Flavor encapsulation

• US 5,601,865 A
• Filed: 04/10/1995
• Issued: 02/11/1997
• Est. Priority Date: 09/22/1992
• Status: Expired due to Fees

• Current Assignee: Mccormick & Company Incorporated
• Original Assignee: Mccormick & Company Incorporated
• Inventors: Popplewell, Lewis M., Fulger, Charles V.
• Primary Examiner(s): PADEN, CAROLYN A
• Application Number:
  US08/419,953
• Time in Patent Office: 673 Days
• Field of Search: 426/96, 426/650, 426/651
• US Class Current: 426/650
• CPC Class Codes: A23L 27/00 Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
• CPC Class Codes: A23L 27/70 Fixation, conservation, or encapsulation of flavouring agents
• CPC Class Codes: C13B 50/002 Addition of chemicals or other foodstuffs

Abstract

A process for incorporating a volatile component into a matrix comprising; (a) forming a melt comprising said volatile component and said matrix, (b) solidifying said melt under a pressure sufficient to prevent substantial volatilization of said volatile component.

Claims

1. A process for incorporating a volatile component into a matrix, comprising:

(1) heating and mixing a matrix and a volatile component to obtain a liquid melt comprising said volatile component and said matrix; and

(2) solidifying said melt under a pressure sufficient to prevent substantial volatilization of said volatile component, wherein said solidifying is carried out in a pressure vessel under a pressure which is greater than the vapor pressure of said volatile component at the temperature of said melt, to obtain a dense, amorphous solid directly upon said solidifying said melt, wherein said volatile component is selected from the group consisting of diacetyl and acetaldehyde.

2. The process of claim 1, wherein said pressure is from 2068 to 3275 kPa.

3. The process of claim 1, wherein said melt is formed by:

admixing a solid matrix material with a plasticizer and heating to form a melt;

reducing the pressure on said melt so as to remove any gases present and to volatize at least a portion of said plasticizer and removing said portion from said melt; and

admixing with the resulting melt said volatile component under pressure and temperature conditions sufficient to prevent substantial volatilization of said volatile component.

4. The process of claim 1, wherein said volatile component is acetaldehyde.

5. The process of claim 1, wherein said matrix is selected from the group consisting of maltodextrins, corn syrup solids, maltose syrup solids, high fructose corn syrup solids, starches, hydrocolloids, gums, proteins, partially hydrolyzed proteins, modified proteins, modified hydrocolloids, and modified celluloses.

6. The process of claim 1, wherein less than 50% of said volatile component is volatized during said solidification.

7. The process of claim 1, wherein less than 25% of said volatile component is volatized during said solidification.

8. The process of claim 1, wherein less than 10% of said volatile component is volatized during said solidification.

9. The process of claim 1, wherein said matrix comprises a modified starch.

10. A process of encapsulating materials dissolved in a volatile solvent in a matrix, comprising:

(a) heating and mixing a matrix and a solution of a material dissolved in a volatile solvent to obtain a liquid melt comprising said matrix and said material dissolved in a volatile solvent;

(b) adjusting at least one of the temperature and pressure of said melt to cause at least a portion of said volatile solvent to volatize to form a melt having a reduced solvent content; and

(c) solidifying the resulting melt, wherein after said at a portion of said volatile solvent is removed, a volatile component is introduced into the resulting melt under pressure sufficient to prevent substantial volatilization of said volatile component to obtain a melt containing a volatile component, and said melt containing a volatile component is subsequently solidified under a pressure which is greater than the vapor pressure of said volatile component at the temperature of said melt, wherein said volatile component is selected from the group consisting of diacetyl and acetaldehyde.

11. The process of claim 10, wherein said material dissolved in said volatile solvent is a natural extract and said volatile solvent is water, ethanol or a water-ethanol mixture.

12. The process of claim 10, wherein said material dissolved in said volatile solvent is a meat hydrolysate and said volatile solvent is water.

13. The process of claim 10, wherein said material dissolved in said volatile solvent is an aqueous reaction flavor and said volatile solvent is water.

14. The process of claim 10, wherein said material dissolved in said volatile solvent is a compounded flavor and said volatile solvent is water, ethanol or a water-ethanol mixture.

15. The process of claim 10, wherein said material dissolved in said volatile solvent is vanilla and said volatile solvent is water, ethanol or a water-ethanol mixture.

16. The process of claim 10, wherein the melt is solidified under temperature and pressure conditions sufficient to produce a dense, amorphous solid.

17. The process of claim 10, wherein less than 50% of said volatile component is volatized during said solidification.

18. The process of claim 10, wherein less than 25% of said volatile component is volatized during said solidification.

19. The process of claim 10, wherein less than 10% of said volatile component is volatized during said solidification.

20. The process of claim 10, wherein said matrix comprises a modified starch.