Apparatus and method for separation of solids from liquid

• US 5,814,230 A
• Filed: 08/30/1996
• Issued: 09/29/1998
• Est. Priority Date: 08/30/1996
• Status: Expired due to Term

• Current Assignee: Tiger Ridge Resources Ltd.
• Original Assignee: Hydrotech Dynamics, Ltd.
• Inventors: Willis, W. Brent, Willis, H. Craig, Willis, Bradley C.
• Primary Examiner(s): Hruskoci, Peter A.
• Application Number:
  US08/697,792
• Time in Patent Office: 760 Days
• Field of Search: 175/66, 175/206, 166/267, 209/5, 209/17, 209/18, 209/44, 209/272, 209/301, 209/308, 210/703, 210/710, 210/712, 210/725, 210/727, 210/728, 210/732, 210/768, 210/770, 210/783, 210/791, 210/803, 210/804, 210/158, 210/160, 210/181, 210/182, 210/195.1 , 210/202, 210/297, 210/324, 210/327, 210/332, 210/333.01, 210/384, 210/391, 210/393, 210/400, 210/408, 210/526, 210/734, 210/748, 210/785, 210/787
• US Class Current: 210/710
• CPC Class Codes: B01D 21/0006 Settling tanks provided with means for cleaning and maintenance
• CPC Class Codes: B01D 21/12 with moving scrapers
• CPC Class Codes: B01D 21/16 provided with flocculating compartments
• CPC Class Codes: B01D 21/183 with multiple scraping mechanisms
• CPC Class Codes: B01D 21/2405 Feed mechanisms for settling tanks
• CPC Class Codes: B01D 21/2427 The feed or discharge opening located at a distant position from the side walls
• CPC Class Codes: B01D 21/2444 Discharge mechanisms for the classified liquid
• CPC Class Codes: B01D 21/2461 Positive-displacement pumps; Screw feeders; Trough conveyors
• CPC Class Codes: B01D 2221/04 Separation devices for treating liquids from earth drilling, mining separation of well effluents E21B43/34, flotation in general B03D1/00
• CPC Class Codes: B01D 33/333 with individual filtering elements moving along a closed path tipping buckets, trays or like sections B01D33/327
• CPC Class Codes: B01D 33/50 with backwash arms, shoes or nozzles
• CPC Class Codes: B01D 33/663 by direct contact with a fluid
• CPC Class Codes: B01D 37/03 using flocculating agents
• CPC Class Codes: E21B 21/066 with further treatment of the solids, e.g. for disposal

Abstract

Method and apparatus are provided for separating coarse and ultrafine solids from a liquid stream to produce a substantially dry solids discharge and a clarified liquid. Apparatus is provided comprising a combination of a settling tank, a plurality of filter screens spaced along an endless link-chain conveyor, a screen vibrator and directed air streams. In operation, coarse solids settle preferentially to the tank bottom. Ultrafines solids remain in suspension. Relatively coarse filter screens are conveyed from a point outside the tank to traverse a prolonged path through the liquid. Ultrafine solids are captured on the screens, by filtering the liquid through an ever finer build-up of filter cake. The relatively large number of passes of the screens through the liquid provides effective filtering of suspended solids. Further, the screens dredge settled solids from the tank bottom. After exiting the liquid, collected coarse and ultrafine solids are dewatered by vibration of the screens and directed blasts of air. Dewatered solids are dumped external to the tank and clarified water is recovered from the tank. Enhanced polymer flocculation may be practised to form flocs from ultrafine solids, after which flocs may be collected (filtered/dredged), dewatered and dumped using the invention. Dewatered solids can further be subjected to compression and decompression cycles to separate even more water from the solids.

Claims

1. A process of separating solids from liquid, the process comprising:

providing a settling tank having sides, a bottom and first and second ends,

flowing liquid containing suspended solids into the tank'"'"'s first end;

maintaining a liquid level in the tank;

separating at least a portion of the suspended solids by gravity which settle onto the tank'"'"'s bottom;

continuously advancing a plurality of spaced-apart screens along an endless path which includes at least descending into the liquid from a first point above the liquid at the tank'"'"'s second end to a second point on the tank'"'"'s bottom, then advancing laterally to a third point on the bottom unique from the second point and adjacent the first end of the tank, and then, ascending to exit the liquid and return to the first point wherein solids are collected on the screens for clarifying the liquid, firstly by dredging solids which have settled by gravity as the screens are advanced along the bottom of the tank between the second and third points, and secondly by filtering progressively finer solids from the suspended solids through the formation of a filter cake of solids on the screens;

substantially dewatering the collected solids by firstly vibrating the solids-containing screens which lay along the ascending portion of the path and are above the liquid level and secondly by directing blasts of air onto the collected solids contained in the screens;

advancing the screens to a fourth point external to the tank;

recovering dewatered collected solids external to the tank by firstly inverting the screens at the fourth point and secondly by directing air onto the back of the inverted screens; and

withdrawing clarified liquid from the second end of the tank at a point adjacent the surface of the liquid.

