Reconstituted tobacco material and method of its production

• US 5,584,306 A
• Filed: 11/09/1994
• Issued: 12/17/1996
• Est. Priority Date: 11/09/1994
• Status: Expired due to Term

• Current Assignee: Philip Morris Incorporated (Altria Group, Inc.), Philip Morris Products Inc (Philip Morris Limited)
• Original Assignee: Philip Morris Incorporated (Altria Group, Inc.), Philip Morris Products Inc (Philip Morris Limited)
• Inventors: Cowling, Patrick, Roope, Roy H., Beauman, Emory, Leister, Diane L.
• Primary Examiner(s): BAHR, JENNIFER DOYLE
• Application Number:
  US08/336,438
• Time in Patent Office: 769 Days
• Field of Search: 131/355, 131/370, 131/372, 131/374
• US Class Current: 131/370
• CPC Class Codes: A24B 15/14 made of tobacco and a binding agent not derived from tobacco
• CPC Class Codes: A24B 3/14 Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products delustering A24C1/40

Abstract

Reconstituted tobacco sheet having improved homogeneity and wet and dry tensile strength are produced by a process including mixing a water-soluble polysaccharide and a humectant under a first high shear; subjecting the resulting aqueous binder composition to a second high shear mixing operation; mixing the resulting aqueous binder composition with tobacco dust under a third shear, the third shear being lower than the first and second shears to form a slurry; casting the slurry onto a supportive surface such as a stainless steel conveyor belt; drying the cast slurry to form a reconstituted tobacco sheet; and recovering the reconstituted tobacco sheet for use such as cut filler for cigarettes.

Claims

1. A process of making a reconstituted tobacco material of constituents essentially limited to tobacco, a gum binder and a humectant, said process comprising the steps of:

(a) dispersing a binder in water under a first shear sufficient to form an aqueous binder dispersion, said binder consisting essentially of a gum;

(b) hydrating said aqueous binder dispersion of step (a) by subjecting the aqueous binder dispersion to a second shear so as to produce a hydrated binder solution;

(c) commingling tobacco particles with said hydrated binder solution of step (b) under a low shear so as to form a slurry, said low shear at a shear rate of less than 100 reciprocal seconds;

(d) casting the slurry; and

(e) drying the cast slurry to form a reconstituted tobacco material.

2. The process as claimed in claim 1, wherein said first and second shears are each at an average shear rate in the range of approximately 100 to 1000 reciprocal seconds, said second shear being at a greater average shear rate than said first shear.

3. The process as claimed in claim 2, wherein the first shear of step (a) is at an average shear rate in the range of approximately 100 to 500 reciprocal seconds.

4. The process as claimed in claim 3, wherein the first shear of step (a) is at an average shear rate in the range of approximately 100 to 300 reciprocal seconds.

5. The process as claimed in claim 4, wherein said second shear of step (b) is at an average shear rate in the range of approximately 600 to 800 reciprocal seconds.

6. The process as set forth in claim 5, wherein said binder comprises guar gum.

7. The process as claimed in claim 6, wherein the tobacco particles have a particle size of approximately 80 mesh or finer.

8. The process as claimed in claim 6, wherein the tobacco particles have a particle size of approximately 120 mesh or finer.

9. The process as claimed in claim 6 further comprising the step of adding a humectant at a level of 2 to 4 percent by weight of the reconstituted tobacco material.

10. A reconstituted tobacco material constructed by the process set forth in claim 6, said reconstituted tobacco material having a tensile strength greater than 20 and binder consisting essentially of guar.

11. The process as claimed in claim 5, wherein said commingling step is performed at an average shear rate in the range of approximately 20 to 50 reciprocal seconds.

12. The process as claimed in claim 3, wherein the first shear of step (a) achieves a viscosity in said dispersion in the range of approximately 2 to 6 poise.

13. The process as claimed in claim 12, wherein the second shear of step (b) achieves a viscosity in said binder solution in the range of approximately 20 to 60 poise.

14. The process as claimed in claim 3, wherein said second shear of step (b) is at an average shear rate in the range of approximately 500 to 1000 reciprocal seconds.

15. The process as claimed in claim 14, wherein said hydrating step (b) includes removing heat so that the temperature of the binder solution remains below 170°

F.

