Connector for detachable column cartridge for gas chromatograph

• US 5,601,785 A
• Filed: 03/28/1994
• Issued: 02/11/1997
• Est. Priority Date: 12/23/1991
• Status: Expired due to Fees

• Current Assignee: Hewlett-Packard Company (HP Inc.)
• Original Assignee: Microsensor Technology, Inc.
• Inventors: Higdon, William R.
• Primary Examiner(s): Warden, Jill
• Assistant Examiner(s): Ludlow, Jan M.
• Application Number:
  US08/218,605
• Time in Patent Office: 1,051 Days
• Field of Search: 422/103, 422/89, 422/70, 73/23.42, 73/61.56, 96/106, 285/422, 285/423, 285/315, 285/331, 285/382, 285/182, 285/177, 285/915, 210/198.2
• US Class Current: 422/546
• CPC Class Codes: F16L 29/00 Joints with fluid cut-off means quick-acting joints with cut-off means F16L37/28
• CPC Class Codes: G01N 2030/8881 Modular construction, specially adapted therefor
• CPC Class Codes: G01N 30/30 of temperature
• CPC Class Codes: G01N 30/6034 joining multiple columns
• CPC Class Codes: G01N 30/6039 in series
• CPC Class Codes: G01N 30/6078 Capillaries
• CPC Class Codes: G01N 30/6091 Cartridges
• CPC Class Codes: G01N 30/88 Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86

Abstract

A detachable column cartridge for a gas chromatograph is disclosed. The cartridge column contains analytical and reference columns, a heater and a thermocouple, and connects via detachable connectors to a base unit containing an injector, a detector and other components normally found in gas chromatographs. The cartridge arrangement permits a substitute column to be connected to the base unit easily, in the field, when different gases are to be separated and analyzed. Also included are specific connectors for detachably connecting the columns with capillary tubes in the base unit of the gas chromatograph.

Claims

1. A connector joining two capillary tubes, said connector comprising:

first and second fittings, each of said first and second fittings having a tapered bore and an orifice at an end of said bore, said orifice being positioned on an axis of said fitting and on a surface of said fitting;

a first capillary tube inserted into said tapered bore of said first fitting;

a second capillary tube inserted into said tapered bore of said second fitting;

an end of said first capillary tube being spaced apart from said orifice of said first fitting and an end of said second capillary tube being spaced apart from said orifice of said second fitting, said orifice of said first fitting having a diameter no greater than an outside diameter of said first capillary tube and said orifice of said second fitting having a diameter no greater than an outside diameter of said second capillary tube;

a sleeve positioned so as to guide the surface of said first fitting into contact with the surface of the second fitting such that the orifice of the first fitting is aligned with the orifice of the second fitting, the contact between the surfaces of the first and second fittings creating a gas tight seal around said orifices.

2. The connector of claim 1 wherein a sealing layer is deposited on at least one of said surfaces, said layer comprising a material selected from the group consisting of gold, aluminum, nickel, tetrafluoroethylene polymer, polyetherether ketone, and polyimide.

3. The connector of claim 1 wherein a raised ring surrounding said orifice is formed in one of said flat surfaces.

4. The connector of claim 1 wherein said tapered bore is tapered at an angle of approximately 21/2 degrees.

5. The connector of claim 1 wherein at least one of said capillary tubes comprises a chromatographic column.

6. The connector of claim 1 wherein said fittings comprise a ceramic material.

7. The connector of claim 6 wherein said fittings comprise a material selected from the group consisting of zirconia and alumina.

8. The connector of claim 1 wherein at least one of said capillary tubes has an exterior surface coated with a material which forms a bond between said capillary tube and one of said fittings.

9. The connector of claim 8 wherein said material comprises polyimide.

10. The connector of claim 1 wherein said surface of at least one of said fittings is flat.

11. The connector of claim 10 wherein said flat surface is perpendicular to said axis of said fitting.

12. The connector of claim 1 wherein said first fitting is mounted within a male side housing and said second fitting is mounted within a female side housing, said female side housing further comprising said sleeve.

13. The connector of claim 12 wherein an O-ring is fitted into an annular notch adjacent one of said surfaces.

14. The connector of claim 12 further comprising a means for holding said male side housing and said female side housing in juxtaposition.

15. The connector of claim 14 further comprising a spring for maintaining a pressure between said surfaces, said pressure being sufficient to create said gas tight seal.