2. The process as set forth in claim 1 wherein the liquid flowing into the first end of the settling tank discharges adjacent the tank'"'"'s bottom.

3. The process as set forth in claim 2 further comprising:

manipulating the viscosity of the liquid in the tank by mixing substantially solids-free liquid with the liquid flowing into the tank so as to alter the fraction of suspended solids which settle and those which remain in suspension.

4. The process as set forth in claim 3 further comprising:

changing the screen passing size so as to alter the fraction of suspended solids which are filtered by the screens versus those dredged from the tank'"'"'s bottom.

5. The process as set forth in claim 4 further comprising:

flowing the liquid containing suspended solids into a cone-shaped vessel having downwardly converging walls and a lower discharge, said vessel being positioned at the first end of the tank and having its discharge located below the liquid level, adjacent and above the path where the screens begin to ascend, so that liquid flowing into the tank impinges on the ascending screens.

6. The process as set forth in claim 5 further comprising:

spinning the liquid within the cone-shaped vessel so that solids in the liquid are urged outwardly against the downwardly converging walls wherein the solids are concentrated against said walls prior to discharging said concentrated solids downwardly onto the ascending screens.

7. The process as set forth in claim 6 further comprising:

spraying the screens with a substantially solids-free liquid prior to their descending into the tank'"'"'s liquid so as to thoroughly wash them of residual solids, washing liquid and residual solids into the tank.

8. The process as set forth in claim 7 wherein a portion of the solids-free screen washing liquid comprises clarified liquid recycled from the second end of the tank.

9. The process as set forth in claim 8 wherein vibration of the solids-containing screens for dewatering the collected solids is achieved by supporting the screens upon and advancing the screens over a vibrating table.

10. The process as set forth in claim 9 wherein the screens are vibrated at a frequency of about 30 Hz.

11. The process as set forth in claim 9 wherein the liquid flowing into the tank is mixed with a flocculant for the aggregation of at least a portion of the suspended solids into floc, the floc being collected firstly by dredging gravity-settled floc from the tank'"'"'s bottom and secondly by filtering suspended floc with the screens, the collected floc being recovered external to the tank.

12. The process as set forth in claim 11 wherein the screens containing the collected solids, in the form of floc, are vibrated at a frequency which is insufficient to breakdown the floc to release solids from the floc.

13. The process as set forth in claim 1 wherein at least a portion of the liquid containing suspended solids is directed into the tank'"'"'s first end and a solids-concentrated slip-stream of the liquid is discharged adjacent the tank'"'"'s bottom for dredging by the screens.

14. The process as set forth in claim 1 wherein the liquid flowing into the tank is mixed with a flocculant for the aggregation of at least a portion of the suspended solids into floc, the floc and solids being collected firstly by dredging gravity-settled floc and solids from the tank'"'"'s bottom and secondly by filtering suspended floc and solids with the screens, the collected floc being recovered external to the tank.

15. The process as set forth in claim 14 wherein the liquid flowing into the tank is a solids-concentrated underflow from hydroclones.

16. The process as set forth in claim 15 wherein the liquid flowing into the tank originates from the mud sump of an oil well drilling rig.

17. The process as set forth in claim 16 wherein the liquid flowing into the tank originates directly from the active mud system of an oil well drilling rig.

18. The process as set forth in claim 1 wherein the solids contained in the liquid flowing into the tank comprise high-density and low density solids, the high-density solids having both a coarse and a fine fraction, the coarse high-density solids being separately recovered by:

reducing the viscosity of the liquid in the tank so that coarse high-density solids preferentially gravity-settle;

collecting the coarse high-density solids substantially by dredging gravity-settled solids from the tank'"'"'s bottom, dewatering and advancing them external to the tank;

recovering dewatered collected coarse high-density solids external to the tank and withdrawing a clarified liquid which, over time, contains an increasing quantity of residual solids comprising fine high-density solids and low-density solids; and

when the quantity of residual solids is too great,

flocculating the residual solids remaining in the liquid in the tank to aggregate at least a portion residual solids form floc, collecting the floc and residual solids being collected firstly by dredging gravity-settled floc and residual solids from the tank'"'"'s bottom and secondly by filtering suspended floc and residual solids with the screens, recovering a clarified liquid and recovering collected floc and residual solids external to the tank, said collected floc and residual solids being recovered separately from the coarse high-density solids recovered previously.