16. The process as set forth in claim 15, wherein temperature of the binder solution is maintained in the range of approximately 120°

to 140°

F.

17. The process as claimed in claim 14, wherein the tobacco particles have a particle size of approximately 80 mesh or finer.

18. The process as claimed in claim 14, wherein the tobacco particles have a particle size of approximately 120 mesh or finer.

19. The process as claimed in claim 14, wherein the binder is selected from the group consisting of fruit pectin, citrus pectin, tobacco pectin, hydroxyethyl guar gum, hydroxypropyl guar gum, hydroxyethyl locust bean gum, hydroxypropyl locust bean gum, alginate, starch, modified starch, derivitized starch, tamarind gum, dextran, pullalon, konjac flour, xanthan gum, and mixtures thereof;

and said tobacco particles having a particle size of 80 mesh or finer.

20. The process as claimed in claim 14, wherein said tobacco particles comprise at least one of tobacco dust, tobacco stem and stemmery discard or a combination thereof.

21. The process as claimed in claim 14, wherein said tobacco particles consists essentially of tobacco dust.

22. The process as claimed in claim 14, wherein said commingling step is performed at an average shear rate in the range of approximately 20 to 50 reciprocal seconds.

23. The process as claimed in claim 3, wherein said second shear of step (b) is at an average shear rate in the range of approximately 600 to 900 reciprocal seconds.

24. The process as claimed in claim 1, wherein the binder is selected from the group consisting of fruit pectin, citrus pectin, tobacco pectin, hydroxyethyl guar gum, hydroxypropyl guar gum, hydroxyethyl locust bean gum, hydroxypropyl locust bean gum, alginate, starch, modified starch, derivitized starch, tamarind gum, dextran, pullalon, konjac flour, xanthan gum, and mixtures thereof.

25. The process as claimed in claim 1, wherein the tobacco particles have a particle size of approximately 80 mesh or finer.

26. The process as claimed in claim 1, wherein the tobacco particles have a particle size of approximately 120 mesh or finer.

27. The process as claimed in claim 1 further comprising the step of adding a humectant at a level of 2 to 4 percent by weight of the reconstituted tobacco material.

28. The process as claimed in claim 1, wherein said tobacco particles comprise at least one of tobacco dust, tobacco stem and stemmery discard or a combination thereof.

29. The process as claimed in claim 1, wherein said tobacco particles consists essentially of tobacco dust.

30. A reconstituted tobacco material constructed by the process set forth in claim 1, said reconstituted tobacco material having a tensile strength of at least 20 kilograms per meter at an average sheet weight of approximately 14.3 g/ft² and with binder consisting essentially of guar.

31. A reconstituted tobacco material constructed by the process set forth in claim 1, said reconstituted tobacco material having a tensile strength of at least 20 kilograms per meter and binder consisting essentially of guar gum, said tobacco material having a maximum wood pulp fiber content of one-half percent by weight of the tobacco material or less.

32. The reconstituted tobacco material as claimed in claim 31 having a maximum wood pulp fiber content less than 0.25% by weight of the tobacco material.

33. The process as claimed in claim 1, wherein said gum consists essentially of guar gum, said first shear of step (a) being at an average shear rate in the range of approximately 100 to 300 reciprocal seconds, said second shear of step (b) being at an average shear rate in the range of approximately 600 to 800 reciprocal seconds.

34. A process of making a reconstituted tobacco material, said process comprising the steps of:

(a) preparing an aqueous binder dispersion by mixing a water-soluble polysaccharide binder under a first shear sufficient to disperse the binder to form an aqueous binder dispersion;

(b) hydrating said aqueous binder dispersion of step (a) by subiecting the aqueous binder dispersion to a second shear so as to produce a hydrated binder solution;

(c) commingling tobacco particles with said hydrated binder solution of step (b) under a low shear so as to form a slurry;

(d) casting the slurry; and

(e) drying the cast slurry to form a reconstituted tobacco material;

wherein said polysaccharide binder comprises guar gum;

wherein said second shear of step (b) is at an average shear rate in the range of approximately 600 to 800 reciprocal seconds;

wherein the first shear of step (a) is at an average shear rate in the range of approximately 100 to 500 reciprocal seconds;

wherein the low shear of the commingling step (c) is at an average rate of about 100 reciprocal seconds or less;

wherein said hydrating step (b) includes removing heat so that the temperature of the binder solution remains below 170°

F.

