Apparatus for purifying metal

• US 5,736,096 A
• Filed: 08/02/1996
• Issued: 04/07/1998
• Est. Priority Date: 08/04/1995
• Status: Expired due to Term

• Current Assignee: Sharp Kabushiki Kaisha (Hon Hai Precision Industry Co., Ltd.), Showa Denko KK
• Original Assignee: Sharp Kabushiki Kaisha (Hon Hai Precision Industry Co., Ltd.), Showa Aluminum Corporation (Resonac Holdings Corp.)
• Inventors: Tomita, Takashi, Machida, Tomohiro, Zhang, Jin, Otsuka, Ryotatsu, Nunoi, Tohru
• Primary Examiner(s): KASTLER, SCOTT R
• Application Number:
  US08/691,320
• Time in Patent Office: 613 Days
• Field of Search: 266/200, 266/204, 266/205, 266/227
• US Class Current: 266/205
• CPC Class Codes: C01B 33/037 Purification by zone-melting C30B13/00
• CPC Class Codes: C22B 21/064 using inert or reactive gases C22B21/066 and C22B21/068 take precedence
• CPC Class Codes: C22B 9/05 Refining by treating with gases, e.g. gas flushing also refining by means of a material generating gas in situ
• CPC Class Codes: C22B 9/103 Methods of introduction of solid or liquid refining or fluxing agents

Abstract

A metal purifying apparatus comprises a closed melting furnace equipped with a heater, molten metal holding crucible disposed within the furnace, a vertical hollow rotary shaft penetrating through a top wall of the furnace, a packing sealing off a clearance in the shaft penetrating portion of the top wall around the shaft, rotary drive means for rotatingly driving the shaft, a hollow rotary cooling body fixedly provided at a lower end of the shaft and having an interior space communicating with an interior space of the shaft, and a cooling fluid supply source for supplying a cooling fluid to the interior of the cooling body. The rotary shaft has disposed therein a cooling fluid discharge pipe with a lower end positioned below the top wall of the furnace. An outer periphery of the discahrge pipe and an inner periphery of the shaft are spaced apart from each other and define a space portion providing a cooling fluid supply channel for passing therethrough the cooling fluid to be supplied from the source to the interior space of the cooling body. The discharge pipe has an interior providing a cooling fluid discharge channel for discharging therethrough the cooling fluid supplied to the interior of the cooling body.

Claims

1. A metal purifying apparatus comprising:

a closed melting furnace equipped with heating means;

a molten metal holding crucible disposed within said melting furnace;

a vertical hollow rotary shaft penetrating through a top wall of said melting furnace;

a packing sealing off a clearance around an outer periphery of said rotary shaft in a shaft penetrating portion of said top wall of said melting furnace;

rotary drive means for rotatingly driving said rotary shaft;

a hollow rotary cooling body which is fixedly provided at a lower end of said rotary shaft and which has a hollow interior space in communication with an interior space of said rotary shaft;

a cooling fluid supply source for supplying a cooling fluid to said hollow interior space of said cooling body; and

wherein said cooling body is immersed in a molten metal placed in said crucible and rotated by rotating said rotary shaft by said drive means while said cooling fluid is being supplied to said hollow interior space of said cooling body from said supply source to crystallize a metal of higher purity on an outer periphery of said cooling body, said rotary shaft having disposed therein a cooling fluid discharge pipe with a top end positioned above said top wall of said melting furnace and a lower end positioned below said top wall of said melting furnace, an outer periphery of said discharge pipe and an inner periphery of said rotary shaft being spaced apart from each other to define said interior space in said rotary shaft which provides a cold cooling fluid supply channel for passing therethrough said cooling fluid to be supplied from said supply source to said hollow interior space of said cooling body, said cooling fluid discharge pipe having an interior providing a hot cooling fluid discharge channel for discharging therethrough a hot cooling fluid supplied to said interior of said cooling body and heated by heat from said molten metal.

2. The metal purifying apparatus as defined in claim 1, wherein a single rotary joint has connected thereto an upper end of said rotary shaft and an upper end of said discharge pipe, and said rotary joint comprises a vertical tubular body having a closed upper end and an open lower end and a vertical rotary pipe rotatably supported within a joint body, said rotary pipe having an upper end positioned below a lower surface of an upper end wall of said joint body and a lower end projecting downwardly beyond said joint body, said joint body having a cooling fluid inlet formed in a peripheral wall thereof and positioned above said rotary pipe, said upper end of said discharge pipe being connected to said cooling fluid outlet, an upper end of said cooling fluid supply channel and an upper end of said cooling fluid discharge channel communicating with said inlet and said outlet, respectively.

3. The metal purifying apparatus as defined in claim 1 or 2, wherein said discharge pipe extends downwardly beyond said lower end of said rotary shaft and has a lower end positioned in an interior lower portion of said cooling body, and a cooling fluid discharge member in the form of a tube having a bottom wall, is attached to said lower end of said rotary shaft, said discharge member being positioned within said cooling body and spaced apart from an inner periphery of said cooling body and said outer periphery of said discharge pipe, said discharge member having a multiplicity of said cooling fluid outlet ports formed in said peripheral wall thereof, said discharge pipe having said lower end rotatably fitted in a through hole formed in said bottom wall of said discharge member, said cooling fluid supply channel being in communication with a space portion defined by an inner surface of said peripheral wall of said discharge member and said outer periphery of said discharge pipe.

4. The metal purifying apparatus as defined in claim 3, wherein said discharge member is made of any one of graphite and a ceramic.

5. The metal purifying apparatus as defined in any one of claim 1 or 2, wherein said rotary shaft is provided at a lengthwise intermediate portion thereof with a partition dividing said interior space of said rotary shaft into an upper portion and a lower portion and positioned below said top wall of said melting furnace, said discharge pipe being disposed in said upper interior portion of said rotary shaft above said partition and having said lower end rotatably fitted in a through bore formed in said partition, said cooling fluid supply channel being provided in said upper portion above said partition, a cooling fluid discharge member being disposed in said lower interior portion of said rotary shaft below said partition and a lower end positioned with said cooling body, said discharge member having a double-walled structure comprising inner and outer tubes, said discharge member being provided with a multiplicity of cooling fluid outlet ports in a tube wall forming a lower portion of said outer tube positioned with said cooling body, said cooling fluid supply channel communicating with said space portion defined by said inner and outer tubes via a through hole formed in said partition, said cooling fluid discharge channel communicating with an interior of said inner tube.

6. The metal purifying apparatus as defined in claim 5, wherein said outer tube of said discharge member has an enlarged portion positioned within said cooling body and formed with said cooling fluid outlet ports.

7. The metal purifying apparatus as defined in claim 5, wherein said lower end of said discharge pipe is fitted in said through bore formed in said partition of said rotary shaft, with any one of a graphite and a ceramic ring provided in said bore around said lower end of said discharge pipe.

8. The metal purifying apparatus as defined in any one of claim 1 or 2, wherein said discharge pipe extends downwardly beyond said lower end of said rotary shaft and has said lower end positioned in an interior lower portion of said cooling body, said discharge pipe having an enlarged portion positioned within said cooling body.