Method and arrangement for identifying crystalline and polycrystalline materials

• US 5,787,145 A
• Filed: 03/21/1996
• Issued: 07/28/1998
• Est. Priority Date: 03/21/1995
• Status: Expired due to Term

• Current Assignee: Heimann Systems GmbH
• Original Assignee: Heimann Systems GmbH
• Inventors: Geus, Georg
• Primary Examiner(s): Church, Craig E.
• Application Number:
  US08/619,410
• Time in Patent Office: 859 Days
• Field of Search: 378/57, 378/88, 378/71
• US Class Current: 378/71
• CPC Class Codes: G01N 23/201 by measuring small-angle scattering
• CPC Class Codes: G01N 23/207 Diffractometry using detectors, e.g. using a probe in a central position and one or more displaceable detectors in circumferential positions
• CPC Class Codes: G01V 5/222 measuring scattered radiation

Abstract

A method and apparatus is provided for identifying crystalline and polycrystalline material in an object placed in an examination region. X-rays having a polychromatic energy distribution are passed through a diaphragm to create a central x-ray beam in a fan plane that is projected into the examination region for irradiating a cross section of the object. The x-rays are diffracted by individual subregions of the object along the cross section in dependence of the presence of crystalline and/or polycrystalline material in the individual subregions. Collimators with collimating windows are arranged beyond the examination region with respect to the diaphragm, each collimating window covering a fixed, predetermined subregion of the examination region and extracting at least one diffracted plane fan beam from the respective individual subregion of the object. Energy spectra of the diffracted x-ray plane fan beams exiting the respective one of the collimating windows are captured with a detector located behind each of the collimating windows for converting the captured energy spectra into signals usable in a data processing arrangement.

Claims

1. A method for identifying crystalline and polycrystalline material in an object, comprising:

placing the object in an examination region;

passing x-rays having a polychromatic energy distribution through a diaphragm to create a central x-ray beam in a fan plane that is projected into the examination region for irradiating a cross section of the object, the x-rays being diffracted by individual subregions of the object along the cross section in dependence of the presence of at least one of crystalline and polycrystalline material in a respective one of the individual subregions;

arranging collimators with collimating windows beyond the examination region with respect to the diaphragm, each collimating window covering a fixed, predetermined subregion of the examination region and extracting at least one diffracted plane fan beam from the respective individual subregion of the object;

providing a detector comprising a silicon photodiode including an end face having an area of 1 mm² to 5 mm² behind a respective one of the collimating windows so that each diffracted x-ray plane fan beam exiting a respective one of the collimating windows is incident on a respective one of the end faces of the silicon photodiodes; and

capturing energy spectra of the diffracted x-ray plane fan beam exiting a respective one of the collimating windows with a respective one of the silicon photodiodes for converting the captured energy spectra into signals usable in a data processing arrangement.

2. The method according to claim 1, wherein the arranging step includes arranging the collimators in a plane which is perpendicular to the fan plane of the central x-ray fan beam for extracting a predetermined number of diffracted, plane fan beams which are incident symmetrically around the axis of the central x-ray fan beam.

3. The method according to claim 1, wherein the arranging step includes arranging the collimators in parallel behind one another, wherein the diffracted fan beams penetrate collimating windows disposed in parallel in the parallel arranged collimators.

4. The method according to claim 1, wherein the arranging step includes arranging the collimators so that each diffracted beam fan penetrates collimating windows of collimators arranged in parallel behind one another.

5. The method according to claim 1, wherein the arranging step includes arranging the collimators with collimating windows that form x-ray fan beams each having a cross section of with a width of≦

1 mm.

6. The method according to claim 1, wherein the width of the cross section of each x-ray fan beam is in a range between about 0.3 to about 0.5 mm, and the cross section has a height of≦

10 mm.

7. The method according to claim 1, wherein the arranging step includes arranging the collimators so that the collimating windows are at a predetermined fixed angle α

in an angular region between about 2° and

4°

with respect to the axis of the central x-ray fan beam.

8. The method according to claim 7, wherein the angle α

is between about 2.4° and

3°

.

9. The method according to claim 1, wherein the capturing step includes providing the respective silicon photoconductors so that each diffracted fan beam is incident into a plane of a sensitive semiconductor layer of the silicon photodetectors.

10. The method according to claim 9, wherein the thickness of the sensitive semiconductor layer operates to additionally collimate a respective one of the diffracted fan beams.

11. An arrangement for identifying crystalline and polycrystalline material in an object, comprising:

an x-ray source including a diaphragm for projecting a central x-ray beam having a polychromatic energy distribution in a fan plane into an examination region containing the object for irradiating a cross section of the object, the x-rays being diffracted by individual subregions of the object along the cross section in dependence of the presence of at least one of crystalline and polycrystalline material in a respective one of the individual subregions;

collimators arranged beyond the examination region relative to the x-ray source, the collimators being arranged in at least one row symmetrically around the axis of the central x-ray beam in a plane extending perpendicularly to the fan plane of the central x-ray beam and including collimating windows extending in parallel with respect to one another and respectively at a fixed angle α

with respect to the axis of the central x-ray beam, each collimating window covering a fixed, predetermined subregion of the examination region and extracting at least one diffracted plane fan beam from the respective individual subregion of the object; and

detectors each arranged at a respective one of the collimating windows of the collimators in the plane of the respectively collimated fan beam for capturing energy spectra of the diffracted x-ray plane fan beam exiting a respective one of the collimating windows and converting the energy spectra into signals for subsequent use in a data processing arrangement, wherein the detectors each comprises a silicon photodiode including an end face having an area of 1 mm² to 5 mm² behind a respective one of the collimating windows so that each diffracted x-ray plane fan beam exiting a respective one of the collimating windows is incident on a respective one of the end faces of the silicon photodiodes.

12. The arrangement according to claim 11, further comprising a support unit on which the collimators are arranged and a central collimator oriented toward a focus of the x-ray source for automatic orientation and adjustment of the detectors.

13. The arrangement according to claim 11, wherein the central collimator includes a pair of detectors for adjustment and orientation of the other collimators, the pair of detectors being decoupled in terms of their signals.

14. The arrangement according to claim 11, wherein the at least one row of collimators includes multiple rows of collimators arranged one behind another.

15. The arrangement according to claim 11, wherein the fixed angle of inclination α

of the collimating windows of the collimators lies in a range between about 2.4°

to about 3°

.

16. The arrangement according to claim 11, wherein the collimating windows of the collimators have a width of≦

1 mm, and a height of≦

10 mm.

17. The arrangement according to claim 16, wherein the width of the collimating windows is in a range between about 0.3 mm to about 0.5 mm.