35. The process as set forth in claim 34, wherein temperature of the binder solution is maintained in the range of approximately 120°

to 140°

F.

36. A process of making a reconstituted tobacco material, said process comprising the steps of:

(a) combining water and a gum binder and applying a first shear to said combined water and gum binder at an average shear rate of approximately 100 to 500 reciprocal seconds, said first shear applying step sufficient to disperse the binder to form an aqueous binder dispersion;

(b) hydrating said aqueous binder dispersion of step (a) by subjecting the aqueous binder dispersion to a second shear at an average shear rate of approximately 500 to 1000 reciprocal seconds so as to produce a hydrated binder solution;

(c) commingling tobacco particles of approximately 80 mesh size or finer with said hydrated binder solution of step (b) under a low shear at an average shear rate of approximately 100 reciprocal seconds or less so as to form an essentially homogeneous slurry, relative proportions of said tobacco particles and said hydrated binder solution of step (b) being selected such that the solids content of said slurry is in the range of approximately 15 to 26%;

(d) casting the slurry; and

(e) drying the cast slurry to form a reconstituted tobacco material.

37. The process as claimed in claim 36, wherein said tobacco particles comprise at least one of tobacco dust, tobacco stem and stemmery discard or a combination thereof.

38. The process as claimed in claim 37, wherein said solids content of the slurry is in the range of approximately 18 to 22%.

39. The process as claimed in claim 36, wherein said tobacco particles consists essentially of tobacco dust.

40. The process as claimed in claim 39, wherein said solids content of the slurry is above 22%.

41. The process as claimed in claim 36, wherein said commingling step is performed at an average shear rate in the range of approximately 20 to 50 reciprocal seconds.

42. A process of making a reconstituted tobacco material, said process comprising the steps of:

combining water and a gum binder and applying a first shear to said combined water and gum binder at an average shear rate of approximately 100 to 500 reciprocal seconds, said first shear applying step sufficient to disperse the binder to form an aqueous binder dispersion;

(b) hydrating said aaueous binder dispersion of step (a) by subjecting the aqueous binder dispersion to a second shear at an average shear rate of approximately 500 to 1000 reciprocal seconds so as to produce a hydrated binder solution;

(c) commingling tobacco particles of approximately 80 mesh size or finer with said hydrated binder solution of step (b) under a low shear at an average shear rate of approximately 100 reciprocal seconds or less so as to form an essentially homogeneous slurry, relative proportions of said tobacco particles and said hydrated binder solution of step (b) being selected such that the solids content of said slurry is in the range of approximately 15 to 26%;

(d) casting the slurry; and

(e) drying the cast slurry to form a reconstituted tobacco material;

wherein said hydrating step (b) includes removing heat so that the temperature of the binder solution remains below 170°

F.

43. The process as claimed in claim 42, wherein said gum consists essentially of guar gum, said first shear of step (a) being at an average shear rate in the range of approximately 100 to 300 reciprocal seconds, said second shear of step (b) being at an average shear rate in the range of approximately 600 to 800 reciprocal seconds.

44. The process as claimed in claim 43, wherein said tobacco particles are of approximately 120 mesh size or finer.

45. The process as claimed in claim 43, wherein said commingling step is performed at an average shear rate in the range of approximately 20 to 50 reciprocal seconds.

46. A process of making a reconstituted tobacco material, said process comprising the steps of:

(a) preparing an aqueous binder dispersion by mixing a water-soluble polysaccharide binder under a first shear sufficient to disperse the binder to form an aqueous binder dispersion;

(b) hydrating said aqueous binder dispersion of step (a) by subjecting the aqueous binder dispersion to a second shear so as to produce a hydrated binder solution;

(c) commingling tobacco particles with said hydrated binder solution of step (b) under a low shear so as to form a slurry;

(d) casting the slurry; and

(e) drying the cast slurry to form a reconstituted tobacco material;

wherein the first shear of step (a) is at an average shear rate in the range of approximately 100 to 300 reciprocal seconds;

wherein the first shear of step (a) forms an aqueous binder dispersion having a solids content of in the range of approximately 1.5% to 1.8% by weight and having a temperature of approximately 120°

F.