19. The process as set forth in claim 18 wherein the viscosity of the liquid flowing into the tank is manipulated by commingling with substantially solids-free liquid.

20. A process of treating used mud from an oil well drilling rig for clarification of drilled solids from the mud, said used mud having been prepared in a mud tank and delivered downhole to aid in the drilling process, the used mud returning as liquid containing solids including coarse cuttings and fine solids, the process comprising:

separating coarse cuttings from the used mud by screening to produce a cuttings-free mud;

separating fine solids from the cuttings-free mud using hydroclones to produce a clarified mud and a hydroclone underflow liquid containing fine solids;

recycling the clarified mud to the mud tank for re-use and reconstitution of more mud;

flowing hydroclone liquid underflow containing fine solids into a settling tank, said tank having a bottom and first and second ends and being initially charged with clear water, said hydroclone underflow flowing into said first end;

maintaining a liquid level in the tank by the addition of solids-free liquid as necessary;

separating at least a portion of the fine solids in the tank'"'"'s liquid by gravity;

collecting fine solids by advancing a plurality of spaced-apart screens along an endless path which includes at least descending into the tank'"'"'s liquid from a first point above the liquid at the tank'"'"'s second end to a second point on the tank'"'"'s bottom, then advancing laterally to a third point on the bottom unique from the second point and adjacent the first end of the tank and then ascending to exit the tank'"'"'s liquid and return to the first point wherein solids are collected on the screens to clarify the tank'"'"'s liquid, firstly by dredging fine solids which have settled by gravity as the screens are advanced along the bottom of the tank between the second and third points, and secondly by filtering progressively finer solids from the suspended solids through the formation of a filter cake of fine solids on the screens;

substantially dewatering the collected fine solids by firstly vibrating the solids-containing screens which lay along the ascending portion of the path and are above the liquid level and secondly by directing blasts of air onto the collected fine solids contained in the screens;

advancing the screens to a fourth point external to the tank;

recovering dewatered collected fine solids external to the tank by firstly inverting the screens at the fourth point and secondly by directing air onto the back of the inverted screens;

withdrawing clarified liquid from the second end of the tank at a point adjacent the surface of the liquid; and

recycling the clarified liquid to the mud tank for preparation of more mud.

21. A process as set forth in claim 20 comprising:

mixing a flocculant with the liquid for the aggregation of at least a portion of the fine solids to form floc, said floc and fine solids being processed collectively as solids.

22. A process as set forth in claim 21 comprising:

mixing a selective flocculant with the hydroclone underflow liquid for aggregation of only that portion of the fine solids which are drilled solids to form floc so as to avoid substantial aggregation of fine solids which are beneficial constituents of the mud.

23. A process as set forth in claim 21 wherein the selective flocculant aggregates drilled solids to form floc without substantial aggregation of bentonitic solids.

24. Apparatus for separating solids from liquid including a settling tank, said tank having side walls, a bottom, and first second ends, comprising;

means for feeding liquid into the first end of the tank;

means for maintaining a liquid level in the tank;

a plurality of discrete means spaced on an endless loop of conveyor for screening the tank'"'"'s contents;

means for advancing said conveyor and screening means through the tank;

means for guiding said conveyor along a path which includes at least descending into the liquid from a first point above the liquid at the tank'"'"'s second end to a second point on the tank'"'"'s bottom for traversing the liquid and collecting solids suspended therein, then advancing laterally to a third point on the bottom unique from the second point and adjacent the first end of the tank for collecting settled solids and then ascending to exit the liquid and return to the first point for again traversing the liquid and collecting solids suspended therein;

means for vibrating those screening means which lay along the ascending portion of the path and which are above the liquid level for dewatering of collected solids;

means for directing stream of air onto the contents of the screening means for further dewatering the collected solids;

means associated with the first path point for inverting the screening means to dump the dewatered solids external to the tank;

means for directing air onto the back of the screening means for cleaning residual solids therefrom and dumping them external to the tank; and

means for withdrawing a clarified liquid from the second end of the tank.

