Concentration of solids in a suspension using hollow fibre membranes

• US 5,643,455 A
• Filed: 02/22/1995
• Issued: 07/01/1997
• Est. Priority Date: 08/07/1991
• Status: Expired due to Term

• Current Assignee: Siemens Industry Incorporated (Siemens AG)
• Original Assignee: Memtel Corporation
• Inventors: Kopp, Clinton Virgil, Doig, Ian Dracup, Streeton, Robert John William, Darzi, Jalel Michel
• Primary Examiner(s): FORTUNA, ANA M
• Application Number:
  US08/185,912
• Time in Patent Office: 860 Days
• Field of Search: 210/636, 210/791, 210/321.78, 210/321.69, 210/323.2, 210/321.79, 210/321.8, 210/321.87, 210/321.88, 210/321.89, 210/333.1, 210/333.07 , 210/650, 210/333.01
• US Class Current: 210/636
• CPC Class Codes: B01D 2315/04 Reciprocation, oscillation or vibration
• CPC Class Codes: B01D 2315/06 Submerged-type; Immersion type
• CPC Class Codes: B01D 2321/04 Backflushing
• CPC Class Codes: B01D 2321/18 Use of gases
• CPC Class Codes: B01D 2321/185 Aeration
• CPC Class Codes: B01D 2321/2066 Pulsated flow
• CPC Class Codes: B01D 65/02 Membrane cleaning or sterilisation ; Membrane regeneration

Abstract

A method of concentrating solids in a liquid suspension using a microporous filter assembly having a plurality of hollow microporous, elastic membranes within a vessel, the method including the steps of applying the suspension to an outer surface of the hollow fibers whereby a portion of the suspension passes through the fibers walls and at least a portion of the solids is retained on or in the hollow fibers or within the vessel as suspended solids; dislodging the retained solids from the fibers by applying a gas under pressure after opening the vessel to atmospheric pressure.

Claims

1. A method of concentrating the solids of a liquid suspension within a vessel consisting of:

(i) applying the liquid suspension under pressure within a vessel to the outer surface of elastic, microporous, hollow fibers or tubular filter elements to induce and sustain filtration through the membrane walls wherein;

(a) some of the liquid suspension passes through the walls the fibers to be drawn off as clarified liquid or filtrate from the hollow fiber lumens, and

(b) at least some of the solids are retained on or in the hollow fibers or otherwise as suspended solids within the liquid of the vessel enclosing the tubular filter elements,

(ii) dislodging the retained solids from the fibers by applying a dislodging medium through the lumens after opening the vessel to atmospheric pressure, wherein the application of the dislodging medium is initially conducted so as to displace liquid within the hollow fiber lumens through the hollow fiber membrane with gas at a pressure below the bubble point of the pores of the fibers followed by subsequent admission to the hollow fiber lumens of gas at a pressure substantially higher than the bubble point of the pores to drive liquid retained in the membrane pores outwards allowing the gas in the lumens to follow the liquid through the fiber walls to provide effective cleaning and scouring event at the most distant point from the lumen inlet thus reducing the natural tendency in a liquid only reverse flow backwash towards preferential washing of pores near the lumen inlet.

2. The method of claim 1 wherein said method is carried out as a continuous process utilising a repetitive cycle of solid accumulation and solid discharge.

3. A method of backwashing a microporous filter said filter having a liquid suspension under pressure within a vessel applied to the outer surface of elastic microporous hollow fibers or tubular filter elements to induce and sustain filtration through the membrane walls, wherein,

(a) some of the liquid suspension passing through the walls of the fibers is drawn off as clarified liquid or filtrate from the hollow fiber lumens and

(b) at least some of the solids being retained on or in the hollow fibers or otherwise as suspended solids within the liquid of the vessel enclosing the tubular filter elements, the method of backwashing including dislodging the retained solids from the fibers by applying a dislodging medium through the lumens after opening the vessel to atmospheric pressure, wherein the application of dislodging medium is initially conducted so as to display liquid within the hollow fiber lumens through the hollow fiber membrane with a gas at a pressure below the bubble point of the pores of the fibers followed by subsequent admission to the hollow fiber lumens of a gas at a pressure substantially higher than the bubble point of the pores, to drive liquid retained in the membrane pores outwardly, allowing gas in the lumens to follow the liquid through the fiber walls to provide effective cleaning and scouring event at the most distant point from the lumen inlet thus reducing the natural tendency in a liquid only reverse backwash towards preferential washing of pores near the lumen inlet.