Method of molding powdered plant fiber into high density materials

• US 5,855,832 A
• Filed: 06/27/1996
• Issued: 01/05/1999
• Est. Priority Date: 06/27/1996
• Status: Expired due to Term

• Current Assignee: Robert N. Clausi
• Original Assignee: Robert N. Clausi
• Inventors: Clausi, Robert N.
• Primary Examiner(s): Turner, A. A.
• Assistant Examiner(s): GRAY, JILL M
• Application Number:
  US08/670,158
• Time in Patent Office: 922 Days
• Field of Search: 264/109, 264/113, 264/118, 264/119, 264/120
• US Class Current: 264/109
• CPC Class Codes: B27N 3/02 from particles
• CPC Class Codes: Y10T 428/249921 Web or sheet containing structurally defined element or component
• CPC Class Codes: Y10T 428/249925 Fiber-containing wood product [e.g., hardboard, lumber, or wood board, etc.]
• CPC Class Codes: Y10T 428/25 Web or sheet containing structurally defined element or component and including a second component containing structurally defined particles
• CPC Class Codes: Y10T 428/26 Web or sheet containing structurally defined element or component, the element or component having a specified physical dimension
• CPC Class Codes: Y10T 428/27 Web or sheet containing structurally defined element or component, the element or component having a specified weight per unit area [e.g., gms/sq cm, lbs/sq ft, etc.]
• CPC Class Codes: Y10T 428/29 Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
• CPC Class Codes: Y10T 428/2973 Particular cross section

Abstract

A high density fiber product is made from natural lignin containing plant fibers. Plant fibers ranging in size below about 3000 microns in diameter are used. Binding agents and other additives may be mixed with the fibers to enhance product or process performance. The plant fibers or mixture of fibers and additives are heated to between about 50 degrees C. to about 140 degrees C. The heated fibers are compressed in a mold to an average density of about 50 pounds per cubic foot to about 100 pounds per cubic foot. Compression pressures of about 500 psi to about 2500 psi are used to achieve product densities within this range. The compressed fibers are cured under these temperature and pressure conditions. After the curing time has elapsed, the compressed fiber product is released from the mold and the mold may be reused. A high density product made from small plant fibers is provided.

Claims

1. A method of manufacturing a high density plant fiber material comprising the steps of:

(a) introducing powdered plant fiber particles containing protolignin and with a diameter less than 3000 microns into a mold;

(b) heating the contents of the mold to a temperature between 50 degrees C. to 220 degrees C.;

(c) compressing the powdered contents of the mold to an average density of at least 50 pounds per cubic foot;

(d) curing the compressed contents within the mold; and

(e) releasing the compressed contents from the mold.

2. The method of claim 1 wherein the contents of the mold are heated to a temperature between 50 degrees C. to 140 degrees C.

3. The method of claim 2 wherein the contents of the mold are heated to a temperature between 60 degrees C. and 140 degrees C.

4. The method of claim 3 wherein the plant fibers are preheated to a temperature of between 40 degrees C. to 60 degrees C.

5. The method of claim 2 wherein the plant fibers are preheated prior to introduction into the mold.

6. The method of claim 2 comprising the step of mixing a thermoset binding agent with the powdered plant fibers prior to introducing the fibers into the mold.

7. The method of claim 6 comprising the step of adding a release agent to the binding agent and powdered plant fiber mixture.

8. The method of claim 6 comprising the step of adding a catalyst to the binding agent and powdered plant fiber mixture.

9. The method of claim 2 wherein the contents of the mold are compressed to an average density of between 50 pounds per cubic foot and 100 pounds per cubic foot.

10. The method of claim 9 comprising the step of introducing reinforcing material into the mold prior to introducing the plant fiber particles into the mold.

11. The method of claim 9 wherein the contents of the mold are heated to a temperature between 50 degrees C. and 100 degrees C.

12. The method of claim 9 comprising the step of blending a thermoset resin and one or more of the group of additives consisting of a pigment, a releasing agent, a catalyst, a flame retardant, a flame resistant agent, a fire resistant agent, and a lubricating agent with the plant fiber material prior to introducing the plant fibers into the mold.

13. The method of claim 12 wherein the plant fiber particles are between 150 microns to 1500 microns in diameter.

14. The method of claim 12 wherein the plant fibers comprise fibers from one or more of the group of fibers consisting of wood flour, straw, hemp, jute, pecan shells, walnut shells, and mixed agricultural fibers.

15. The method of claim 12 comprising the step of introducing at least one non deformable member into the mold before introducing the plant fibers into the mold.

