow of ambient air into said conduit in surrounding relationship with said drizzle of particles.

4. The dry particle analyzer of claim 3 wherein said means for creating a sub-ambient pressure includes a vacuum source communicating with said conduit.

5. The dry particle analyzer of claim 3 wherein said means for creating a sub-ambient pressure includes an aspirator receiving pressurized air and ejecting this pressurized air in a direction along the length of said conduit to provide said sub-ambient pressure therein.

6. The dry particle analyzer of claim 2 further including means for agitating said sieve cup, said means for agitating said sieve cup imposing a vertical orbital oscillation on said sieve cup.

7. The dry particle analyzer of claim 1 wherein said means for suddenly changing the flow regime of said drizzling particles and first sheath air to a flow regime with a surrounding second sheath of high velocity air causing high shear and acceleration of said drizzling particles and first sheath air flow and with admixture of said second sheath air includes an aspirator receiving pressurized air and providing an opening through which said drizzling particles and first sheath air is received, said aspirator defining an annular radial gap in surrounding relationship with said opening and said drizzling particles and first sheath air flow and from which said pressurized air is discharged axially along a length of said conduit.

8. The dry particle analyzer of claim 1 wherein said means for columnating and decelerating said particles and said admixture of first sheath air and second sheath air includes a divergent nozzle member receiving said drizzle of particles and first sheath air flow along with said high velocity air of said second sheath air flow, said divergent nozzle member diffusing said first and second air flows to a lower velocity and discharging said drizzled particles and said first and second air flows columnated into said downwardly extending optical analysis cell passage.

9. The dry particle analyzer of claim 8 wherein said divergent nozzle member defines an outlet which is of substantially rectangular shape in cross section, said nozzle member outlet having a major dimension which is perpendicular to an optical interrogation axis through said optical analysis cell passage, and discharging said drizzled particles and said first and second air flows together in a curtain of generally rectangular shape across said optical interrogation axis.

10. The dry particle analyzer of claim 8 wherein said divergent nozzle member further defines a step-wise discontinuity in the surface profile presented for bounding said high velocity said second sheath air flow, thereby to provide additional turbulence in said drizzle of particles and first sheath air flow along with said high velocity air of said second sheath air flow upon said nozzle member receiving said air flows.

11. The dry particle analyzer of claim 1 wherein said means for providing a downward and columnar flow of third sheath ambient air around said columnated drizzled particles and first and second air flows admixed together and substantially in velocity union therewith includes a flow guide member surrounding said columnated drizzled particles and first and second air flows admixed together and separated therefrom, said flow guide member including an opening receiving ambient air, and downwardly opening to said optical analysis cell passage.

12. The dry particle analyzer of claim 1 wherein said means defining a vertically downwardly extending optical analysis cell passage receiving the unified downward flow of drizzled particles and admixed first and second sheath air surrounded by said third sheath air for columnated downward flow therein includes a base member defining a generally J-shaped passage, said J-shaped passage having a descending leg which in an upper portion there of defines said optical analysis cell passage.

13. The dry particle analyzer of claim 12 wherein said J-shaped passage includes a convergent-divergent venturi nozzle shape.

14. The dry particle analyzer of claim 13 wherein said J-shaped passage further includes a divergent pressure-recovery section leading to an exit port.

15. The dry particle analyzer of claim 12 including said base member defining therein said analysis cell passage and said carrying opposed transparent windows bounding said analysis cell passage and providing for optical interrogation of said drizzled particles.

16. A dry particle analyzer apparatus comprising:

means for providing a cloud of drizzled particles gravitationally descending in a relatively low-velocity laminar bulk flow of surrounding ambient first sheath air with a surrounding low-velocity viscous boundary layer, and a de-agglomerator for affecting attrition of agglomerations of said particulates, said de-agglomerator including;

a Coanda type aspirator defining an opening through which said bulk flow of drizzled particles and first sheath ambient air is received, said aspirator receiving pressurized air and defining an annular radial gap surrounding said opening and from which a high-velocity second sheath air flow is discharged axially of said opening, thereby to apply a sudden high air flow shear to said particles and first sheath air flow.

17. The dry particle analyzer of claim 16 wherein said de-agglomerator further includes a step-wise boundary surface profile change spaced downstream of said annular radial gap with respect to said second sheath air flow, said second sheath air flow traversing said step-wise boundary surface change to impose additional turbulence on said drizzled particles and first sheath air flow.

18. The dry particle analyzer of claim 17 wherein said de-agglomerator further includes a divergent nozzle member receiving said drizzled particles and first sheath air flow along with said second sheath air flow subsequent to said step-wise boundary surface change.

19. The dry particle analyzer of claim 18 wherein said divergent nozzle member defines corners providing said step-wise boundary surface profile change.

20. The dry particle analyzer of claim 18 wherein said divergent nozzle member defines an inlet opening, and a plurality of corners circumscribing said inlet opening to provide a like plurality of step-wise boundary surface profile changes, one profile change at each corner.

21. A method of de-agglomerating particles for optical dry particle analysis, said method comprising steps of:

drizzling particles from a bulk sample thereof;

providing a downward flow of first sheath ambient air around said drizzling particles in a flow regime of laminar bulk flow with a surrounding viscous boundary layer;

suddenly changing the flow regime of said drizzling particles and first sheath air to a flow regime with a surrounding second sheath of high velocity air;

using said second sheath of high velocity air to cause high shear and acceleration of said drizzling particles and first sheath air flow;

effecting admixture of said second sheath air with said first sheath air;

columnating and decelerating said particles and said admixture of first sheath air and second sheath air;

providing a downward and columnar flow of third sheath ambient air around said columnated drizzled particles and admixed first and second sheath air flows and substantially in velocity union therewith; and

receiving the unified downward flow of drizzled particles and admixed first and second sheath air surrounded by said third sheath air into a vertically downwardly extending optical analysis cell passage for columnated downward flow therein.

22. The method of claim 21 further including the step of imparting high turbulence to said drizzled flow of particles and first and second sheath air flows before decelerating said admixed first and second sheath air flows.