Process for producing cold water soluble tea extract

• US 5,827,560 A
• Filed: 04/14/1997
• Issued: 10/27/1998
• Est. Priority Date: 04/14/1997
• Status: Expired due to Term

• Current Assignee: Nestec SA (Nestle SA)
• Original Assignee: Nestec SA (Nestle SA)
• Inventors: Nickle, Lawrence, Fu, Xiaoping, Rahmani, Rachid, Liu, Richard Tien-Szu
• Primary Examiner(s): Weier, Anthony J.
• Application Number:
  US08/840,157
• Time in Patent Office: 561 Days
• Field of Search: 426/597, 426/435, 426/427, 426/471
• US Class Current: 426/435
• CPC Class Codes: A23F 3/16 Tea extraction; Tea extracts; Treating tea extract; Making instant tea

Abstract

A continuous process for producing a tea extract which contains solubilized tannins and which has good color. Tea solids are extracted from tea leaves using an extraction liquid to provide a tea extract containing soluble tea solids and insoluble tannins. The insoluble tannins are separated from the tea extract and oxidized and solubilized under raised temperature conditions to provide a solubilized tannin liquor. The solubilized tannin liquor is either returned to the extraction liquid during extraction of tea solids or added to the tea extract after separation of the insoluble tannins. The tea extract which contains solubilized tea tannins is collected.

Claims

1. A process for producing a tea extract which contains solubilized tannins, the process comprising:

i) extracting tea solids from tea leaves using an extraction liquid to provide a tea extract containing soluble tea solids and insoluble tannins;

ii) separating the insoluble tannins from the tea extract to obtain a clarified tea extract;

iii) oxidizing and solubilizing the tannins under raised temperature conditions to provide a solubilized tannin liquor; and

iv) adding the solubilized tannin liquor to the extraction liquid during extraction of tea solids from tea leaves in step i); and

v) collecting the clarified tea extract of step ii) to obtain a tea extract which contains solubilized tea tannins.

2. A process according to claim 1 in which the tea solids are extracted from the tea leaves in a series of inter-connected fixed-bed reactors;

the solubilized tannin liquor of step iv) being added to the extraction liquid between one or more adjacent pairs of fixed-bed reactors of the series.

3. A process according to claim 2 in which one of the fixed-bed reactors contains fresh tea leaves and the solubilized tannin liquor is added to the extraction liquid immediately prior to the fixed-bed reactor containing the fresh tea leaves.

4. A process according to claim 1 in which the insoluble tannins are oxidized using a gaseous oxidizing agent.

5. A process according to claim 4 in which the gaseous oxidizing agent is selected from ozone, oxygen and mixtures of these gases with air.

6. A process according to claim 1 in which the temperature at which the insoluble tannins are oxidized is about 80°

C. to about 130°

C.

7. A process according to claim 6 in which the insoluble tannins are oxidized at a pressure of about 1.5 MPa to about 2.0 MPa.

8. A process according to claim 1 further comprising the step of removing acids from at least a portion of the solubilized tannin liquor of step iv) prior to adding the solubilized tannin liquor to the extraction liquid.

9. A process according to claim 8 in which the acids are removed by ultrafiltration of the solubilized tannin liquor, by steam stripping of the solubilized tannin liquor, or by contacting the solubilized tannin liquor with spent tea leaves, or combinations thereof.

10. A process according to claim 1 further comprising separating solubilized tannin liquor of step iv) into a first and a second stream, removing acids from the solubilized tannin liquor in the first stream, and combining the first stream with the second stream prior to adding the solubilized tannin liquor to the extraction liquid.

11. A process according to claim 10 in which the acids are removed by ultrafiltration of the solubilized tannin liquor, by steam stripping of the solubilized tannin liquor, or by contacting the solubilized tannin liquor with spent tea leaves, or combinations thereof.

12. A process for producing a tea extract which contains solubilized tannins, the process comprising:

i) extracting tea solids from tea leaves using an extraction liquid to provide a tea extract containing soluble tea solids and insoluble tannins;

ii) separating the insoluble tannins from the tea extract to obtain a clarified tea extract;

iii) oxidizing and solubilizing the tannins under raised temperature conditions to provide a solubilized tannin liquor;

iv) removing acids from at least a portion of the solubilized tannin liquor; and

v) adding the solubilized tannin liquor to the extraction liquid during extraction of tea solids from tea leaves in step i); and

vi) collecting the clarified tea extract of step ii) to obtain a tea extract which contains solubilized tea tannins.

13. A process according to claim 12 in which the tea solids are extracted from the tea leaves in a series of inter-connected fixed-bed reactors;

the solubilized tannin liquor of step v) being added to the extraction liquid between one or more adjacent pairs of fixed-bed reactors of the series.

14. A process according to claim 13 in which one of the fixed-bed reactors contains fresh tea leaves and the solubilized tannin liquor is added to the extraction liquid immediately prior to the fixed-bed reactor containing the fresh tea leaves.

15. A process for producing a tea extract which contains solubilized tannins, the process comprising:

i) extracting tea solids from tea leaves in a series of inter-connected fixed-bed reactors using an extraction liquid to provide a tea extract containing soluble tea solids and insoluble tannins;

ii) separating the insoluble tannins from the tea extract;

iii) oxidizing and solubilizing the tannins under raised temperature conditions to provide a solubilized tannin liquor; and

iv) adding the solubilized tannin liquor to the extraction liquid between one or more adjacent pairs of fixed-bed reactors of the series during extraction of tea solids from tea leaves in step i); and

v) collecting the tea extract of step ii) which contains solubilized tea tannins.

16. A process according to claim 15 further comprising the step of removing acids from at least a portion of the solubilized tannin liquor prior to adding the solubilized tannin liquor to the extraction liquid.

17. A process according to claim 16 in which the acids are removed by ultrafiltration of the solubilized tannin liquor, by steam stripping of the solubilized tannin liquor, or by contacting the solubilized tannin liquor with spent tea leaves, or combinations thereof.