Method for dispersing cellulose based fibers in water

• US 5,849,155 A
• Filed: 11/06/1995
• Issued: 12/15/1998
• Est. Priority Date: 02/02/1993
• Status: Expired due to Fees

• Current Assignee: E. Khashoggi Industries, LLC
• Original Assignee: E. Khashoggi Industries, LLC
• Inventors: Gasland, Stein
• Primary Examiner(s): Alvo, Steven
• Application Number:
  US08/500,890
• Time in Patent Office: 1,135 Days
• Field of Search: 162/101, 162/145, 162/146, 162/147, 162/158, 162/168.1, 162/174, 162/177, 162/178, 162/218, 162/183, 264/165, 264/175, 264/176.1, 264/204
• US Class Current: 162/158
• CPC Class Codes: C08L 2666/02 Organic macromolecular compounds, natural resins, waxes or and bituminous materials
• CPC Class Codes: C08L 3/02 Starch; Degradation products thereof, e.g. dextrin
• CPC Class Codes: D21B 1/342 Mixing apparatus
• CPC Class Codes: D21F 1/0018 Devices for dispensing fibres in a fluid
• CPC Class Codes: D21H 11/14 Secondary fibres working-up waste paper D21C5/02
• CPC Class Codes: D21H 17/28 Starch
• CPC Class Codes: D21H 23/16 Addition before or during pulp beating or refining disintegrating fibrous raw materials in mills in the presence of chemical agents D21B1/16; methods of beating D21D1/02; methods of refining D21D1/20

Abstract

The invention describes a method for dispersion of cellulose based fibers in water. The raw material, which particularly may be recycled paper, is first wetted with water. By a combination of addition of hydrocolloid which binds water, and strong kneading at high solid content, the mixture is transformed into a modulable paste. The high viscosity of the paste effectively conveys the shear forces of the kneading machine to make the fibers flexible and tear them apart. When the kneading is terminated, the hydrocolloid prevents the fibers from reassociation into fiber bundles.

Claims

1. A method for dispersing cellulose based fibers in water comprising the steps of:

combining together water, a fibrous material, and a hydrocolloid to form an initial fibrous mixture in which the fibrous material is not initially dispersed in the water and has an initial solids content in a range from about 35% to about 80% by weight of the initial fibrous mixture, wherein sufficient hydrocolloid is included so as to bind substantially all of the water;

kneading the initial fibrous mixture using strong mechanical action in order to liberate and disperse individual fibers from the fibrous material and form a final fibrous mixture in which the fibers are substantially dispersed throughout the final fibrous mixture; and

shaping the final fibrous mixture into a desired shape by a process selected from the group consisting of extrusion, injection molding, coating, pressing, rolling, and combinations thereof.

2. A method as defined in claim 1, wherein the hydrocolloid is included in the initial fibrous mixture at a sufficient initial concentration such that all of the water is completely bound within the initial fibrous mixture.

3. A method as defined in claim 2, wherein the weight of the hydrocolloid in the initial fibrous mixture is in a range from about 0.4% to about 20% of the weight of the water that is initially included in the initial fibrous mixture.

4. A method as defined in claim 1, wherein dispersion of the fibers during the kneading step is conducted at a temperature of about 200°

C. or less.

5. A method as defined in claim 1, wherein the fibrous material comprises fibers that are selected from the group consisting of cellulose, semichemical cellulose, groundwood, and recycled paper.

6. A method as defined in claim 1, wherein the hydrocolloid comprises starch or a starch derivative.

7. A method as defined in claim 1, wherein the hydrocolloid is initially added to the initial fibrous mixture in an ungelatinized form, and is thereafter gelatinized by supplying thermal energy to the fibrous mixture.

8. A method as defined in claim 1, further including the step of heating the fibrous mixture in order to evaporate a portion of the water in order to further increase the solids concentration.

9. A method as defined in claim 1, wherein the hydrocolloid is selected from the group consisting of polyvinyl alcohol, cellulose derivatives, proteins, vegetable gums, synthetic hydrocolloids, and flours.

10. A method as defined in claim 1, further comprising the step of adding to the fibrous mixture a material selected from the group consisting of waxes, latex emulsions, and combinations of the foregoing.

11. A method for dispersing cellulose based fibers in water comprising the steps of:

combining together water, a fibrous material, and a hydrocolloid to form an initial fibrous mixture in which the fibrous material is not initially dispersed in the water and having an initial solids content in a range from about 40% to about 80% by weight of the initial fibrous mixture, wherein sufficient hydrocolloid is included so as to bind substantially all of the water;

kneading the initial fibrous mixture using strong mechanical action in order to liberate and disperse individual fibers from the fibrous material and form a final fibrous mixture in which the fibers are substantially dispersed throughout the final fibrous mixture while heating the final fibrous mixture in order to evaporate a portion of the water in order to further increase the solids concentration; and

shaping the final fibrous mixture into a desired shape by a process selected from the group consisting of extrusion, injection molding, coating, pressing, rolling, and combinations thereof.

12. A method as defined in claim 11, wherein the amount of hydrocolloid initially included in the initial fibrous mixture is sufficiently high such that all the water is completely bound within the initial fibrous mixture.

13. A method as defined in claim 11, wherein dispersion of the fibers during the kneading step is conducted at a temperature no greater than about 200°

C.

14. A method as defined in claim 11, wherein the fibrous material comprises fibers that are selected from the group consisting of cellulose, semichemical cellulose, groundwood, and recycled paper.

15. A method as defined in claim 11, wherein the hydrocolloid comprises starch or a starch derivative.

16. A method as defined in claim 11, wherein the hydrocolloid is selected from the group consisting of polyvinyl alcohol, cellulose derivatives, proteins, vegetable gums, synthetic hydrocolloids, and flours.

17. A method as defined in claim 11, wherein the hydrocolloid is initially added to the initial fibrous mixture in an ungelatinized form, and is thereafter gelatinized by supplying thermal energy to the fibrous mixture.

18. A method for dispersing cellulose based fibers in water, comprising the steps of:

combining water, a fibrous material comprising agglomerated fibers, and a hydrocolloid to form an initial fibrous mixture in which the fibrous material is not initially dispersed in the water, the hydrocolloid being included at a sufficient concentration such that the water is completely bound within the initial fibrous mixture, wherein the fibrous material is included in an amount in a range from about 35% to about 80% by weight of the initial fibrous mixture;

kneading the initial fibrous mixture at a temperature of less than about 200°

C. using strong mechanical action in order to liberate and disperse individual fibers from the fibrous material and form a final fibrous mixture in which the fibers are substantially dispersed throughout the final fibrous mixture while heating the fibrous mixture in order to evaporate a portion of the water in order to further increase the solids concentration; and

shaping the final fibrous mixture into a desired shape by a process selected from the group consisting of extrusion, injection molding, coating, pressing, rolling, and combinations thereof.