Device for colorimetric detection of explosives and narcotics

• US 5,648,047 A
• Filed: 03/29/1996
• Issued: 07/15/1997
• Est. Priority Date: 03/29/1996
• Status: Expired due to Fees

• Current Assignee: Israel Levy
• Original Assignee: Israel Levy, Nitza Kardish
• Inventors: Levy, Israel, Kardish, Nitza
• Primary Examiner(s): SNAY, JEFFREY R
• Application Number:
  US08/623,805
• Time in Patent Office: 473 Days
• Field of Search: 422/55, 422/56, 422/57, 422/58, 422/61, 436/44, 436/901, 436/110, 436/92
• US Class Current: 422/411
• CPC Class Codes: G01N 21/29 using visual detection G01N21/31 takes precedence
• CPC Class Codes: G01N 33/0057 Warfare agents or explosives
• CPC Class Codes: Y10S 436/901 Drugs of abuse, e.g. narcotics, amphetamine
• CPC Class Codes: Y10T 436/141111 Diverse hetero atoms in same or different rings [e.g., alkaloids, opiates, etc.]
• CPC Class Codes: Y10T 436/173076 Nitrite or nitrate

Abstract

A hand-held device for rapid colorimertic detection of explosives, narcotics, and other chemicals which can be accurately operated by non-skilled personnel and perform numerous tests in a quick sequential manner without exposing a user to hazardous reagents and without exposing sensitive reagents to deteriorating environmental conditions, the device comprising (a) a housing for handling and using the device, the housing including a sampling area an a testing area; (b) a roll of substrate for sampling materials suspected as including the chemical; (b) a feeding reel being rotatably connected to the housing, the feeding reel being for accommodating the roll of substrate; (c) at least one container for accommodating at least one detecting reagent, the at least one detecting reagent is for the colorimetric detection of the chemical; and (d) at least one dispensing mechanism for dispensing a predetermined volume of the at least one reagent onto the substrate at the testing area.

Claims

1. A hand-held device for colorimetric detection of a chemical obtained by sampling a surface of an object for enabling a large number of tests to be successively performed, the hand-held device comprising:

(a) a housing having means for handling and using the hand-held device, said housing including a sapling area and a testing area, said sampling area being formed as a tip, said tip being dimensioned and positioned for permitting the sampling of the surface of the object by wiping the surface of the object;

(b) a roll of substrate for sampling materials suspected as including the chemical from the surface of the object;

(c) a feeding reel being rotatably connected to said housing, said feeding reel accommodating said roll of substrate, said substrate extending at least from said feeding reel to said tip and said testing area;

(d) at least one container for accommodating at least one detecting reagent, wherein said at least one detecting reagent is for the colorimetric detection of the chemical; and

(e) at least one dispensing mechanism for dispensing a predetermined volume of said at least one reagent onto said substrate at said testing area.

2. A device as in claim 1, wherein said means for handling and using the device include a handle.

3. A device as in claim 1, wherein said substrate is selected from the group consisting of a paper, a cloth and a synthetic membrane.

4. A device as in claim 1, wherein said substrate is supplemented with an adsorbing agent for increased sampling capabilities of said suspected material.

5. A device as in claim 1, wherein said substrate is supplemented with a supporting film.

6. A device as in claim 1, wherein each of said at least one containers is made of an elastic material.

7. A device as in claim 1, wherein at least one of said at least one containers contains at least one breakable ampoule, each of said at least one ampoules contains one of said at least one reagents.

8. A device as in claim 1, wherein the number of containers is selected from the group consisting of one, two, three and four, and each of said containers has a corresponding dispensing mechanism.

9. A device as in claim 1, wherein each of said dispensing mechanisms is formed as a lever system and includes a dispensing button.

10. A device as in claim 1, wherein said feeding reel includes a biasing mechanism for keeping said advancing of said substrate along said sampling area smooth.

11. A device as in claim 1, wherein said housing includes at least one roller for keeping said advancing of said substrate along said sampling area smooth.

12. A device as in claim 1, wherein said housing includes a cover for protecting said substrate.

13. A device as in claim 1, wherein the chemical is an explosive chemical, said at least one reagent is selected from the group consisting of alkaline solution of a diazotizable aminoaromatic azo-dye precursor, an acidic solution containing a nitrate to nitrite ion reducing agent and a diazo-coupler, a zinc powder suspended in a liquid, an aniline salt in a homogenous strongly acidic solution including a water-miscible organic solvent, a 2.5-20% V/V of tetra alkyl phosphonium hydroxide in a solvent including at least 60% V/V dimethyl sulfoxide and about 30% V/V methanol or water, and a 2.5-20% V/V of tetra alkyl ammonium hydroxide in a solvent including at least 60% V/V dimethyl sulfoxide and about 30% V/V methanol or water.

14. A device as in claim 1, wherein the chemical is a narcotic chemical, said at least one reagent is selected from the group consisting of a cocaine visualization reagent, heroin visualization reagent, tetrahydrocannabinol visualization reagent.

15. A device as in claim 1, further comprising:

(f) a take-up reel being rotatably connected to said housing for advancing said substrate along said sampling area into said testing area.

16. A device as in claim 15, wherein said testing area and said take-up real are in said housing, said housing includes a transparent region for permitting a user to view said testing area.

17. A device as in claim 15, wherein said take-up reel includes a ratchet mechanism for stepwise advancing said substrate along said sampling and testing areas.

18. A device as in claim 1, wherein said housing includes a base and a body.

19. A device as in claim 18, wherein said base and body are separatable one from the other.

20. A device as in claim 18, wherein said base and body are rotatable one relative to the other.

21. A device as in claim 1, wherein each of said at least one containers is contained by a tube for directing said each of said at least one reagent to said testing area.

22. A device as in claim 21, wherein each of said tubes has a diameter permitting formation of a capillary effect for effecting said dispensing of said predetermined volume of said at least one reagent onto said substrate at said testing area.

23. A device as in claim 1, wherein said chemical is selected from the group consisting of an explosive chemical and a narcotic chemical.

24. A device as in claim 23, wherein said explosive chemical includes a chemical moiety selected from the group consisting of a nitromatic moiety, organic nitrate moiety, nitramine moiety, inorganic nitrate moiety, chlorate moiety and bromate moiety.

25. A device as in claim 23, wherein said narcotic chemical includes a chemical selected from the group consisting of cannabinoids, cocainoids and heroinoids.

26. A device as in claim 1, wherein the chemical is used during preparation, treatment or storage of narcotic chemicals.

27. A device as in claim 26, wherein the chemical used during preparation, treatment or storage of narcotic chemicals is selected from the group consisting of organic bases and acetic acid.