Procedure and device for the measurement of water vapor transfer through textiles and other plate-like materials

• US 5,907,091 A
• Filed: 10/20/1997
• Issued: 05/25/1999
• Est. Priority Date: 10/26/1996
• Status: Expired due to Term

• Current Assignee: Barbara Hildegard Pause
• Original Assignee: Barbara Hildegard Pause
• Inventors: Pause, Barbara Hildegard
• Primary Examiner(s): Williams, Hezron
• Assistant Examiner(s): WIGGINS, JOHN DAVID
• Application Number:
  US08/954,017
• Time in Patent Office: 582 Days
• Field of Search: 73/38, 73/40, 73/29.01, 73/73
• US Class Current: 73/38
• CPC Class Codes: G01N 15/082 Investigating permeability by forcing a fluid through a sample
• CPC Class Codes: G01N 33/367 Fabric or woven textiles optical analysis of moving sheets G01N21/86

Abstract

The invention provides a method for measurement of characteristics related to water vapor transfer through plate-like material samples, in particular textile materials, and a measuring unit device with a water container, a water container atmosphere or headspace, air chamber, and measuring chamber, where the water container headspace and air chamber are separated by such plate-like material sample for carrying out such measurements under stationary air flow conditions according to detecting an absolute humidity increase of 1% in an air chamber atmosphere, and where determinations of water vapor transmission rate, water vapor resistance, water vapor permeability and water vapor pressure differential across the plate-like material sample are obtained via use of appropriate sensors installed within the housing of such testing device, including air temperature and humidity sensors, water temperature sensor, and an evaporative heat flux thermal sensor.

Claims

1. A process for simultaneous determination of two or more characteristics related to water vapor transfer through plate-like samples, in particular textile materials, which requires the steps of:

(a) arranging the test sample atop of a container of water at a certain temperature located at the bottom of a measuring chamber possessing a certain air volume in an air chamber at a certain air temperature and a defined starting humidity;

(b) measuring the humidity change in the measuring chamber over a time interval which occurs when water vapor penetrates the test sample as a result of the difference in water vapor pressure between the water bath and the chamber air;

(c) calculating two or more characteristics related to water vapor transfer using the absolute humidity gain in the air volume within the measuring interval, the difference in water vapor pressure and a thermal measurement of any evaporative heat flux evolved during the water vapor transfer thru such textile test sample.

2. The process according to claim 1 where the characteristics related to water vapor transfer are the water vapor transmission rate, the water vapor resistance and the water vapor permeability.

3. The process according to claim 2 where the water vapor transmission rate is calculated using the absolute humidity gain in the air volume per measuring interval and sample area which is penetrated by the water vapor.

4. The process according to claim 2 where the water vapor resistance is determined using the calculated water vapor transmission rate, the water vapor pressure difference and the evaporative heat flux.

5. The process according to claim 2 where the water vapor permeability is determined using the calculated water vapor resistance and the evaporative heat flux.

6. The process according to claim 1 where the measuring conditions such as starting humidity and air temperature in the measuring chamber as well as the water bath temperature can be varied by moistening or drying the chamber air and by preheating the water bath and the chamber air prior to initiating the measurement process.

7. The process according to claim 1 where a humidity measurement is carried out at point suspended within chamber air of said measuring chamber and the temperature measurements are made at points suspended within chamber air of said measuring chamber and at a location within the water in said container.

8. The process according to claim 1 where the characteristics related to water vapor transfer through the test sample are determined from a very slight variation in humidity within the measuring chamber and under constant air and water temperatures.

9. A measuring unit for measuring characteristics related to water vapor transfer through test samples under stationary air flow conditions, said measuring unit consisting of an open liquid water supply measuring chamber with an overhead air space of chamber air, within which device the following components are situated during an assessment of water vapor permeability properties for said test samples:

a container completely full of water serving also as a water bath, a sample holder for ensuring proper positioning of said test samples, a means for performing a sample exchange between different pairs of said test samples, a temperature measuring sensor for said water bath, air temperature and humidity measuring sensors for said chamber air as well as means used to vary chamber air conditions such as humidity and temperature where said container of water is situated beneath said test samples and is disposed at the bottom of said measuring chamber.

10. The device according to claim 9 in which the sample is affixed to a sample holder in such way as to completely cover the water container and separate the water container and water vapor in a container atmosphere above the level of water in said water container from said measuring chamber.

11. The device according to claim 9 equipped with a slide-type mechanism to carry out the sample exchange, thereby preventing any undesired water vapor transfer prior to measurement initiations.

12. The device according to claim 9 where the sample lies atop a fine mesh lattice during the measurement to maintain a constant water vapor transfer to the sample.

13. The device according to claim 9 where the measuring unit is equipped with a moistening and drying system which is used to obtain a desired starting humidity and to dry the chamber air upon measurement completion and that the moistening and drying system consists of canisters containing chemical solutions immersed therein, and the device includes means to measure, which solutions are covered with plates capable of providing a sealing function, the opening and closing of which is controlled by computer.

14. The device according to claim 9 where the measuring unit is equipped with a heating system for preheating the water bath and chamber air.

15. The device according to claim 9 where the temperature of the water bath is measured with a temperature sensor, and the chamber air temperature and humidity are measured by a second sensor capable of measuring both conditions simultaneously.

16. The device according to claim 9 further having an amplification and a control system as well as a computer for calculating, recording, processing and performing assessment of the measured values including said water temperature, air temperature and humidity conditions, water vapor permeation properties and water vapor transfer characteristics such as water vapor transmission rate and water vapor resistance.