Process and device for producing sintered parts

• US 5,628,045 A
• Filed: 06/07/1996
• Issued: 05/06/1997
• Est. Priority Date: 06/07/1995
• Status: Expired due to Fees

• Current Assignee: QMP Metal Powders GmbH, Sinterwerke Herne GmbH (Sumitomo Corporation)
• Original Assignee: Sinterwerke Herne GmbH (Sumitomo Corporation), Mannesmann AG (Vodafone Group PLC)
• Inventors: Schneider, Rudolf, Lindner, Karl-Heinz
• Primary Examiner(s): Jordan, Charles T.
• Assistant Examiner(s): JENKINS, DANIEL J
• Application Number:
  US08/659,948
• Time in Patent Office: 333 Days
• Field of Search: 419/11, 419/25, 419/57, 425/78, 432/152, 266/257
• US Class Current: 419/25
• CPC Class Codes: C22C 33/02 by powder metallurgy working metallic powder B22F

Abstract

A process for producing sintered parts with high wear resistance and good dynamic strength properties from formed bodies, which have been pressed as green parts from a completely-alloyed air-hardened heat-treatment steel powder with a carbon content of at least 0.3% added in the form of graphite. The process includes sintering the parts under protective gas at a sintering temperature of at least 1000° C. and subsequent cooling. The sintered parts are cooled immediately after sintering from the sintering temperature to a first holding temperature in the range of Ar₃ to a maximum of 150° C. above Ar₃ and are held for a first holding period of 5 to 25 minutes at this temperature (austenitizing phase). Immediately after this, the sintered parts are cooled in accelerated fashion to a second holding temperature by convective gas cooling and are held at this temperature for a second holding period. The second holding temperature lies in a temperature range in which a bainitic structure forms and is of such a length that a bainitic structure portion of at least 50% is established. The sintered parts are then cooled to room temperature.

Claims

1. A process for producing a sintered part with high wear resistance and good dynamic strength properties from a formed body which has been pressed as a green part from a completely-alloyed air-hardened heat-treatment steel powder with a carbon content of at least 0.3% added as graphite, the process comprising the steps of:

sintering the part under protective gas at a sintering temperature of at least 1000°

C.;

immediately cooling, the sintered part from the sintered temperature to a first holding temperature in a range of Ar₃ to a maximum of 150°

C. above Ar₃ and holding the part at the first holding temperature for a first holding period of 5-25 minutes;

cooling the sintered part in an accelerated manner by convective gas cooling to a second holding temperature and holding the cooled part at this temperature for a second holding period, the second holding temperature lying in a temperature range in which a bainitic structure forms, the second holding period having a length so that the part has a bainite structure portion of at least 50%; and

subsequently cooling the part to room temperature.

2. A process as defined in claim 1, wherein the step of cooling the part to a first holding temperature includes cooling to a first holding temperature at a maximum of 50°

-100°

C. above Ar₃.

3. A process as defined in claim 1, wherein the step of cooling the part to a first holding temperature includes holding the part at the first holding temperature for a period of 10-20 minutes.

4. A process as defined in claim 1, wherein the convective gas cooling step is carried out at 3°

-6°

C./s.

5. A process as defined in claim 1, wherein the step of cooling the part to the first holding temperature is carried out at 0.5°

-1.5°

C./s.

6. A process as defined in claim 1, wherein the convective gas cooling step includes holding the part at the second holding temperature for a period so that the bainitic structure portion is no more than 95%.

7. A process as defined in claim 6, convective gas cooling step includes holding the part at the second holding temperature so that the bainitic structure portion is 60-80%.

8. A process as in claim 1, including adjusting the protective gas atmosphere to a C potential that causes a carburization of the sintered part.

9. A device for producing a sintered part with high wear resistance and good dynamic strength properties from a formed body which has been pressed as a green part from a completely-alloyed air-hardened heat-treatment steel powder with a carbon content of at least 0.3% added as graphite, comprising:

an electronically controlled sintering furnace having a sintering zone, a sudden cooling zone located behind the sintering zone and having gas cooling, and a conventional cooling zone located behind the sudden cooling zone;

an austenitizing zone arranged between the sintering zone and the sudden cooling zone; and

a bainitizing zone arranged between the sudden cooling zone and the conventional cooling zone.

10. A device as defined in claim 9, and further comprising an additional conventional cooling zone, the conventional cooling zones being arranged parallel to one another relative to a material flow direction, and still further comprising a cross-transport device arranged so as to feed one of the two conventional cooling zones, the other of the conventional cooling zones being directly attached to the sudden cooling zone so as to permit selective avoidance of the bainitizing zone.

11. A device as defined in claim 10, wherein the cross-transport device is arranged between the sudden cooling zone and the bainitizing zone.

12. A device as defined in claim 11, wherein the additional conventional cooling zone and the bainitizing zone have a parallel transport direction opposite to a transport direction of the sintering zone, the austenitizing zone and the sudden cooling zone.