25. Separation apparatus as cited in claim 24 wherein the tank'"'"'s side walls slope inwardly towards the bottom, funnelling solids which settle towards the path of the screening means as they advance along the tank'"'"'s bottom.

26. Separation apparatus as cited in claim 25 wherein the endless conveyor comprises link chain, the advancing means comprising a drive sprocket and the guide means comprising the drive sprocket and at least two idler sprockets.

27. Separation apparatus as cited in claim 26 wherein the sprocket at the first point of the path is positioned such that when the buckets round the head sprocket, the screening means project outwards and become inverted for dumping collected solids outside the extents of the second end of the tank.

28. Separation apparatus as cited in claim 27 wherein the screening means comprise a bucket having walls forming a concave pocket which has an opening facing the direction of advance and the bucket walls are formed of screen material, said buckets extending radially outwards from the loop of conveyor so as to depend downwardly from the conveyor while descending and advancing along the tank bottom, and to stand radially upwardly from the conveyor when ascending.

29. Separation apparatus as cited in claim 28 wherein each bucket defines a right prism volume, having a rectangular backing wall, a leading rectangular opening and substantially trapezoidal side walls, each wall formed of replaceable screening material.

30. Separation apparatus as cited in claim 29 wherein the clarified liquid removal means comprises a weir over which clarified water flows.

31. Separation apparatus as cited in claim 30 further comprising

means for collecting the dumped solids;

and

means for advancing the dumped solids to a discharge location remote from the settling tank.

32. Separation apparatus as cited in claim 31 wherein the dumped solids advancing means comprises

means for cyclically subjected the solids to compression and decompression, so that during compression, additional water is separated from the solids to collect along the interface of the solids and pumping means, and during decompression, the liquid drains free of the solids whereby the solids are further dewatered before discharge at the remote location.

33. A process of separating solids from liquid, the process comprising:

providing a settling tank having sides, a bottom and first and second ends;

maintaining a liquid level in the tank;

withdrawing clarified liquid from the second end of the tank at a point adjacent the surface of the liquid;

recycling clarified liquid to the tank'"'"'s first end;

feeding coarse solids contaminated with ultrafine solids to the tank'"'"'s first end;

washing ultrafine solids from the coarse solids by mixing them with the recycled liquid and forming a suspension of ultrafines in the recycled liquid;

flowing the liquid containing washed coarse solids and ultrafine suspension into the tank'"'"'s first end;

separating the coarse solids by gravity so that the coarse solids settle onto the tank'"'"'s bottom;

continuously advancing a plurality of spaced-apart screens along an endless path which includes at least descending into the liquid from a first point above the liquid at the tank'"'"'s second end to a second point on the tank'"'"'s bottom, then advancing laterally to a third point on the bottom unique from the second point and adjacent the first end of the tank, and then, ascending to exit the liquid and return to the first point, the screens having coarse screen openings for passing substantially all solids but the coarse solids, wherein coarse solids are collected on the screens for clarifying the liquid by dredging solids which have settled by gravity and which constitute the largest portion of the coarse solids as the screens are advanced along the bottom of the tank between the second and third points;

advancing the screens to a point external to the tank and dumping collected solids by inverting the screens for recovery of collected, substantially ultrafine-free solids external to the tank;

repeatedly feeding, washing and collecting coarse solids until the concentration of ultrafine solids in the liquid in the tank is such that the coarse solids are which are collected are no longer substantially free of ultrafine solids;

then

discontinuing the feeding of solids to the tank;

mixing a flocculant with the recycled liquid for the aggregation of at least a portion of the ultrafine solids into floc having sufficient bulk to facilitate their collection on the screens;

flowing the liquid containing floc and ultrafine solids into the tank'"'"'s first end and separating at least a portion of the floc and ultrafine solids by gravity which settle onto the tank'"'"'s bottom;

collecting floc and ultrafine solids by continuously advancing the plurality of spaced-apart screens along the endless path wherein floc and ultrafine solids are collected by the screens;

dewatering the collected floc and ultrafine solids by vibrating the solids-containing screens which lay along the ascending portion of the path and are above the liquid level and further by directing blasts of air onto the screen contents; and

advancing the screens to a point external to the tank and dumping the dewatered collected floc and ultrafine solids by inverting the buckets external to the tank and cleaning residual floc and residual ultrafine solids from the screens by directing air onto the back of the screens for recovering the dewatered floc and ultrafine solids external to the tank.