Pretreatment of high solid microbial sludges

• US 5,785,852 A
• Filed: 04/06/1995
• Issued: 07/28/1998
• Est. Priority Date: 04/06/1995
• Status: Expired due to Fees

• Current Assignee: Midwest Research Institute
• Original Assignee: Midwest Research Institute
• Inventors: Rivard, Christopher J., Nagle, Nicholas J.
• Primary Examiner(s): Wyse, Thomas G.
• Application Number:
  US08/418,592
• Time in Patent Office: 1,209 Days
• Field of Search: 210/761, 210/603, 210/605, 210/613, 210/630, 210/631, 210/750, 210/766, 210/774
• US Class Current: 210/613
• CPC Class Codes: C02F 11/18 by thermal conditioning by pyrolysis C02F11/10

Abstract

A process and apparatus for pretreating microbial sludges in order to enhance secondary anaerobic digestion. The pretreatment process involves disrupting the cellular integrity of municipal sewage sludge through a combination of thermal, explosive decompression and shear forces. The sludge is pressurized and pumped to a pretreatment reactor where it is mixed with steam to heat and soften the sludge. The pressure of the sludge is suddenly reduced and explosive decompression forces are imparted which partially disrupt the cellular integrity of the sludge. Shear forces are then applied to the sludge to further disrupt the cellular integrity of the sludge. Disrupting cellular integrity releases both soluble and insoluble organic constituents and thereby renders municipal sewage sludge more amenable to secondary anaerobic digestion.

Claims

1. A process for pretreating microbial sludge in order to disrupt cellular integrity of the sludge and enhance secondary anaerobic digestion, comprising:

a) pressurizing and pumping the sludge to be pretreated to a pretreatment reactor;

b) providing steam to the pretreatment reactor;

c) mixing the steam and sludge in the pretreatment reactor to heat the sludge;

d) flashing the sludge to decrease the pressure;

e) applying shear forces to the sludge wherein the cellular integrity of the sludge is disrupted.

2. A process as claimed in claim 1 wherein the flashing of the sludge occurs after the mixing of the steam and sludge in the pretreatment reactor.

3. A process as claimed in claim 1 wherein the applying shear forces occurs after the flashing of the sludge.

4. A process as claimed in claim 1 comprising dewatering the sludge to greater than 10% total solids prior to pressurizing and pumping the sludge to the pretreatment reactor.

5. A process as claimed in claim 1 wherein the step of pressurizing and pumping comprises pressurizing the sludge to a pressure in the range of 100-600 psi.

6. A process as claimed in claim 5 wherein the step of pressurizing and pumping comprises pressurizing the sludge to a pressure of 200-300 psi.

7. A process as claimed in claim 1 wherein the step of mixing the steam and sludge comprises heating the sludge to a temperature in the range of 180°

F.-385°

F.

8. A process as claimed in claim 7 wherein the step of mixing the steam and sludge comprises heating the sludge to a temperature of 250°

F.-350°

F.

9. A process as claimed in claim 1 wherein the sludge to be pretreated has a total solid content of at least 10%.

10. A process as claimed in claim 1 wherein the step of mixing softens the sludge.

11. A process as claimed in claim 1 wherein the pretreatment reactor is a hydroheater.

12. A process as claimed in claim 1 further comprising releasing steam from the sludge during the flashing.

13. A process as claimed in claim 12 further comprising condensing the released steam to any recover ammonia contained therein.

14. The process of claim 1 wherein the step of flashing lowers the pressure of the sludge to atmospheric pressure.

15. The process of claim 1 wherein disruption of the cellular integrity of the sludge releases soluble and insoluble organic constituents of the sludge.

16. The process of claim 1 wherein the flashing imparts explosive decompression forces.

17. A process for treating microbial sludge, comprising:

a) pressurizing and pumping sludge to a pretreatment reactor;

b) providing steam to the pretreatment reactor;

c) mixing the steam and sludge in the pretreatment reactor to heat and soften the sludge;

d) flashing the mixed sludge to lower pressure;

e) applying shear forces to the flashed sludge;

f) treating the sludge after the application of shear forces to secondary anaerobic digestion.

18. The process of claim 17 wherein the sludge has a total solid content of at least 10%.