16. The method of claim 12 wherein the binding agent is a thermoset resin.

17. The method of claim 16 wherein the resin is one or more of the group of additives consisting of unsaturated polyester resin, polymeric diphenyl methane di-isocyanate, methane di-isocyanate, melamine, urea, ester containing compounds, urea formaldehyde, and melamine-formaldehyde.

18. The method of claim 9 comprising the step of coating the cavity of the mold with a surface additive prior to introducing the plant fibers into the mold.

19. The method of claim 9 comprising the step of taking the compressed contents of the mold and introducing the contents into a second mold, pressing the contents to a higher density, curing the compressed contents of the second mold, and releasing the contents from the second mold.

20. The method of claim 19 wherein a surface additive is applied to the surface of the mold cavity prior to introducing the contents of the first mold into the second mold.

21. The method of claim 19 comprising the step of introducing plant fiber material into the second mold before the step of introducing the contents of first mold.

22. The method of claim 9 wherein the contents of the mold are compressed by applying a surface pressure of at least 500 psi.

23. The method of claim 22 wherein the water content of the plant fibers is between 5 per cent to 20 per cent by weight.

24. The method of claim 23 comprising the step of introducing a thermoset binding agent and a release agent to the plant fibers before the fibers are introduced to the mold.

25. The method of claim 24 wherein the concentration of binding agent is between 0.25 per cent and 20 per cent by weight of plant fiber mixture.

26. The method of claim 25 wherein the contents of the mold are heated to a temperature between 50 degrees C. and 100 degrees C.

32. A product of any of the methods of claims 1 to 31.

27. A method of forming a high density plant fiber product comprising the steps of:

(a) providing plant fibers containing protolignin and containing less than 20 per cent water by weight, the fibers being between 50 microns to 3000 microns in diameter;

(b) blending a fluidized mixture of plant fibers and one or more of the group of additives consisting of a thermoset binding agent, a pigment, a releasing agent, a catalyst, a flame retardant, a flame resistant agent, a fire resistant agent, and a lubricating agent;

(c) introducing the fluidized mixture of plant fibers and additives into the cavity of a mold;

(d) compressing the mixture by applying a pressure of at least 500 psi to the surface of the mixture;

(e) heating the contents of the mold cavity to between 50 degrees C. to 220 degrees C.;

(f) curing the compressed contents; and

(g) removing the compressed contents from the mold.

28. The method of claim 27 wherein the contents of the mold are heated to a temperature of between 50 degrees C. and 140 degrees C.

29. The method of claim 28 wherein the binding agent is one or more of the group of agents consisting of unsaturated polyester resin, polymeric diphenyl methane di-isocyanate, methane di-isocyanate, melamine, urea, ester containing compounds, urea formaldehyde, and melamine-formaldehyde.

30. The method of claim 28 wherein the blended mixture of plant fibers and additives are preheated to a temperature of between 40 degrees C. to 60 degrees C.

31. The method of claim 28 wherein the contents of the mold are heated to a temperature of between 60 degrees C. and 100 degrees C.

33. A method of manufacturing a high density plant fiber material comprising the steps of:

(a) preparing a particulate mixture comprising plant fibers less than 1500 microns in diameter and containing protolignin, a thermoset binding agent, and one or more of the group of additives consisting of a pigment, a releasing agent, a catalyst, a flame retardant, a flame resistant agent, and a lubricating agent;

(b) introducing the particulate mixture into a mold;

(c) heating the particulate mixture to a temperature between 60 degrees C. and 220 degrees C.;

(d) compressing the mixture to an average density of at least 60 pounds per cubic foot within the mold; and

(e) removing the compressed contents from the mold.

34. The method of claim of 33 wherein the particulate mixture is compressed in a single step to an average density of at least 60 pounds per cubic foot.

35. The method of claim 34 wherein the thermoset binding agent is at least one of the group of agents consisting of unsaturated polyester resin, polymeric diphenyl methane di-isocyante, methane di-isocyante, melamine, urea, ester containing compounds, urea formaldehyde, and melamine-formaldehyde.

36. The method of claim 35 wherein the concentration of binding agent is less than 50 per cent by weight of plant mixture.

37. The method of claim 35 wherein the concentration of binding agent is less than 30 per cent by weight of plant fiber mixture.

38. The method of claim 35 wherein the concentration of binding agent is less than 10 per cent by weight of plant fiber mixture.

39. The method of claim 36, 37, or 38, wherein the plant fiber mixture is compressed to an average density of at least 80 pounds per cubic foot.

40. The method of claim 39 wherein the compressed plant fiber mixture is cooled under controlled conditions.