Method for liquefying starch

• US 5,652,127 A
• Filed: 06/02/1995
• Issued: 07/29/1997
• Est. Priority Date: 06/02/1995
• Status: Expired due to Term

• Current Assignee: Genencor International Incorporated (International Flavors & Fragrances Incorporated)
• Original Assignee: Genencor International Incorporated (International Flavors & Fragrances Incorporated)
• Inventors: Mitchinson, Colin, Solheim, Leif P.
• Primary Examiner(s): Wityshyn, Michael G.
• Assistant Examiner(s): LANKFORD JR, LEON B
• Application Number:
  US08/459,984
• Time in Patent Office: 788 Days
• Field of Search: 435/99, 435/201, 435/72, 435/202, 435/203, 435/204, 435/275
• US Class Current: 435/99
• CPC Class Codes: C08B 30/12 Degraded, destructured or non-chemically modified starch , e.g. mechanically, enzymatically or by irradiation; Bleaching of starch preparation of chemical derivatives of starch C08B31/00
• CPC Class Codes: C12P 19/14 produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase , e.g. by cellulase, hemicellulase

Abstract

According to the invention a method is provided for liquefying starch comprising the steps of adding a sodium composition to the starch prior to or simultaneously with liquefying the starch; adding α-amylase to the treated starch; and reacting the treated starch for a time and at a temperature effective to liquefy the treated starch. Preferred sodium compositions comprise sodium chloride, sodium bicarbonate, sodium benzoate, sodium sulfate, sodium bisulfite, sodium ascorbate, sodium acetate, sodium nitrate, sodium tartrate, sodium tetraborate, sodium propionate, sodium citrate, sodium succinate, monosodium glutamate, trisodium citrate, sodium phosphate or a mixture thereof.

Claims

1. A method for liquefying a starch slurry comprising the steps of:

(a) adding a sodium composition to said starch slurry, wherein a final sodium concentration of said starch slurry is present in a concentration greater than 20 ppm;

(b) adding α

-amylase to said starch slurry; and

(c) incubating said starch slurry with said sodium composition and said α

-amylase for a time and under conditions suitable to liquefy said starch to form a liquefied starch solution;

whereby said step (c) is carried out under conditions such that an anti-oxidant is present in said starch slurry in a concentration less than 5 mM.

2. The method according to claim 1, wherein said sodium composition comprises sodium chloride, sodium bicarbonate, sodium benzoate, sodium sulfate, sodium bisulfite, sodium ascorbate, sodium acetate, sodium nitrate, sodium tartrate, sodium tetraborate, sodium propionate, sodium citrate, sodium succinate, monosodium glutamate, trisodium citrate, sodium phosphate or a mixture thereof.

3. The method according to claim 1, wherein said sodium composition is present in a final concentration of from about 20 ppm to about 10,000 ppm.

4. The method according to claim 1, wherein said sodium composition is present in a final concentration of from about 50 ppm to about 1000 ppm.

5. The method according to claim 1, wherein said sodium composition is present in a final concentration of from about 100 ppm to about 500 ppm.

6. The method according to claim 1, wherein said step (c) is at a pH of less than about 5.9.

7. The method according to claim 1, wherein said step (c) is at a pH between about 4.5 and about 5.7.

8. The method according to claim 1, wherein said step (c) is at a pH of between about 4.5 and about 5.5.

9. The method according to claim 1, wherein said step (a) is prior to said step (b).

10. The method according to claim 1, wherein said step (a) is simultaneous with said step (b).