Method and apparatus for automatic sample preparation and handling

• US 5,800,777 A
• Filed: 11/13/1996
• Issued: 09/01/1998
• Est. Priority Date: 11/13/1996
• Status: Expired due to Fees

• Current Assignee: Eastman Kodak Company
• Original Assignee: Eastman Kodak Company
• Inventors: Jehan, Howard P.
• Primary Examiner(s): Cain, Edward J.
• Application Number:
  US08/751,531
• Time in Patent Office: 657 Days
• Field of Search: 422/63, 422/65, 422/66, 422/67
• US Class Current: 422/63
• CPC Class Codes: G01N 35/00 Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor

Abstract

A method and apparatus for automatic sample preparation and handling which includes a computer controlled arm capable of both rotary and vertical movement wherein the arm has disposed at the distal end thereof two different part acquisition tools. There is a vacuum cup capable of acquiring sample disks, and there is a pair of tongs movable from a converged, non-engaging position to a diverged engaging position such that sample cups and/or weighted rings can be engaged on an inner surface thereof and lifted. A sample retrieval mechanism delivers individually retrieved samples from a sample magazine to a sample transport mechanism. The sample is then automatically positioned within a punch and a sample disk is punched therefrom. The computer controlled arm then automatically assembles the sample disk in a sample cup and delivers the assembled sample cup to a spectrometer or other downstream test device. When testing of the sample disk is completed, the computer controlled arm automatically reacquires the assembled sample cup from the spectrometer, disassembles the sample cup, and discards the tested sample disk.

Claims

1. An apparatus for automatic sample preparation and handling for a spectrometer, said apparatus comprising:

(a) a housing;

(b) a sample magazine located within said housing, said sample magazine holding a plurality of samples forming a stack;

(c) a sample acquisition system within said housing, said sample acquisition system automatically acquiring an individual one of said samples from the stack of samples;

(d) a sample transport system within said housing, said sample acquisition system delivering said individual ones of said samples to said sample transport system;

(e) a punch mechanism within said housing, said sample transport system automatically positioning said individual ones of said samples of said stack in said punch mechanism, said punch mechanism automatically cutting a sample disk from each of said individual ones of said samples;

(f) a sample assembly/disassembly arm mechanism for automatically acquiring said sample disks from said punch mechanism, preparing each of said sample disks in a sample cup, and delivering said sample cup to a spectrometer.

2. An apparatus as recited in claim 1 wherein:

said sample assembly/disassembly arm mechanism also automatically retrieves said sample cup from the spectrometer and prepares the sample cup for receipt of another sample disk.

3. An apparatus as recited in claim 1 further comprising:

a computer for controlling said sample acquisition system, said sample transport system, said punch mechanism, and said sample assembly/disassembly arm mechanism.

4. An apparatus as recited in claim 1 further comprising:

a magazine holder located at a fixed position within said housing providing residence for said sample magazine.

5. An apparatus for automatic sample preparation and handling for delivery to and from a testing device, said apparatus comprising:

(a) a housing;

(b) a sample magazine located within said housing, said sample magazine holding a plurality of samples forming a stack;

(c) a vacuum pad for acquiring individual ones of said samples from said sample magazine, said vacuum pad mounted on an arm extending from a slide mechanism for moving said vacuum pad in both a horizontal direction and a vertical direction;

(d) a sample transport means within said housing, said sample transport means receiving said individual ones of said samples from said arm mechanism and said vacuum pad;

(e) a punch mechanism within said housing, said sample transport system automatically positioning said individual ones of said samples of said stack in said punch mechanism, said punch mechanism automatically cutting a sample disk from each of said individual ones of said samples;

(f) a sample assembly/disassembly arm mechanism for automatically acquiring said sample disks from said punch mechanism, preparing each of said sample disks in a sample cup and delivering an assembled sample cup to the testing device.

6. An apparatus as recited in claim 5 wherein:

said sample assembly/disassembly arm mechanism also automatically retrieves said assembled sample cup from the spectrometer and disassembles said assembled sample cup in preparation for receipt of another sample disk.

7. An apparatus as recited in claim 5 further comprising:

a computer for controlling said sample acquisition system, said vacuum pad, said slide mechanism, said punch, and said sample assembly/disassembly arm mechanism.

8. An apparatus as recited in claim 5 further comprising:

a magazine holder located at a fixed position within said housing providing residence for said sample magazine.

9. An apparatus as recited in claim 5, said sample assembly/disassembly arm mechanism comprising:

(a) a drive shaft;

(b) means for rotating said drive shaft;

(c) a bracket affixed to said drive shaft;

(d) a tubular sleeve supported at a proximal end thereof from said bracket, said tubular sleeve having a rod inserted therethrough past a distal end of said tubular sleeve;

(e) means mounted to said bracket for rotating said rod within said tubular sleeve;

(f) a pair of tong members supported from said distal end of said tubular sleeve and from said rod, said tong members being spreadable from one another to engage said sample cup on an interior surface thereof in response to rotation of said rod;

(g) a vacuum cup supported proximate said distal end of said tubular sleeve.

10. An apparatus as recited in claim 9, said sample assembly/disassembly arm mechanism further comprising:

(a) a first plate affixed to said rod, said first plate including a first gear edge, one of said pair of tong members attached to said first plate;

(b) a second plate including a second gear edge which intermeshes with said first gear edge, the other of said pair of tong members attached to said second plate.

11. An apparatus as recited in claim 10, said sample assembly/disassembly arm mechanism further comprising:

(a) a bridge bracket affixed to said distal end of said tubular sleeve;

(b) an axle rotatably supported by said bridge bracket, said second plate being affixed to said axle.

12. An apparatus as recited in claim 9, said sample assembly/disassembly arm mechanism further comprising:

(a) a linear slide mechanism mounted within said housing, said linear slide mechanism including a traveling portion positioned to move vertically within said housing;

(b) a frame affixed to said traveling portion, said means for rotating said drive shaft being supported on said frame.

13. An apparatus as recited in claim 9 wherein:

said vacuum cup is attached to a conduit extending downwardly between said pair of tong members such that said vacuum cup projects past said distal ends of said tong members, said tong members and said vacuum cup being simultaneously insertable into the sample cup.

14. An apparatus for automatic sample preparation and handling for delivery to and from a testing device, said apparatus comprising:

(a) a housing;

(b) a sample magazine located within said housing, said sample magazine holding a plurality of samples forming a stack;

(c) a vacuum pad for acquiring individual ones of said samples from said sample magazine, said vacuum pad mounted on an arm extending from a slide mechanism for moving said vacuum pad in both a horizontal direction and a vertical direction;

(d) a sample transport means within said housing, said sample transport means receiving said individual ones of said samples from said arm mechanism and said vacuum pad;

(e) a punch located within said housing, said sample transport means automatically positioning said individual ones of said samples in said punch, said punch automatically cutting a sample disk from each of said samples;

(f) a sample assembly/disassembly arm mechanism for automatically acquiring said sample disks from said punch mechanism, preparing each of said sample disks in a sample cup and delivering an assembled sample cup to the testing device, said sample assembly/disassembly arm mechanism having a grasping tool and a vacuum cup mounted to a distal end thereof, said sample assembly/disassembly arm mechanism capable of vertically displacing and rotating in a horizontal plane said grasping tool and said vacuum cup;

(g) a computer for controlling said sample acquisition system, said vacuum pad, said slide mechanism, said transport means, said punch, and said sample assembly/disassembly arm mechanism.

15. An method for automatic sample preparation and handling for a spectrometer, said method comprising the steps of:

(a) automatically acquiring a substantially planar sample from a stack of samples;

(b) automatically transporting the sample to a punch mechanism;

(c) automatically punching a sample disk from the sample;

(d) automatically delivering the sample disk to a sample cup;

(e) automatically placing a weighed ring in the sample cup on top of the sample disk to yield an assembled sample cup;

(f) automatically delivering the assembled sample cup to a test apparatus.

16. An method as recited in claim 15 further comprising the steps of:

(a) automatically retrieving the assembled sample cup from the test apparatus;

(b) automatically disassembling the assembled sample cup.

17. An method for automatic sample preparation and handling for a spectrometer, said method comprising the steps of:

(a) automatically acquiring a substantially planar sample from a stack of samples with a vacuum pad;

(b) automatically transporting the sample to a punch mechanism;

(c) automatically punching a sample disk from the sample;

(d) automatically delivering the sample disk to a sample cup;

(e) automatically engaging an inner surface of a weighted ring to thereby lift and place the weighted ring in the sample cup on top of the sample disk to yield an assembled sample cup;

(f) automatically engaging an inner surface of the sample cup to thereby deliver the assembled sample cup to a test apparatus.